1. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Small Smart Integrated Sensor & Sampling Systems Tutorial Session Sponsored by the Oil & Petrochemical Focus Group 1999 Fall Sponsor Meeting Center for Process Analytical Chemistry

2. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Session Agenda 8:30 Welcome and Introduction Mel Koch- CPAC Peter van Vuuren - Exxon 8:45 Smart Sensors Bill Dodge - DuPont 9:10 Sampling System Components Kevin Mracek - Swagelok 9:35 Modular Sampling Systems Don Mayeaux- A+ 10:00 Break 10:20 Advanced Modular Sample System Richard Hughes- Autoflow 10:45 Smart/Modular SHS and Field John Gajewski- Rosemount Mounted Analyzers 11:10 Break Out Session All 12:00 Adjourn

3. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Introduction and Background Peter van Vuuren Exxon Chemical

4. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Driving Forces for Change Reduce Cost of Ownership Non Recurring Costs Operating Cost Data Validation (Fit for Use)

5. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Process Control System Perspective System within a System

6. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Analyzer Computing System Hierarchy

7. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Validation=Verify Validation = Trust but Verify Reliability vs Credibility Measurement Reliability Credibility Time Costly Event (M$)

8. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Moral of the Validation Story Unless the Analyzer can Validate the Analytical Measurement Validate the Analytical Measurement it has Little or No Value in a Process Control Environment

9. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Validation Data Domains/Hierarchy

10. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 A F T P AnalyzerController Field LAN Integration of Sample System and Sensors Sample Conditioning System Level 0 Level 1 Process Stream All System Components in Contact with Sample including the Sensors All Additional Electronic and Computing Components Required to Generate Analytical Result Mainly a Trust Configuration Now a Trust & Verify Configuration

11. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Integrated Sampling/Sensor System A F T P Level 0 Subsystem Integration Sample Conditioning System Level 0 Process Stream Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) Opportunity: Packaging as an Integrated Sensor and Sampling System Size Cost Issues: Size Standardization VMAS

12. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Separation or Integration of Level 0/1 Subsystems A F T P AnalyzerController Field LAN Level 0 Level 1 Process Stream Integrated Sampling/Sensor System Objective: Close to Sample Tap Options: RemoteRemote Separate but CloseSeparate but Close IntegratedIntegrated

13. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Integrated Sampling/Sensor/Controller System A F T P AnalyzerController Field LAN Integration of Level 0/1 Subsystems Level 0 Level 1 Process Stream $$

14. Small Smart Integrated Sensor & Sampling Systems CPAC: Nov 1, 1999 Objectives for Tutorial Understand: State-of-the Art Sample System Components and DesignsState-of-the Art Sample System Components and Designs Opportunities/Benefits of Sensor Integration and MiniaturizationOpportunities/Benefits of Sensor Integration and Miniaturization LimitationsLimitations Preview: New DevelopmentsNew DevelopmentsFollow-up?