T<1700 o C He atmosphere Graphite heater Kapton film protection FixDif: unique instrument for high- temperature XRD studies (small sample size) HT X-ray.

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Presentation transcript:

T<1700 o C He atmosphere Graphite heater Kapton film protection FixDif: unique instrument for high- temperature XRD studies (small sample size) HT X-ray studies

In situ HT X-ray studies PanAnalytical X-Pert Pro + HTK Study of phase changes, stress, oxidation kinetics until 1200 o C - Quantitative phase content estimation using Rietveld refinement

ESEM (environmental SEM) FEG XL30, equipped with EDX (Empa) (T< 1500 o C at low-vacuum) Water cooling Heater Crucible (Ø < 4.5 mm, thickness < 1 mm) Thermal shield Connector to gaseous secondary electron detector In situ HT SEM studies

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