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6890 GC Detectors - The Flame Ionization Detector

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Presentation on theme: "6890 GC Detectors - The Flame Ionization Detector"— Presentation transcript:

1 6890 GC Detectors - The Flame Ionization Detector

2 6890 GC Detectors - The Flame Ionization Detector - Main Components
Igniter Teflon Insulator Collector Interconnect/Spring Electrometer Jet Heater/Sensor Assembly Detector Base Assembly Column Adapter

3 6890 GC Detectors - The Flame Ionization Detector

4 6890 GC Detectors - The Flame Ionization Detector - Theory of Operation
1. H2 - Air Flame 2. Sample is burned in flame 3. When burned produces charged Ions 4. Ions attracted to collector 5. Collector current converted to output via Electrometer

5 6890 GC Detectors - The Flame Ionization Detector
FID EPC Flow Manifold Detector Pneumatic Connection Gas Connections to GC FID Flow Measurement Tool FID Jet Plugged FID Jet

6 6890 GC Detectors - The Flame Ionization Detector
FID Igniter Replacement Complete Detector Assembly FID Collector Removal

7 6890 GC Detectors - The Flame Ionization Detector - Jets
Jets for Capillary-Optimized FID Jet Type Part Number Jet Tip id Capillary G 0.29 mm 0.011" High Temp G 0.47mm 0.018" Jets for Adaptable FID Jet Type Part Number Jet Tip id Capillary 0.29mm 0.011" Packed 0.47mm 0.018" Wide bore 0.030" Packed High Temp Capillary 0.47mm 0.018"

8 6890 GC Detectors - The Flame Ionization Detector

9 6890 GC Detectors - The Flame Ionization Detector

10 6890 GC Detectors - The Flame Ionization Detector
6890 EPC Module Original Design New Detector Mini-fold

11 6890 GC Detectors - The Flame Ionization Detector

12 6890 GC Detectors - The Flame Ionization Detector

13 6890 GC Detectors - The Flame Ionization Detector

14 6890 GC Detectors - The Flame Ionization Detector

15 6890 GC Detectors - The Flame Ionization Detector

16 6890 GC Detectors - The Flame Ionization Detector

17 6890 GC Detectors - The Flame Ionization Detector
Flame won't light Measure Flows Clean/Replace Jet (6850 Jet Test) Are column and fittings tight ? Is the tank pressure high enough ? Is the Detector ON ?

18 6890 GC Detectors - The Flame Ionization Detector
Noisy Baseline Turn off Air/H2 No Contamination Still Noisy problem Yes Electronic/Mechanical Problem Check: Filters,Traps,Gasses Clean Jet Replace Detector Verify Column max Board/ interconnect/ Teflon Insulators

19 HP 6890 - Flame Ionization Detector
Planned Maintenance - Replace Jet (per Customer) - Clean/Replace Collector - Inspect interconnect and spring - Inspect ignitor glo-plug - replace if necessary - Measure H2/Air/Makeup Flows - Turn off H2 and measure FID Leakage Current - < 2pA - Ignite FID - monitor background and noise <20 pA and stable - Run customer sample or Agilent Checkout per Service Manual section 600.


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