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AAnalyst 600 ES Hwang Inorganic Product Specialist PerkinElmer Korea.

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Presentation on theme: "AAnalyst 600 ES Hwang Inorganic Product Specialist PerkinElmer Korea."— Presentation transcript:

1 AAnalyst 600 ES Hwang Inorganic Product Specialist PerkinElmer Korea

2 AAnalyst 600… Features Features Dedicated THGA furnace Dedicated THGA furnace High sensitivity segmented solid-state photodiode detector High sensitivity segmented solid-state photodiode detector Simultaneous measurement of sample and reference beams Simultaneous measurement of sample and reference beams Transversely heated graphite furnaceTransversely heated graphite furnace Longitudinal Zeeman effect background correctionLongitudinal Zeeman effect background correction Benefits THGA furnace reduces interferences in difficult matrices Exceptional analytical performance and detection limits Highest Long-term Stability Minimized interferences and memory effects Shorter analysis time (fast furnace programs) Best possible background correction with no light loss … the best dedicated THGA furnace system

3 AAnalyst 600 AA Spectrometers

4 AAnalyst 600 Revolutionary Optical System

5 AAnalyst 600 Unique Features First AA spectrometer First AA spectrometer Integrated furnace Integrated furnace Zeeman-THGA graphite furnace Zeeman-THGA graphite furnace

6 AAnalyst 600 Unique Features First AA spectrometer First AA spectrometer 8-lamp holder 8-lamp holder Automatic lamp selection and adjustment Automatic lamp selection and adjustment Built-in power supplies Built-in power supplies Hollow cathode lamps Hollow cathode lamps Electrodeless discharge lamps Electrodeless discharge lamps

7 AAnalyst 600 Highly Versatile Furnace Autosampler User Benefits: User Benefits: Automatic generation of reference solutions Automatic generation of reference solutions Automatic multiple injections Automatic multiple injections Automatic dilution Automatic dilution Automatic injection into a preheated tube Automatic injection into a preheated tube Variable pipetting speed Variable pipetting speed Ease-of-operation Ease-of-operation

8 AAnalyst 600 Revolutionary Optical System Real time double beam system Real time double beam system High sensitivity segmented solid-state photodiode detector High sensitivity segmented solid-state photodiode detector User Benefits: User Benefits: Exceptional analytical performance Exceptional analytical performance Highest Long-term Stability Highest Long-term Stability

9 AAnalyst 600 Customized Solid-State Detector l Highest quantum efficiency l Integrated low noise CMOS charge amplifier array l Exceptional signal-to-noise ratio

10 AAnalyst 600 Quantum Efficiency of Detectors photomultiplier solid state detector

11 AAnalyst 600 Furnace (THGA) Instrument Detection Limits THGA Instrument detection limits (IDL) / pg Element PMTPhotodiode As 9 6 As 9 6 Cr Cr Cu 5 4 Cu 5 4 Mn Mn Pb 3 3 Pb 3 3 Tl Tl 7.5 7

12 AAnalyst 600 Automatic Lamp Selector l 8-Lamp holder l Built-in power supplies for hollow cathode and electrodeless discharge lamps l Automatic alignment, element, wavelength and slit selection

13 AAnalyst 600 Unique Overall Conception Total system control via AA WinLab32 software for highest versatility and simplest operating convenience Total system control via AA WinLab32 software for highest versatility and simplest operating convenience Atomizer control Atomizer control Lamp and lamp current control Lamp and lamp current control THGA control THGA control Accessory control Accessory control

14 AAnalyst 600 Unique Software Conception Automatic system setup from stored users methods Automatic system setup from stored users methods Direct from Workspace Direct from Workspace Method Method Sample information Sample information Individual screen design, window selection etc. Individual screen design, window selection etc. User Benefits: User Benefits: Analytical reliability Analytical reliability Ease-of-operation Ease-of-operation Time-saving Time-saving

15 Bringing a new level of productivity to high-performance AA WinLab32 for AA

16 AA WinLab32 - Features and Benefits Improve productivity Improve productivity Data Reprocessing *Data Reprocessing * WinLab32 Offline *WinLab32 Offline * Priority samples *Priority samples * Append to Analysis List *Append to Analysis List * Edit CalibrationEdit Calibration Recall CalibrationRecall Calibration Furnace Method Development wizard *Furnace Method Development wizard * Improve ease of use and reduce training Improve ease of use and reduce training Tool tips (available in 6 languages) *Tool tips (available in 6 languages) * Wizards *Wizards * Analysis List *Analysis List * AS-93 parameters integrated *AS-93 parameters integrated * * New features not present in 16-bit AA WinLab

17 AA WinLab32 - Features and Benefits Reduce training and support Reduce training and support Common look and feel with WinLab32 for ICP-OESCommon look and feel with WinLab32 for ICP-OES CD Document PackCD Document Pack Improve stability and data accessibility Improve stability and data accessibility Access database *Access database * Method and data security Method and data security Password protection *Password protection * Multiple user levels *Multiple user levels * Data check sums to detect changes *Data check sums to detect changes * 21 CFR Part 11 Compliant21 CFR Part 11 Compliant * New features not present in 16-bit AA WinLab

18 WinLab32 for AA Workspace Toolbar Automated Analysis Results Status Monitor Common look and feel with WinLab32 for ICP for easy cross platform training Calibration

19 Data Reprocessing Recalculation of analytical data Recalculation of analytical data Correct SIF errorsCorrect SIF errors Change calibration functionChange calibration function Delete replicate(s)Delete replicate(s) Performed using the raw data Performed using the raw data Samples can be reprocessed in any sequence Samples can be reprocessed in any sequence Original data are preserved Original data are preserved Analytical log can be printed Analytical log can be printed Reprocessed data are identified Reprocessed data are identified

20 Data Reprocessing Select samples in the order you want them reprocessed. Status display Change sample information in these columns

21 Furnace Method Development Wizard Define Furnace Steps to cycle Temperatures Define Solutions To Analyze Analyze Solutions and Display Results

22 Align Autosampler Tip Wizard

23 Auto dilution by system

24 Priority Sample Samples can be added without interrupting current analyses

25 Exporting Data to LABWORKS Export data to LABWORKS

26 WinLab32 Enhanced Security Option Enhancement to WinLab32 for AA (and ICP) Enhancement to WinLab32 for AA (and ICP) Significant set of new features Significant set of new features Audit trailsAudit trails File versioningFile versioning Enable compliance with new regulations Enable compliance with new regulations 21 CFR Part 11 - Pharmaceutical21 CFR Part 11 - Pharmaceutical 40 CFR Part 3 - Environmental (proposed)40 CFR Part 3 - Environmental (proposed) OthersOthers Primarily for highly regulated laboratories Primarily for highly regulated laboratories Users actions are restrictedUsers actions are restricted Increased storage space requirementsIncreased storage space requirements Additional information entry requirementsAdditional information entry requirements Requires more system housekeepingRequires more system housekeeping

27 AAnalyst 600 Total Range Graphite Furnace AA THGA-type furnace with Zeeman-effect background correction THGA-type furnace with Zeeman-effect background correction User Benefits: User Benefits: Selection of the best system for individual requirements and budgets Selection of the best system for individual requirements and budgets High performance, near interference-free trace analysis with STPF concept High performance, near interference-free trace analysis with STPF concept

28 AAnalyst 600 Integrated THGA Furnace System

29 AAnalyst 600 Zeeman THGA Furnace Transversely heated graphite furnace Transversely heated graphite furnace Longitudinal Zeeman effect background correction Longitudinal Zeeman effect background correction User Benefits: Exceptional detection limits Exceptional detection limits Minimized interferences and memory effects Minimized interferences and memory effects Best possible background correction Best possible background correction Mimimum sample preparation time Mimimum sample preparation time Shorter analysis time (fast furnace programs) Shorter analysis time (fast furnace programs)

30 AAnalyst 600 Integrated THGA System THGA Concept: more than 2500 systems in use THGA Concept: more than 2500 systems in use Longitudinal Zeeman- Effect: highly resolved background compensation without light loss Longitudinal Zeeman- Effect: highly resolved background compensation without light loss DC furnace power supply DC furnace power supply Closest approach to the "ideal system" Closest approach to the "ideal system"

31 AAnalyst 600 Integrated THGA System Atomic and background signals for Ba, 20uL, 25 ug/L

32 AAnalyst 600 Zeeman versus D 2 Background Correction Background correction independent of wavelength Background correction independent of wavelength True double-beam with only one optical path True double-beam with only one optical path Baseline noise at least 2x lower Baseline noise at least 2x lower Optical resolution is 100x better Optical resolution is 100x better Char. mass typically 10 and 20 % poorer than with D 2 (the m 0 for the worst case, Cu, is 50% poorer) Char. mass typically 10 and 20 % poorer than with D 2 (the m 0 for the worst case, Cu, is 50% poorer) Zeeman-effect background correction gives superior detection limits in real samples Zeeman-effect background correction gives superior detection limits in real samples

33 AAnalyst 600 Highly Versatile Furnace Autosampler High-capacity, interchangeable sample trays High-capacity, interchangeable sample trays 88 or 146 sample positions 88 or 146 sample positions Full AA WinLab32 control including multi-tasking Full AA WinLab32 control including multi-tasking User Benefits: User Benefits: Automatic generation of reference solutions Automatic generation of reference solutions Automatic multiple injections Automatic multiple injections Automatic dilution Automatic dilution Automatic injection into a preheated tube Automatic injection into a preheated tube Variable pipetting speed Variable pipetting speed Ease-of-operation Ease-of-operation

34 AAnalyst 600 Flow Injection - Furnace Coupling Optional accessory for coupling FI-MHS with furnace AA Optional accessory for coupling FI-MHS with furnace AA Software controlled automatic operation Software controlled automatic operation User Benefits: Detection limits in range of ng/L Detection limits in range of ng/L Time-savings by automatic on-line operation Time-savings by automatic on-line operation Less interferences since matrix components are removed in the FI system Less interferences since matrix components are removed in the FI system

35 AAnalyst 600 Automatic Slurry Sampling Optional ultrasonic probe integrated in the autosampler Optional ultrasonic probe integrated in the autosampler Automatic introduction of solid samples as slurries Automatic introduction of solid samples as slurries Full software control Full software control User Benefits: Reduced sample preparation and analysis time Reduced sample preparation and analysis time Reduced potential for contamination Reduced potential for contamination Easy operation Easy operation

36 What else can PerkinElmer offer? Sample Preparation Solutions Sample Preparation Solutions Multiwave 3000Multiwave 3000 High Pressure Asher (HPA)High Pressure Asher (HPA) Flow Injection Technology (FIAS) Flow Injection Technology (FIAS) For sample pre-treatmentFor sample pre-treatment Hydride generationHydride generation Stand-alone Mercury systems (FIMS) Stand-alone Mercury systems (FIMS) Sample Introduction Systems Sample Introduction Systems AutodilutorsAutodilutors Laser Ablation systemsLaser Ablation systems World class service and support World class service and support

37 Inorganic sample preparation…. Multiwave 3000 Multiwave 3000 Reduced digestion timesReduced digestion times Superior digestion qualitySuperior digestion quality Time-savingTime-saving Easy operationEasy operation Maximum safetyMaximum safety High Pressure Asher High Pressure Asher Complete sample mineralizationComplete sample mineralization Minimum organic residueMinimum organic residue No elemental lossesNo elemental losses No contaminationNo contamination …a clear solution for sample preparation ! Multiwave 3000 HPA system

38 FIAS – Flow Injection Systems 2 Models FIAS 100 (1 valve, 1 pump) FIAS 400 (1 valve, 2 pumps) Automated sampling for Flame AA Dilution Add reagents or modifiers Matrix removal Preconcentration Improved sample handling Small sample volumes High solids samples Hydride generation Determination of As, Se, Te, Be, Sb, Sn FIAS 100 system FIAS 400 system

39 Flow Injection Mercury Systems FIMS 400 FIMS 400 Determines Mercury via Cold Vapor AA (CVAA)Determines Mercury via Cold Vapor AA (CVAA) Small footprintSmall footprint Fully automatedFully automated Easy to operateEasy to operate Stand alone systemStand alone system Cost effectiveCost effective Now with WinLab32 for AA softwareNow with WinLab32 for AA software

40 AAnalyst 600 Conclusions Not just another AA! Not just another AA! No compromises! No compromises! Easiest, simplest AA furnace Easiest, simplest AA furnace Full automation Full automation Full range of accessories Full range of accessories Power of AA WinLab32 software Power of AA WinLab32 software Ultimate in performance Ultimate in performance The AA instrument to take you beyond The AA instrument to take you beyond


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