New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 NeSSI (New Sampling/Sensor Initiative) 2001 Spring Sponsor Meeting Center for Process Analytical Chemistry

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Agenda Status and Update- PV2 Introduction (Why CPAC) What is NeSSI What has happened/is happening Status and Update- PV2 Introduction (Why CPAC) What is NeSSI What has happened/is happening NeSSI Team Goals- Rdubois NeSSI Team Goals- Rdubois Bluetooth- Mike Horton (Crossbow) Bluetooth- Mike Horton (Crossbow) Connectivity- PV2 Connectivity- PV2

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 CPAC as a Multi-Purpose PA Forum Legal Umbrella for Sponsors to Meet Legal Umbrella for Sponsors to Meet R&D: Long Range / Short Range Information Clearing House Enabling Mechanism to Address Other Common Needs Focus Groups: Forum to Focus Groups: Forum to Review R&D Programs Present Industry Common Needs - RFP Address Other Industry Common Needs Fieldbus Datalink Specification - Done NeSSI /Micro-Reactor Analytics - In progress Chemometrics On-line/Connectivity - Future?

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 What is NeSSI? Adapt Modular Surface Mount Technology from the SEMI Industry to Sampling System Design in the Chemical IndustryAdapt Modular Surface Mount Technology from the SEMI Industry to Sampling System Design in the Chemical Industry Driving Forces for ChangeDriving Forces for Change Cost to Build/ Cost of Ownership Traditional Sampling System Designs Same for Last 20+ Years Weak Link in Overall Analyzer Reliability Integrate Other Sensors (Smart Sampling System) Sample Validation

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 What is NeSSI? Picture courtesy Swagelok ®

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 What is NeSSI? New 5 Channel Design by Parker Picture courtesy Parker

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 What is NeSSI? - It is SMART P Legend: Pressure Sensor Temp Sensor Valve Analytical Sensor V A T

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 NeSSI Vision (Now)

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 NeSSI Vision (Next Step) V T P A Signal to ACSensor Analytical Manager (SAM) Signal Wires Only Shared Power Bus

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Background and Chronology of NeSSI Activities Oil&Petrochemical (O&P) Focus Group May 1999 Oil&Petrochemical (O&P) Focus Group May 1999 Identified Sampling Systems as Common Area Of Interest Sponsored Tutorial for Nov99 Sponsor Meeting Tutorial Nov99 CPAC Meeting Tutorial Nov99 CPAC Meeting Background/Reasons for Interest Presentations by Suppliers/ End Users Participation in IFPAC2000 MeetingParticipation in IFPAC2000 Meeting Plenary/General Papers (SS Enjoyed High Profile) Workshop

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Background and Chronology of NeSSI Activities (cnt’d) Ad-hoc O&P Pittcon2000 Ad-hoc O&P Pittcon2000 End-users Discuss Initial Target Designs CPAC2000 Spring Meeting CPAC2000 Spring Meeting Formed SS Focus Group Defined Information Package (basis of RFP) Distributed Request for Proposal (RFP) (July 2000)Distributed Request for Proposal (RFP) (July 2000) Clarification Meeting at ISAEXPO2000 (40 attendees) Received Proposals/Feedback from Swagelok, Parker, Autoflow,ABB Analytical, SAAI, Rosemount Analytical

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Background and Chronology of NeSSI Activities (cnt’d) CPAC2000 Fall Meeting CPAC2000 Fall Meeting Previewed Swagelok/Parker Proposals Micro-Reactor Proposal (Micro-Analytics) Planning (CD Deliverable, IFPAC2001, Pittcon etc.) IFPAC2001 IFPAC2001 Sampling System Session at IFPAC2001 Review and Summary of NeSSI Effort (RD/PV2) Papers by Swagelok, Parker, Autoflow, ABB, Rosemount Ad-hoc Meeting (Standing Room only Interest)

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Background and Chronology of NeSSI Activities (cnt’d) Pittcon2000 Meeting Pittcon2000 Meeting NeSSI Ad-hoc Forum Meeting Confirmed viability of NeSSI designs Introduced the Role of Wireless (Bluetooth) Focus on Special Issues/Problems Swagelok, Parker, ABB Highlighted Special Problems 4 Subteams (Intrinsic Safety, Component availability etc.) Miscellaneous/In the PipelineMiscellaneous/In the Pipeline Proposal for Additional Resource Jim Tatera (retiree from Dow Corning) Part-time to lead key sub-team activities Deliverables/schedule defined Report at next CPAC Meeting (Nov) More details of proposal etc. at SSFG (Wednesday)

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Background and Chronology of NeSSI Activities (cnt’d) Miscellaneous/In the Pipeline (cnt’d)Miscellaneous/In the Pipeline (cnt’d) Testing/Evaluation Two Systems in Design Phase (EMCC) Rosemount Laboratory Tests Completed (see SSFG) Test System Available More Participation by End-users needed NeSSI Deliverable Completed CD Issued NeSSI Website Up-to-date NeSSI Promotional efforts Distribution List > 150 names Present Hour Tutorial at ISA2001 Meeting (Sept01) Globalization efforts CPACT Presentation Apr01 (high interest, additional names) Paper tentatively accepted for INTERMAC Meeting (Nov01) Extending SP76 to IEC standard

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001Acknowledgements DowRon O’Reily/Brian Worthington/Walter Henslee Dow CorningJim Tatera /Gary Bokerman DuPont Joe Adrisani, Chuck Miller, Bob Bucher, Bruce Johnson Rohm&HaasJoe Sung Honeywell Ken Creasy, Ullrich Bonne, Troy Francisco ExxonMobil Dan Podkulski/Rajko Puzic/Paul Hromadka/John Cumbus/Jeff Gunnell SwagelokDave Simko/Rick Ales & Colleagues ParkerSteve Doe, Frank Ruiz & Colleagues RosemountJohn Gajewski & Colleagues ThermoOnixJerry Evans CPACLloyd Burgess/Larry Ricker OthersABB, Panametrics, AAI, Sterling Chemicals

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 …. and they lived happily ever after FINI

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 O&P Focus Group Meeting May 99 Recognized Modular Sampling System Efforts in Semi Conductor Industry (Standard) Vendors like Autoflow, A+, Swagelok etc. promoted modular designs Recognized that current implementations of sample systems designs have not changed for many years CPAC has promoted Versatile Micro Analytical Systems (VMAS) as a basis for future micro-analytical techniques O&P decided to sponsor a SSISSS (Small Smart Integrated Sensor and Sampling System) Tutorial at CPAC Nov Meeting

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Driving Forces for Change Reduce Cost of Ownership Non Recurring Costs = Cost to Build Operating Cost Data Validation (Fit for Use)

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 A F T P AnalyzerController Field LAN Integration of Sample System and Sensors Sample Conditioning System Level 0 Level 1 Process Stream All System Components in Contact with Sample including the Sensors All Additional Electronic and Computing Components Required to Generate Analytical Result Mainly a Trust Configuration Now a Trust & Verify Configuration

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Integrated Sampling/Sensor System A F T P Level 0 Subsystem Integration Sample Conditioning System Level 0 Process Stream Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) Opportunity: Packaging as an Integrated Sensor and Sampling System Size Cost Issues: Size Standardization VMAS

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 A F T P AnalyzerController Field LAN Separation or Integration of Level 0/1 Subsystems Level 0 Level 1 Process Stream Integrated Sampling/Sensor System Objective: Close to Sample Tap Options: RemoteRemote Separate but CloseSeparate but Close IntegratedIntegrated

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Integrated Sampling/Sensor/Controller System A F T P AnalyzerController Field LAN Integration of Level 0/1 Subsystems Level 0 Level 1 Process Stream $$

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Nov99 CPAC SSISSS Tutorial (Vendor Presentations) Autoflow RosemountA+ Swagelok

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) and Micro Fluidics Sensors/Analyzers

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design for SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 TODAY’S COST OF BUILD For a major greenfield project

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 TODAY’S COST OF OWNERSHIP

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IMAGINE THE FUTURE A T P AnalyzerController Field LAN Level 0 Level 1 Process Stream F

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IMAGINE THE FUTURE FLAN (Optical Fiber) Sensor/Signal Bus IA Controller (ASIC) & Interface Module Original Picture of Gas Delivery System courtesy Valin Corporation; A T P F Sensor = Moisture Probe

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IMAGINE THE FUTURE A T P F Sensor = RAMAN Probe Interface Module

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 Pittcon2000 (New Orleans) O&P Ad-Hoc Meeting of Sponsor End-users DuPont, Dow, Dow-Corning, CPAC, Rohm&Haas, ExxonMobil Main Goal: Identify Typical Sample System Designs as Candidates for Modular Design Reviewed some typical gas/liquid sample System Designs Rob DuBois Presented a Modular Component/Service Matrix Discussed next steps Present Sample System Data at May CPAC Meeting Next Step is to Open Up Discussion (3 rd parties) Leverage ISA Meeting in New Orleans (Aug00) Role of CPAC in Facilitating Development/Testing of a Prototype System Larry Ricker/Lloyd Burgess to Present Proposal

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001Status CPAC Meeting May 1999Done O&P Identified Modular Sampling Systems CPAC Meeting Nov 1999Done O&P Sponsored Tutorial IFPAC2000 MeetingDone Plenary Presentation Promoted SSISS Session on Modular Sampling Systems CPAC Sponsored Workshop Pittcon2000Done Ad-hoc O&P Meeting Propose Candidate Sampling System Descriptions CPAC Meeting May 2000TBD

New Sampling/Sensor Initiative (NeSSI) CPAC: May 7, 2001 What is Next? CPAC Meeting May 2000 (Sampling Focus Group – Wednesday) Review and Agree on Sample System Information Package Involvement of 3 rd parties How do we distribute package (Distribution List, Meeting?) Expectations for proposals from Suppliers (Paper designs?) Joint Effort with ISA (Meeting in Aug, New Orleans) Evaluation of Designs - Recommendation Prototype design/manufacturing/testing at CPAC Larry Ricker/Lloyd Burgess proposal Program to Evaluate Test Platforms fro Micro Analytical Devices CPAC Proposal – Lloyd Burgess