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Volumetric Analysis.

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Presentation on theme: "Volumetric Analysis."— Presentation transcript:

1 Volumetric Analysis

2 Study design content • sources of acids and bases found in water (may include dissolved carbon dioxide, mining activity and industrial wastes) • volume-volume stoichiometry (solutions only) and application of volumetric analysis including the use of indicators, calculations related to preparation of standard solutions, dilution of solutions and use of acid-base titrations to determine the concentration of an acid or a base in a water sample.

3 Volumetric Analysis Volumetric analysis involves reacting the sample of unknown concentration with a standard solution – a solution in which the concentration is accurately known. Aim is to find the concentration of a sample experimentally. An acid-base titration is an experimental method that uses specialised equipment to determine the concentration of a solution.

4 Equipment: Volumetric Flask – used to prepare standard solution (accurately weighed/measured sample of the compound is placed into flask and dissolved in de-ionised water) Pipette – Used to accurately measure an aliquot of the solution of unknown concentration to a conical flask Burette- The standard solution is placed in the burette which delivers accurately known volumes of solution.

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6 Titration Volumes from the burette (titres) are added to the conical flask until the solutions are in stoichiometrically equivalent amounts – the equivalence point. The indicator (usually added to the conical flask) usually changes colour at the end point, about one drop after the equivalence point.

7 Experimentation Miniscus:
White tile: A white tile is usually placed beneath the conical flask to help identify the slightest indicator colour changes.

8 Problem:

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