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Freeze of Nozzle/Receptacle during Hydrogen Fueling

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Presentation on theme: "Freeze of Nozzle/Receptacle during Hydrogen Fueling"— Presentation transcript:

1 Freeze of Nozzle/Receptacle during Hydrogen Fueling
Wataru Hiraki1, Hiroyuki Mitsuishi1 1Japan Automobile Research Institute

2 Hydrogen station Compressor Pressure vessel Dispenser FCV Overpressure Pressure [MPa] Overheat Temperature [°C] Overfill 85 70 15 SOC 100% 87.5 -40 use Pre-cool Hydrogen station is possible about fast-fueling safely, using pre-cool

3 Issue of nozzle/receptacle freeze lock
Disconnection Freeze lock Ice forms during fueling which causes the nozzle and receptacle to freeze together. This phenomenon is not specific to a single nozzle/receptacle design.

4 Object Safety evaluation of the nozzle/receptacle freeze lock
Confirmation of a water amount to cause the freeze lock

5 Test condition & Experiment setup
Fueling gas: Hydrogen, 35 MPa Nozzle Receptacle Thermocouple T Gas Sensor Incubator N2 Nitrogen Gas temperature: -40°C Ambient temperature: 30°C Hydrogen Ambient humidity: 95 %RH Flow rate: 650 g/min Fueling time: 3 min Test interval: 10 min Nozzle: A, B(Two types) Water added : Nozzle, Receptacle Condition for the end of the test: Freeze lock occured or pass for 5 times

6 Experiment setup Receptacle Incubator Nozzle connected nozzle

7 Disconnect procedure Procedure for identification of freeze lock
(1) Slidable locking sleeve is released (2) Draw out the nozzle  ⇒  disconnect Receptacle Nozzle Chuck Sleeve Receptacle Nozzle Chuck Sleeve (1') Chuck goes up Receptacle Nozzle Chuck Sleeve (※Shape of the sleeve and inner chuck are estimated) Procedure for identification of freeze lock Check immediately after the fueling Action for the disconnection; Revolve → Release the locking mechanism → Draw out Identify as freeze lock if the nozzle is not disconnected in the above condition

8 Water Spraying Position
Nozzle Receptacle Chuck Sleeve Hydrogen Gas Line Pin Cover spray Nozzle Receptacle Fitting part Fitting part

9 Release the Locking mechanism
Freeze lock Nozzle Water added Results Freeze lock Revolve Release the Locking mechanism Darw out A Receptacle 2nd fueling possible impossible

10 Release the Locking mechanism
Freeze lock Nozzle Water added Results Freeze lock Revolve Release the Locking mechanism Darw out A Nozzle, Receptacle 1st fueling possible impossible

11 Release the Locking mechanism
Freeze lock Nozzle Water added Results Freeze lock Revolve Release the Locking mechanism Darw out B Receptacle 5th fueling possible impossible

12 Release the Locking mechanism
Freeze lock Nozzle Water added Results Freeze lock Revolve Release the Locking mechanism Darw out B 1st fueling possible impossible

13 Result Freeze lock is caused by water inside the nozzle.
Hydrogen does not leak from the nozzle/receptacle even if the nozzle/receptacle were freeze lock. Freeze lock does not cause any damage of the equipment.

14 Estimation of freezing part
Result Incidence Revolve Release the Locking mechanism Draw out possible impossible 14/16 (Nozzle A) 13/14 (Nozzle B) Clearance of sleeve Chuck part Fitting part Receptacle Nozzle Chuck Sleeve Estimated freezing part:Clearance of sleeve, Chuck part

15 Water injection method
Effect of a water amount on freeze lock Water injection method Micropipette Nozzle head Water is injected to the nozzle inside before fueling. Connect to receptacle and flow -40°C gas Freeze lock?

16 Test condition & Experiment setup
Nozzle Receptacle Thermocouple T Gas Sensor Incubator N2 Nitrogen Fueling gas: Hydrogen, 35 MPa Gas temperature: -40°C Ambient temperature: 30°C Hydrogen Ambient humidity: 60 %RH Flow rate: 650 g/min Fueling time: 3 min Nozzle: A Water added : injection the Nozzle

17 Release the loking mechanism
Result of Quantification Water injection [μL] Results Revolve Release the loking mechanism Draw out 500 possible 750 1000 impossible After fueling Freeze lock

18 Conclusions ・ The nozzle and the receptacle are safely, even if the freeze lock occurred ・ The freeze lock is caused by the water freezing in the locking mechanism of the nozzle ・ The freeze lock occurred after fueling when water of 1000 μL over 750 μL injected to the nozzle A

19 Next step Experiment of the freeze lock
Investigation of the freeze lock with other nozzles. Investigation of ambient condition when the freeze lock occurs. Investigation of a technique that protect the freeze lock. Proposition of the freeze lock testing condition and procedure

20 Thank you for your attention
ACKNOWLEDGEMENTS This study is a summary of the “Hydrogen Using Technology Research and Development Project”, and the "Hydrogen production, transportation and storage system technology development" under consignment by the New Energy and Industrial Technology Development Organization (NEDO). Thank you for your attention


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