1. CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

2. CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis Course Information Sheet Lecture 10:00 – 10:50 am MWF Room: CCIS L1-140 Dr. James Harynuk Chem W4-25A 492-8303 james.harynuk@ualberta.ca Office Hours: Monday 1:00-2:30 Wednesday 1:00-2:30 or by appointment Webpage: www.ualberta.ca/elearning

3. Labs Dr. Greg KiemaChem W2–03A gregory.kiema@ualberta.ca Webpage: http://www.chem.ualberta.ca/undergrad.html then “Courses” then “Chem 213” Much of this info is/will be duplicated on the eClass site CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis Course Information Sheet

4. Grading Mid-term (in class Wed, Feb 29)25% Final (Monday, April 23 9:00 AM)37% location TBD Laboratory35% Class/Laboratory Participation3% CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis Course Information Sheet

5. For some Participation points Help Dr. Harynuk and the TAs get to know you Attach a photo of yourself to your Moodle profile so that we can see who you are when answering your questions Please do this by January 20 th

6. Analytical Chemistry seeks ever improved means of measuring the chemical composition of natural and artificial materials. ACS.

7. Instrumental Analysis UV spectroscopy Ion trap MS IR spectroscopy Time of flight MS Raman spectroscopy Electrospray MS Flame atomic absorbance MALDI-TOFMS Electrothermal AAS Potentiometry Flame atomic emission Coulometry ICP-optical emission Voltammetry ICP-Mass Spec Amperometry X-ray fluorescence Surface probe microscopy Fluorescence spectroscopy Gas chromatography Magnetic sector MS HPLC Double focusing MS Ion chromatography Quadrupole MS Capillary Electrophoresis

8. If you happened to have already taken 313… Why are you here??? You MAY NOT take this course for credit if you already have credit for CHEM 313.

9. Labs Start Monday January 16 213 Lab Manual (2011-2012) (bookstore) Lab notebook – black ‘Physics notes’ book Safety glasses Lab coat CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

10. How to do well in the 213 Lab ? Read procedures BEFORE entering lab Will preview labs in class (Hot Tips) Hot Tip sheets are posted on Moodle Talk to your friends Take care in sample preparation Take care in calculations/data handling CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

11. Labs Trace Iron by Spectrophotometry Fluoride by Ion Selective Electrode Benzene by Gas Chromatography Nitroanilines Isomers by Liquid Chromatography Sucrose and Glucose by Autoanalysis of Glucose Quinine in Tonic Water by Fluorescence Copper by Atomic Absorption Spectroscopy Dextromethorphan in Cough Syrup by Solvent Extraction Literature Search Lab Notebook CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis Lockers 1 – 12 start with Lockers 13 – 24 start with one of

12. Lectures Preview of Lab Experiments (5 lectures) Ch. 4 Statistics (Sec. 4.7, 4.8) Ch. 5 Calibration Methods (Sec. 5.3, 5.4) Spectroscopy (12 lectures) Ch. 18 Fundamentals of Spectrophotometry Ch. 20 Spectrophotometers, UV-VIS, FTIR Ch. 21 Atomic Spectroscopy Midterm : (in class February 29) 25% CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

13. Midterm Based on: lectures suggested problems assigned readings experiments Will include some : Multiple choice/matching, Definitions, descriptions, diagrams, calculations ~75% descriptive ~25% calculation CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

14. Lectures (post midterm) Separations Ch. 23 Introduction to Analytical Separations Ch. 24 Gas Chromatography Ch. 25 High Performance Liquid Chromatography Ch. 26 Other Chromatographic Methods Mass Spectroscopy Ch. 22 Mass spectrometry Electrochemistry Ch. 15 Potentiometry and Ion-Selective Electrodes (ISEs) (Ch. 8 Activity) Final (April 23, 9:00 AM, location TBD) 37% CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

15. Final Semi-cumulative ~ 1 / 3 on material before midterm ~ 2 / 3 on material after midterm Similar format to midterm probably more choice and more calculations CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

16. attend class read text do suggested problems will post answers for these problems do additional problems focus on descriptive ask questions online forum in Lecture section of course website How to do well in 213 exams ? CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis

17. Course Information Sheet www.uofaweb.ualberta.ca/tie/ You have a set of handouts about academic integrity, plagiarism, and ways to avoid plagiarism. It is understood that you will have read them and be familiar with the Code of Student Behaviour. This is your warning.