1. PPE Use Standard (SSP-0011) Y Full Face Shield / Goggles Hood Clothing—Chemical Protection Gloves—Chemical Personal Fall Protection Respirator / Filter Mask Supplied Air Job Hazards Y es Job Hazards Y es Access and EgressMoving Parts Activities of OthersNoise Adverse WeatherRail Movement Chemical ExposureSharp Edges ElectricitySlips, Trips, and Falls FatigueStatic Electricity Fire and ExplosionTrip Injuries Ground ContaminationTrapped Pressure Manual HandlingWorking at Height Other: References / Documents  ASTM D130 3 AreaUnitOperating Procedure #Certified byRevision #DatePage 3LabOPS-LB-PT-00810.11.20111 of 2 Copper Strip Corrosion of Diesel, Gasoline EnvironmentalSpecial Instructions Copper Strip Corrosion of Diesel, Gasoline 1 Observe sample – if suspended water is evident, dry sample by filtering through P8 qualitative paper directly into test tube for a final volume of 30 ml, then stopper with vented cork or rubber stopper. 2Place a sheet of silicon carbide paper on a flat surface and moisten with isooctane. 3Using steel wool or 220 grit silicon carbide paper, remove all surface blemishes from all 6 sides of copper test coupon. 4Finish with 220 grit paper ensuring all marks are removed so that end result is a smooth, lustrous finish. 5Store strip in isooctane until final polishing. 6Pour 30-ml sample into clean, dry test tube and stopper with vented cork or rubber stopper. 7Remove test coupon from isooctane and place on silicon carbide paper. NOTE: To prevent contamination during final polishing, never allow test coupon to come into contact with bare fingers or water. 8 Polish first the ends and then the sides with 150-mesh silicon carbide grains picked up with a pad of absorbent cotton moistened with isooctane. 9Polish strip uniformly using long strokes that carry beyond the end of the copper strip. 10Remove any metal dust with clean cotton pads moistened with isooctane. 11When strip is clean, with minimal delay, slide copper strip into sample tube and re-stopper. EquipmentMaterials and Reagents  Water bath or solid block bath, accuracy 122±2°F.  Test Tubes, Borosilicate Glass, 25 X 150 mm  ASTM Copper Strip Corrosion Standard Plaque  Silicon Carbide Grit Paper, 220 grit  150-grit Silicon Carbide Grains  Forceps  Temperature Sensing Device (TSD), accuracy ± 1°C (2°F)  Copper Test Strips (see specifications ASTM D130)  Steel wool; OU grade or finer  Isooctane  P8 Qualitative Filter Paper Scope / Objective This procedure covers the determination of the corrosiveness to copper of hydrocarbon samples having a vapor pressure no greater than 18 psi @ 100°F. Note: This procedure is only valid at the time of printing. The control version can be found on the Meraux Refinery intranet. Completed Date:Prepared By:Approved By:

2. 3 AreaUnitOperating Procedure #Certified byRevision #DatePage 3LabOPS-LB-PT-00810.11.20112 of 2 Copper Strip Corrosion of Diesel, Gasoline Continued 12Place sample tube in bath equipped with vertical supports such that sample tube is held in upright position. 13After 3h ±5 min., remove sample tube from bath using forceps. 14Empty contents of tube into beaker and withdraw strip with forceps. 15Immerse strip in isooctane and withdraw immediately. 16Blot strip dry (do not rub) with filter paper. 17Compare test strip with copper strip corrosion standard holding both at approximately 45° angle from the light source. 18 Interpret results as follows: a.Select the color standard that most closely matches the test strip and rate the sample accordingly. b.If strip is in transition state between 2 standards, rate the sample as the more tarnished classification. c.Refer to Table 1 of ASTM D130 for a written description of each sample classification if needed. Note: This procedure is only valid at the time of printing. The control version can be found on the Meraux Refinery intranet. Completed Date:Prepared By:Approved By: