1. MM002plus/007HF comparison #33120: middle resolution range case:
MM002plus: 0.75, 5min!, 3.3Å HF: 0.75deg, 5sec!!, 3.2Å

2. MM002plus Resolving power on large unit cell
35658
0.75deg,
150mm
indexable in R3
5min exp.
2.25Å

3. Low resolution case: #32789
exposure, quality 5.5Å with MM002 and 20min, quality 5
MM002plus: 5min, 0.75deg, 3.3Å min,0.75deg, 2.97Å

4. Data collection with 007HF: #32789: 5.5Å with the old MM002
60sec exposure per 0.5o oscillation,
61 images short data set with:
Summary of data collection statistics
Spacegroup R3
Unit cell dimensions
Mosaicity
Resolution range ( )
Total number of reflections
Number of unique reflections
Average redundancy (1.27)
% completeness (67.2)
Rmerge (0.348)
Reduced ChiSquared (1.17)
Output <I/sigI> (1.6)
5min exposure, 3.3Å spots
20min exposure, 2.97Å spots

5. Summary of resolution limits on data with MM002plus and 007HF source:
XtalID MM002+ MM HF 007HF oldMM002 1_5data
5min 20min 5sec 60sec (20min!)
33120* 3.09 Å 2.75 Å 3.3 Å 2.83 Å 4.4 Å
31470*†/‡ 1.49 Å Å
32513* 4.18 Å 3.58 Å 4.6 Å 3.47 Å 5.0 Å
32789‡ 3.3 Å 3.00 Å 5.5 Å 2.8 Å 5.5 Å
33176‡ 2.25 Å 2.02 Å 3.25 Å 2.98 Å 4.1 Å
35658* 2.1 Å Å
10min
35660* 3.5 Å 3.25 Å Å
26760‡/† 2.6 Å Å 2.57 Å Å
(only007HFtests):
S26291* Å 1.5 Å Å
S26759* Å 2.91 Å Å
* ice on sample, possible damage and less reliable resolution interpretation because of ice rings and spots!
† data collection on MM002plus
‡ data collection on 007HF source
†/‡ data collection first on MM002plus, then on 007HF
‡/† data collection first on 007HF then on MM002plus

6. 26760* data 007HF/MM002plus 007HF: 5min, 156 images
CCD Saturn 944 detector
First data set:
MM002plus:5min, 200 images
IP RAXIS IV detector
Second data set:
Spacegroup I23
Unit cell dimensions
Mosaicity
Resolution range ( )
Total number of reflections
Number of unique reflections
Average redundancy (12.06)
% completeness (100.0)
Rmerge (0.498)
Reduced ChiSquared (1.35)
Output <I/sigI> (3.6)
Average Counts (46)
Spacegroup I23
Unit cell dimensions
Mosaicity
Resolution range ( )
Total number of reflections
Number of unique reflections
Average redundancy (8.80)
% completeness (100.0)
Rmerge (0.359)
Reduced ChiSquared (1.14)
Output <I/sigI> (4.4)
Average Counts (1249)
*Crystal was manually transferred after data collection on HF source, to MM002plus unit.

7. 31470* data MM02plus/007HF MM002plus:5min, 160 images
IP RAXIS IV detector
Second data set:
007HF: 5sec, 360 images
CCD Saturn 944 detector
Second data set:
Spacegroup P212121
Unit cell dimensions
Mosaicity
Resolution range ( )
Total number of reflections
Number of unique reflections
Average redundancy (1.37)
% completeness (42.3)
Rmerge (0.321)
Reduced ChiSquared (1.16)
Output <I/sigI> (1.7)
Average Counts (82)
Spacegroup P222
Unit cell dimensions
Mosaicity
Resolution range ( )
Total number of reflections
Number of unique reflections
Average redundancy (1.91)
% completeness (79.4)
Rmerge (0.173)
Reduced ChiSquared (0.27)
Output <I/sigI> (1.9)
Average Counts (3714)
*Crystal was manually transferred after data collection on MM002plus source,
to 007HF rotating anode source.

8. Cost of MM-002+ / MM-007 HF Price w/discount $138,000 $253,000
Service Contract (est) $19, $15,000
Filiments N/A $1350-$ $1030/3 need 4-5/yr
Anode Rebuild N/A $ (1/yr included in service contract price)
4 yr cost of ownership $196,500 $301,000 w/ service contract (Est)