1. Introduction to Analytical Chemistry Dr Carl HallX1/12 c.e.hall@hud.ac.uk SFC1004 Analytical Science 1

2. Module Outline l 24 Lectures v Tuesdays 11.15 - 12.15 n Autumn Term - Carl Hall n Spring Term - Richard Southam l 24 Tutorials v Tuesdays 12.15 - 1.15 l 6 four hour labs v Last six weeks of Spring term

3. Module Outline l Lectures v The PowerPoint lecture material is only the outline of the course YOU NEED TO MAKE YOUR OWN NOTES AS WELL! v Handouts will be available at beginning of lecture. v The lecture material is also available from the Universities Blackboard website at http://vitual.hud.ac.uk. http://www.hud.ac.uk http://icilda.hud.ac.uk/?bbatt=Y

5. Assessment Profile l Continuous Assessment - 35% v Tutorials in Autumn term - 10 minute MCQ tests based on selected tutorial questions. n Weekly feedback for students n Identifies strengths and weaknesses n Ensures that tutorial work is completed n Removes the need for additional assessments l Practicals - 25% l Exam - 40% v 2 x 1 hour tests in weeks 16 and 31

7. Outline Syllabus l Quantitative Analysis n Types of method n Units l Data Handling n Significant figures n Origin of errors n Estimation of uncertainty n Accuracy and Precision n Basic Statistics n Data presentation

8. Outline Syllabus l Titrimetric analysis l Gravimetric analysis l Colorimetric analysis l Spectroscopic Analysis n Infra-red - ir n UV visible

9. References l Quantitative Chemical Analysis v Daniel Harris - 6th Edition - 2002 n Supporting material available on website l Exploring Chemical Analysis v Daniel Harris - 2nd Edition - 2001 l Analytical Chemistry - An Introduction v Skoog, West, Holler and Crouch - 7th Edition - 2000 l Quantitative Chemical Analysis v Vogel - 6th Edition

10. References l Introduction to Spectroscopy v Pavia, Lampman and Kriz - 2nd Edition - 1996 l The Molecular World - Separation, Purification and Identification v Lesley Smart - 2002 l Spectroscopic Methods in Organic Chemistry v Dudley Williams and Ian Fleming - 5th Edition -1995