1 Measurement Techniques Technical Information and Some Hints for the Reports Practical Measurement Techniques, University of Bremen, summer 2014 Andreas Richter room U2090 tel: Christian Mertens room M 3140 Tel:

General Information I The Measurement Techniques course consists of a series of lectures about selected measurement techniques in environmental science a series of lectures related to the lab experiments the lab experiments an oral exam at the end - 2 -A. Richter & C. Mertens, Measurement Techniques summer 2014

Preliminary Time Schedule: Lectures - 3 -A. Richter & C. Mertens, Measurement Techniques summer :15– 10:4511:15 – 12:4514:15 – 15:4516:00 – 17:00 April 23 Introduction / DOASDOAS (Mertens / Richter) Absorption Spectroscopy (Gorshelev) Measurements of Trace Gases (Richter) Safety instructions (Thomssen) April 30 Measurement Techniques in Oceanography (Mertens) Radioactivity (Pittauerova) Satellite Image Analysis (Melsheimer) May 7 Cavity Ring Down Spectroscopy (Horstjann) Fourier Transform Spectroscopy (Petri) Meteorological Measurements (Richter)

General Information I In total 4 lab experiments have to be completed successfully The labs will take place on Wednesdays from 10 a.m. until 5 p.m. if not stated otherwise The labs will be performed in groups of 2 students each Lab instructions, including descriptions of the experimental setup, the tasks to be performed and further literature are available for every experiment on the Measurement Techniques website A. Richter & C. Mertens, Measurement Techniques summer 2014

General Information II Please get a copy of the lab instructions from the web at least 2 weeks before the lab takes place At least one week before the labs take place contact the lab instructor about the exact time and location of the lab, and perhaps have a first look at the instruments you will use For each lab experiment a lab report / protocol has to be written - 5 -A. Richter & C. Mertens, Measurement Techniques summer 2014

General information III The complete reports have to be handed in 2 weeks after the lab to the tutor If the report is not accepted by the lab instructor it can be corrected no more than twice within two weeks after receiving it from the lab instructor A special report form will accompany you through the practical and the review process. This form will be given to you during the first lab and has to be handed in at the end of semester You will need this report with all signatures to receive the credit points for this course - 6 -A. Richter & C. Mertens, Measurement Techniques summer 2014

General information IV Note: If you:  fail to show up,  are not prepared appropriately,  submit a revised report which is still not accepted by the instructor you will have to do an additional experiment at the end of the semester to be admitted for the exam. Extra experiments can only be done once and should you fail this one also, you will not pass the course A. Richter & C. Mertens, Measurement Techniques summer 2014

Safety Considerations In this set of experiments, you will not be exposed to undue danger by inflammable or hazardous material or ionizing or other harmful radiation. However, you should be aware of some general safety considerations.  Don‘t eat or smoke (this might damage the experiment).  If anything is defect, inform your tutor immediately.  Never construct, modify, or disconnect electrical circuits under voltage applied.  Never look into laser beams.  Be informed about emergency exits and fire extinguisher sites.  On alert, immediately leave the lab room.  Don‘t cause danger to yourself or anybody else ! - 8 -A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy - 9 -A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

The available Experiments Satellite Image Analysis Natural and man-made radioactivity in soil DOAS (Differential Optical Absorption Spectroscopy) measurements of stratospheric species Acoustic Current Measurements FTS Measurements Cavity Ring Down Measurements Ozone Absorption Spectroscopy A. Richter & C. Mertens, Measurement Techniques summer 2014

Prelimiary Time Schedule: Practicals A. Richter & C. Mertens, Measurement Techniques summer 2014 Experiment / GroupABCDEFGHIJ Satellite Image Analysis Passive DOAS Radioactivity Acoustical flow Measurements (Oceanography) FTS Cavity Ring Down Spectroscopy (CRDS) Ozone Absorption Spectroscopy

Reporting on the experiments for each experiment, you will have to submit a report students within one group submit joint reports after the experiment, you have 2 weeks for writing the report and submitting it to the tutor the tutor will read the report and usually ask for some revisions / corrections / additions / changes you then have another week to submit a corrected report if necessary, you will have to submit a second revision should the supervisor still not accept your report, this will be discussed with the lecturers (A. Richter and C. Mertens). If all else fails, you will have to take another (additional) experiment Only with 4 of your reports having been accepted and with a successful exam you will get the credit points for this course A. Richter & C. Mertens, Measurement Techniques summer 2014

Contents of the Report ideally, your report should enable another scientist to set-up a similar experiment, to repeat the measurements and to compare his results with yours it should also give the motivation why things have been done the way they were done for the purpose of the practical, it should show that you have understood the experiment questions to answer in the report: 1.What have you done? 2.Why have you done it? 3.How have you done it? 4.What are the results? 5.What are the associated errors? 6.What are the conclusions? A. Richter & C. Mertens, Measurement Techniques summer 2014

Structure of Report 1.Title of the experiment; group and name of the students; date 2.Introduction: Short description of the experiment and its objectives 3.Theoretical background: Scientific background on which the experiment is based 4.Experimental set up: Description of the set up used; components and their principle of operation 5.Experimental procedure: Description of each step followed during the experiment, indicating the time and relevant details 6.Data analysis: Description of the data obtained, analysis and conversion procedures applied to obtain the results for interpretation 7.Results and error analysis: Final numerical and graphical results with the corresponding associated error. A detailed description of the error analysis should also be included 8.Discussion of results: Interpretation of the final results in relation to the objectives of the experiment. You can use the questions given in the instructions for the experiment as a guideline 9.Appendix: Raw data in a table, in graphs or in digital form A. Richter & C. Mertens, Measurement Techniques summer 2014

Use of external sources of information in addition to the explanations provided in the experiment description and lecture, you are expected to use other sources of information (papers, books, web pages, discussion with your colleagues) any information source used must be acknowledged in the text through appropriate citations quoting another text verbatim (“cut and paste”) is usually not acceptable, and has always to be indicated by using quotation marks if you can’t say it in your own words, you have probably not understood it quotes from the experiment description are not acceptable using data or text from the reports of other groups, or using un-referenced cut-and-paste text from some internet source, is considered to be fraud A. Richter & C. Mertens, Measurement Techniques summer 2014

Use of graphical data representations Graphical representation of data and results is highly recommended “Ein Bild sagt mehr als 100 Worte” All figures must have  clear axis labels indicating the quantity plotted and the units used  figure captions explaining the contents of the figure  figure numbers for reference  proper reference and explanation in the text figures must be large enough to see all the necessary details line thickness and symbol sizes must be adequate, colours often help the ranges used for x and y axis must be appropriate for the range of values shown individual measurement points should be shown by symbols connecting lines should usually be linear, not spline or polynomials where possible, add error bars A. Richter & C. Mertens, Measurement Techniques summer 2014

Example for graphical representations useless Fig 1: Variation of tropospheric NO 2 -column with latitude. Data from GEOSCHEM model for July 1997 [Martin et al., 2001]. useful A. Richter & C. Mertens, Measurement Techniques summer 2014

Numerical results often, a numerical result is expected from your experiment all numerical results have to be given with units checking units often helps to find errors all results must be accompanied by error estimates the number of digits given must make sense with the errors:  E = W m -2 => E = W m -2  E = 3E W m -2 => E = W m -2 all results should be put into context e.g.  is of expected order of magnitude  lies within 5% of the predicted value  is twice as large as expected for clean situations A. Richter & C. Mertens, Measurement Techniques summer 2014

Overall form form matters! use section numbering use clear section headers use numbering for equations, figures and tables don’t forget page numbers before submitting, check your report for  logic  completeness  grammar and spelling submit your report in a binder and not as a staple of sheets clearly indicate your names, date of the experiment, date of submission of report on the cover sheet reports are prepared with a word processor (word, latex, …) The length of the report is typically 6 – 8 pages A. Richter & C. Mertens, Measurement Techniques summer 2014

Final Exam Type of exam:Oral exam (45 minutes) Successful completion of all 4 labs Content:15 minutes presentation on one experiment Questions related to the lectures Questions to the 4 labs Date:On August , 2014 exact times TBD Contact: Andreas RichterChristian Mertens Room: U-2090Room: M-3140 Phone: Phone: A. Richter & C. Mertens, Measurement Techniques summer 2014