Field Assisted Sintering of Advanced Ceramic Materials

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Presentation transcript:

Field Assisted Sintering of Advanced Ceramic Materials Nikhil Mohip Seth Mongbeh Alejandro Vera   Advisor: Professor Zhe Cheng

Presentation Outline Problem Statement Literature Survey Project Description Motivation and Goals Literature Survey Sintering Sintering Driving Force Sintering Types Field Assisted Sintering

Presentation Outline Flash Sintering Mechanism Related Standards Joule Heating Related Standards International Organization of Standardization Challenges Global Design Components Initial Die Design Die Design Alternatives

Presentation Outline Proposed System Design 2015 Time Line Poster Board

Problem Statement Project Description: Design and build a Flash sintering machine. Successfully Flash sinter a sample or samples of ceramic material. Record sample’s temperature in real time. Test the sample’s mechanical properties.

Problem Statement Motivation and Goals: Control or eliminate undesirable reactions to high temperatures. Reduce harmful and unwanted waste. Investigate the Flash sintering mechanism.

Literature Survey Sintering: Inter - particle pores in a granular material are eliminated by atomic diffusion. Sintering Driving Force: The curvature of the particle surface An externally applied pressure Chemical reaction

Literature Survey Sintering Types: Pressure Assisted Sintering. Hot Pressing. Microwave Sintering. Field Assisted Sintering

Literature Survey Field Assisted Sintering: Use of a DC electric current in the sintering process cause retardation in growth grain. Ceramics could be sintered in less than 5 seconds . Relating common used materials are: Mg-O Alumina, SiC, and ZrB2.

Literature Survey Joule Heating: Increment in the sample temperature from the scattering of electrical energy. Assumes the sample transmits radiation like a dark body.

Flash Sintering Mechanism Joule Heating: Volumetric thermal expansion caused by increase in temperature.

Related Standards International Organization for Standardization: ISO has published more than 19500 International Standards covering almost every industry.

Related Standards

Challenges Assemble a Field Assisted Sintering apparatus centered around the FIU Nano – Fabrication Lab furnaces. Densify material up to 90% then aim to increase densification. Record temperature increase in real time.

Global Design Components Conversion of currency Translation of the experimental design procedures Contacting of individuals who have performed flash sintering experiments

Initial Die Design Conventional die used to press ceramic powder On the outsides is the die assembly In the middle is the press used to apply pressure

Die Design Alternatives Dog-bone shaped sample found to have even current distribution Rectangular die less complex to manufacture

Proposed System Design On far left – top view of flash sintering system Middle – front view of die and sample being pressed On right – close-up of sample while in furnace

2015 Time Line

FIELD-ASSISTED SINTERING OF ADVANCED CERAMIC MATERIALS Challenges Global Learning Converting currencies . Translate the experimental design. Warning labels in different languages. Contacting previous flash sintering designers from other countries. Problem Statement An economical and efficient way to investigate the flash sintered material’s mechanical properties, and to compare these properties to those of conventional sintering processes. Assemble a flash sintering machine centered around the FIU Nano – Fabrication Lab furnaces. Densify material up to 90% then aim to increase densification. Proposed Design Motivation Study the mechanism of flash sintering. Understand how flash sintering influences the ceramic material and its properties. Further material research conducted by the Florida International University’s Mechanical and Materials Engineering Department. Objectives Become pioneers in the subject of flash sintering for the Florida International University’s Department of Mechanical & Materials Engineering. Successfully flash-sinter a sample or samples of ceramic material. Propose optimization of this process as part of the manufacturing of ceramic objects. Time Line Nikhil Mohip Seth Mongbeh Alejandro Vera   Advisor: Professor Zhe Cheng