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HIGH PURITY PIPING SYSTEMS PURAD. Material properties with leach-out behaviour Production and quality control Supply Program Application in the high tech.

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Presentation on theme: "HIGH PURITY PIPING SYSTEMS PURAD. Material properties with leach-out behaviour Production and quality control Supply Program Application in the high tech."— Presentation transcript:

1 HIGH PURITY PIPING SYSTEMS PURAD

2 Material properties with leach-out behaviour Production and quality control Supply Program Application in the high tech industries Seal clean gasket Product library CONTENT Material properties Production Supply Program Application Seal clean gasket Product library 2

3 Materials important, which do not contain any or only leach-out resistant additives and avoid the growth of micro-organisms like: PVDF UHP (PVDF Ultra High Purity) PP-Pure (PP-HP grey) Polypure (PP-natural) ECTFE PURAD Program includes all those piping systems which transport ultra pure water or exhausts. PREFERRED MATERIALS Material properties Production Supply Program Application Seal clean gasket Product library 3

4 PVDF (Polyvinylidene-fluoride) Operating temperature: From - 40 °C up to °C PP (Polypropylene) Operating temperature: From - 5 °C up to °C ECTFE (Ethylenchlortrifluorethylen) Operating temperature: From - 76 °C up to °C CC F H H n F STRUCTURE CCCC H Cl F HFF H H n CC HCH 3 HH n Material properties Production Supply Program Application Seal clean gasket Product library 4

5 PVDF PROPERTIES Translucent material Density of 1.78 g/cm3 FM approved material Fire resistant (UL 94-V0) Excellent chemical resistance (even at high temperature) Resistant against UV- and gamma radiation Excellent mechanical, insulating and abrasion properties Very good processing characteristics Physiologically non-toxic Material properties Production Supply Program Application Seal clean gasket Product library 5

6 Pipes, fittings, valves and semi-finished products are produced with one type of raw material. Pipe Solef 1010 Fitting Solef 1008 Valve Solef 1008 Semi-finish. Solef 6010SolefSolef PVDF UHP Solef is a Product of SOLVAY Solexis S.A. Belgium TYPE OF RAW MATERIAL Material properties Production Supply Program Application Seal clean gasket Product library 6

7 PVDF Suspension Grade Solef ® Emulsion Grade Kynar ® lower number of molecular defects higher crystalinity higher melting temperature better mechanical properties better long term behaviour higher cleanliness higher number of molecular defects lower crystalinity limited mechanical properties reduced pressure resistance at elevated temperatures lower purity and higher yellowness MATERIAL GRADES AVAILABLE Material properties Production Supply Program Application Seal clean gasket Product library 7

8 Suspension Grade PVDF Superior Mechanical Strength Better Purity Performance Stronger Weldings MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 8

9 Solef ® Kynar ® Time factor: service life SOLEF - service life KYNAR ~ 3,5 Long term tensile test at 95 °C with arcopal N-100 Higher Service life based on similar stress levels MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 9

10 TRANSPORT BOX Material properties Production Supply Program Application Seal clean gasket Product library 10

11 Pipes, fittings, valves and semi-finished products out of the same moulding compound: Identical colour index Better weldability of the components (MFR) Better long term welding factor Higher reliability Better pressure resistance Identical mechanical properties Product cleanliness Best surface smoothness Best leach-out behaviour PVDF UHP COMPONENT ADVANTAGES Material properties Production Supply Program Application Seal clean gasket Product library 11

12 Semi Spec. for (up to OD 225): Extruded pipes: Ra = 0,25 µm Injection moulded fittings: Ra = 0,38 µm 0 0,05 0,1 0,15 0,2 0,25 0, >250 UHP pipesAct. Values Ra [µm] OD [mm] Semi Spec. limit for pipes. UHP fittings Better surface quality MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 12

13 PURITY TESTING SEMI F Classic Leach-out Test for Piping Components Test of Pipe Component Surface Suitable for Production Control SEMI F Bulk Trace Metals Analyses Test of Pipe Material Suitable for Resin/Raw Material Control MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 13

14 Leach out test acc. Semi F 057 MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 14

15 values given in [µg/m2] Source: Test reports from M+W STATIC LEACH-OUT TEST F057 Material properties Production Supply Program Application Seal clean gasket Product library 15

16 Leach out behaviour (TOC) Style 800 Source: Solvay test labratory (2006) STATIC LEACH-OUT TEST F057 Material properties Production Supply Program Application Seal clean gasket Product library 16

17 Leach out behaviour (FLUORINE) Style 800 Source: Solvay test labratory (2006) STATIC LEACH-OUT TEST F057 Material properties Production Supply Program Application Seal clean gasket Product library 17

18 Style 800 STATIC LEACH-OUT TEST F057 Material properties Production Supply Program Application Seal clean gasket Product library 18

19 SEMI F-48 TESTING Material properties Production Supply Program Application Seal clean gasket Product library 19

20 PVDF-UHP Piping Colour index and thermal stability MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 20

21 Solef PVDF meets the following standards: US FDA Title 21, Part 177, Sect NSF/ANSI Standard 51 Food Equipment Materials NSF/ANSI Standard 61 Drinking Water System Components 3A Sanitary Standards for MultipleUse Plastic Materials Used as Product Contact Surfaces for Dairy Equipment United States Pharmacopia (USP) Classification VI E UL/ Bulletin 94V0 ASTM E84 Modified Steiner Tunnel Test FM Global 4910 specification tested products PVDF APPROVALS Material properties Production Supply Program Application Seal clean gasket Product library 21

22 Low specific weight of 0.91 g/cm³ (PVC 1.40) High creep and ageing resistance Very good chemical resistance Physiological non-toxic Good weldable Excellent abrasion resistance Non-conductive Very good processable Not UV-resistant PP PROPERTIES Material properties Production Supply Program Application Seal clean gasket Product library 22

23 3 different Types according DIN 8078: Type 1:PP-H (Homopolymer) P – P – P – P – P – P Type 2:PP-B (Block-Copolymer) P – E – E – E – P – P Type 3:PP-R (Random-Copolymer) P – E – P – P – E – P By copolymerisation with ethylene special properties are achieved as in PP types 2 and 3 (improved processability, higher impact strength). PP TYPES Material properties Production Supply Program Application Seal clean gasket Product library 23

24 Pipes, fittings, valves and semi-finished products are produced with one type of raw material. TYPE OF RAW MATERIAL PP-RPP-R PP-Pure (PP-HP grey) PP-Pure Pipe PP-R grey Fitting PP-R grey Valve PP-R grey Semi-finish. PP-R grey Material properties Production Supply Program Application Seal clean gasket Product library 24

25 Pipes, fittings, valves and semi-finished products are produced with one type of raw material. PP-RPP-R Polypure (PP natural) Polypure Pipe PP-R natural Fitting PP-R natural Valve PP-R natural Semi-finish. PP-R natural TYPE OF RAW MATERIAL Material properties Production Supply Program Application Seal clean gasket Product library 25

26 Same material properties as PP-Pure differences: no color pigments translucent material MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 26

27 values given in [µg/m2] Source: Test reports from M+W STATIC LEACH-OUT TEST F057 Material properties Production Supply Program Application Seal clean gasket Product library 27

28 PP-HPP-R Welding quality (e.g. bending angle acc. DVS ) Significant lower than PP-R (PP-H with PP-H and PP-B) Bending angle > 160 ° (even with PP-H, PP-B and PP-R) c m -factor (material safety coefficient) 1.6 – 1.4 – 1.25 Permissible operating pressure lower 10.5 bar 1.25 Very good impact resistance 13.1 bar Voids (of fittings) Increasing riskGood processibility E-modulus Higher E-modulus support distance higher Lower E-modulus support distance lower COMPARISON PP-H vs. PP-R Material properties Production Supply Program Application Seal clean gasket Product library 28

29 PP-HPP-R Impact strength Lower impact strength, Operation Temperature: + 5 °C up to + 95 °C Higher impact strength, Operation Temperature: – 5 °C up to + 95 °C Tension-relaxion Low relaxation because of higher E-modulus Fast relaxation because of lower E-modulus Surface quality Sufficient Smoother surface due to ethylene-compounds Leach-out behaviour Satisfactory (typical PP) Much better due to surface quality COMPARISON PP-H vs. PP-R Material properties Production Supply Program Application Seal clean gasket Product library 29

30 Higher applicable working pressures for PP-R MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 30

31 Source: Hessel Ingenieurtechnik GmbH 2002/ °C / 2% liquid wetting agent Nm5 (4 N/mm2) FNCT basic material Time in hours Higher Service life based on similar stress levels MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 31

32 Minimum required bending angle (DVS ) Bending angle Specimen thickness PPH PPR MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 32

33 0 0,2 0,4 0,6 0,8 1,0 1, fittings pipes Ra [µm] OD [mm] Excellent surface quality MATERIAL GRADE COMPARISON Material properties Production Supply Program Application Seal clean gasket Product library 33

34 MaterialBrand nameGeneral chem. Resistance Polypropylene PP-Pure Polypure Hydrous solutions of acids, alkalis and salts as well as a large number of organic solvents. Unsuitable for concentrated oxydizing acids. Polyvinylidene- fluoride PVDF UHP Acids, solutions of salt, alpatic, aromatic and chlorinated hydrocarbons, alcohols and halogens, conditionally suitable for ketones, esters, ether, organic bases and alkaline solutions. For detailed information please refer to our PURAD High Purity Piping System Catalogue or browse our web: CHEMICAL RESISTANCE Material properties Production Supply Program Application Seal clean gasket Product library 34

35 FM-approval for the Solef PVDF raw material APPROVALS Material properties Production Supply Program Application Seal clean gasket Product library 35

36 FDA-approval for the materials: Solef PVDF PP-grey PP-natural APPROVALS Material properties Production Supply Program Application Seal clean gasket Product library 36

37 FACILITIES Factory I: Injection moulding of fittings, packaging, machining, assembling and tooling facility Clean room area: 200 m²Class 100 acc. Federal Standard 900 m²Semi clean area Output capacity: ~ HP - fittings / year PRODUCTION Material properties Production Supply Program Application Seal clean gasket Product library 37

38 Resin supply Designated mould stock Injection moulding under cleanroom condition PRODUCTION FACILITIES Factory I: Injection moulding of fittings, packaging, machining, assembling and tooling facility Material properties Production Supply Program Application Seal clean gasket Product library 38

39 Cleaning/rinsing plant Moulding set upMachining-box fully automatizised PRODUCTION FACILITIES Factory I: Injection moulding of fittings, packaging, machining, assembling and tooling facility Material properties Production Supply Program Application Seal clean gasket Product library 39

40 Final product packagingCleanroom for assembling and packaging Cleanroom monitoring system FACILITIES Factory I: Injection moulding of fittings, packaging, machining, assembling and tooling facility PRODUCTION Material properties Production Supply Program Application Seal clean gasket Product library 40

41 Clean room area: 200 m² Class 100/1000 acc. Federal Standard Output capacity: m HP - pipes / year (~ 1800 tons of PVDF-HP pipes) 2 production units for PVDF- HP 1 production unit for PP-Pure/Polypure PRODUCTION FACILITIES Factory II: Extrusion of pipe s and semi- finished products, packaging Material properties Production Supply Program Application Seal clean gasket Product library 41

42 Extrusion lines in cleanroom Pipe extrusion department PRODUCTION FACILITIES Factory II: Extrusion of pipes and semi- finished products, packaging Material properties Production Supply Program Application Seal clean gasket Product library 42

43 Final product packagingPackaging area in cleanroom FACILITIES Factory II: Extrusion of pipes and semi- finished products, packaging PRODUCTION Material properties Production Supply Program Application Seal clean gasket Product library 43

44 Set up for PP-Pure and POLYPURE production (packaging under laminar flow) Automatizised Cleanroom monitoring system Analytical surface testing in cleanroom PRODUCTION FACILITIES Factory II: Extrusion of pipes and semi- finished products, packaging Material properties Production Supply Program Application Seal clean gasket Product library 44

45 Purity Test MFR Moisture Yellowness QC- Document of Supplier Batch testing Documentation QUALITY CONTROL Material properties Production Supply Program Application Seal clean gasket Product library 45

46 Batch testing Documentation Surface characteristic Purity Yellowness index MFR Long term pressure test Dimension/Marking control X-Ray testing fitting Packaging control Leak testing of valves 100% visual product control QUALITY CONTROL Material properties Production Supply Program Application Seal clean gasket Product library 46

47 Product testing Documentation Surface behavior Leach out testing TÜV-Testing (mechanical tests) FM-certification Customer audits Batch testing Documentation Monitoring of stock level (Computer controlled) Controlled storage conditions First in / First out system or based on batch numbers Product storage External product validation QUALITY CONTROL Material properties Production Supply Program Application Seal clean gasket Product library 47

48 Documentation External product validation Product storage Production of pipes, fittings, valves Storage of approved POLYMER QC- Certificate Documentation QUALITY CONTROL Material properties Production Supply Program Application Seal clean gasket Product library 48

49 Full traceability for all production parameters, QC, polymer are ensured by batch numbers on each component. All relevant product properties, specifications, QC procedures are fixed in an internal company standard. QUALITY CONTROL Material properties Production Supply Program Application Seal clean gasket Product library 49

50 Complete portfolio of: Pipes, fittings & valves Electro fusion fittings Semi-finished products Flow meters Custom made fittings Pipe clips Sanitary joint fitting Welding equipment Service & training One-Stop ShoppingOne-Stop Shopping Pipe & Sheet stock SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 50

51 Pipes: Fittings: SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 51

52 Electro Fusion Fittings: Valves, Flow Meters, Fittings: SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 52

53 Pipe Code 705 Stub Flange DIN, ANSI, JIS Code 012 Bend Code 001 Code 068 Tee Code 006 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 53

54 Union Type 24 Code 024 Adaptor Male Thread Code 033 Adaptor Female Thread Code 032 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 54

55 Elbow 45 ° Code 060 Tee long Code 066 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 55

56 Tee reduced long Code 065 Tee reduced short Code 016 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 56

57 Tee reduced Machined Code 307 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 57

58 Instrumentation Fitting Injection moulded Code 030 Instrumentation Fitting Machined Code 303 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 58

59 Sanitary Joint Fitting Code 306 Reducer concentric Code 007 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 59

60 Reducer concentric Code 067 Reducer concentric Machined Code 317 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 60

61 Restrained Fitting Code 028 Restrained Fitting Machined Code 301 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 61

62 End Cap Code 064 Transition Fitting Code 047 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 62

63 HPF-socket Code 073 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 63

64 Ball Valve Butt welding, Flange connection Code 335 Sampling Valve Code 337 Material: PVDF UHP, Pressure: MOP 10 bar Dimension: OD 10 mm SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 64

65 Diaphragm Valve Union connection Code 340 Diaphragm Valve Flange connection Code 242 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 65

66 Diaphragm Valve Butt-, IR- and HPF Code 342 T-Diaphragm Valve Code 343 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 66

67 Diaphragm Valve Pneumatic Closed, open and double effective impulse Code 341 T-Diaphragm Valve Pneumatic Closed, open and double effective impulse Code 345 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 67

68 Check Valve + Spring Code 336 Swing Type Check Valve With or without spring Code 339 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 68

69 Pressure Reducing Valve V82 With gauge guard/PTFE Code 241 Pressure Reducing Valve V782 Without gauge guard/PTFE Code 243 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 69

70 Pressure Retaining Valve Code 244 Pressure Relief Valve Code 245 Gauge Guard Code 248 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 70

71 Flow Meter M123 Code 246 Flow Meter M23, M335 Code 247 SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 71

72 SUPPLY PROGRAM ECTFE Pipe Code 705 Stub Flange DIN, ANSI, JIS Code 012 Bend Code 001 Code 068 Tee Code 006 Material properties Production Supply Program Application Seal clean gasket Product library 72

73 SUPPLY PROGRAM ECTFE Union Type 24 Code 024 Adaptor Male Thread Code 033 Adaptor Female Thread Code 032 Material properties Production Supply Program Application Seal clean gasket Product library 73

74 SUPPLY PROGRAM ECTFE Elbow 45 ° Code 060 Reducer concentric Code 067 Material properties Production Supply Program Application Seal clean gasket Product library 74

75 SUPPLY PROGRAM ECTFE End Cap Code 064 Transition Fitting Code 047 Material properties Production Supply Program Application Seal clean gasket Product library 75

76 SUPPLY PROGRAM ECTFE Diaphragm Valve Butt-, IR- and HPF Code 342 Diaphragm Valve Pneumatic Closed, open and double effective impulse Code 341 Material properties Production Supply Program Application Seal clean gasket Product library 76

77 Custom made Components: SUPPLY PROGRAM Material properties Production Supply Program Application Seal clean gasket Product library 77

78 Special components: PRUDUCT AVAILABILITY Material properties Production Supply Program Application Seal clean gasket Product library 78

79 SYSTEM SOLUTIONS FROM AGRU APPLICATION IN THE HIGH TECH INDUSTRIES

80 in use since 1980 strongly rising application without plastic systems the product qualities and technologies obtained today could not be achieved high efficiency highest quality for highest requirements most cost effective solution complete solutions available GENERAL Material properties Production Supply Program Application Seal clean gasket Product library 80

81 Application range Semi-conductor Logic/D-Ram/Flash Silicium-Wafer- manufacturing Polycrystalline silicon discs/sheets Photovoltaic Silicon cells (Poly-(Multi) Crystalline) Nanotechnology CD-production Flat Panel (FPD) TFT/LCD/PDP Electronic industry (PCB) Print-Circuit-Board Hard-Disc-Drives SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 81

82 Application range Food-industry Brewery, beverage industry Hospitals Maintenance of ultra pure media, dialysis systems Universities Construction of power plants Research facilities Pharma production Biotechnology Production of ultra pure media Chemicals, cosmetics and automotive industry SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 82

83 Fab design CUB... Central Utility Building (building technology – premises) - high purity water system - process cooling water treatment - waste water processing facility (usually separate building) SUBFAB (supply fab) cleanroom conditions: cl to / 5 to 7 - exhaust air treatment - exhaust air piping - treatment of chemicals - supply system for production process - electrical installations CLEANROOM cl. 1 to complete equipment for product manufacturing - processing units - hook up installation SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 83

84 Fab – supply and production systems Chemical supply system Polishing system Waste water treatment Chemicals/ waste water disposal Exhaust air Compressed air (pure dry air) Process vacuum Ultra high purity water maintenance Specific water quality Process cooling water Tanks Process facilities Customer specific facilities SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 84

85 Fabs comparison similar technology in manufacturing reduced quality of high- purity-media (currently) smaller plant sizes (currently) Different way of project- processing (system-solution of general contractor) no CMP-Slurries in use reduced requirement to purity of product (currently) SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 85

86 Ultra high purity water supply Differences exist in the water quality Bacteria quantity:...cfu/ml TOC:...ppb or µg/l Conductivity:...µs or MOhm Anions/Cations:...ppb or µg/l Temperature:...cold (15 – 20 °C)...hot (85 °C) UPW...Ultra Pure Water AP...Purified Water HPW...High Purified Water DI...Dionisized Water WFI...Water for injection...Specified Water SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 86

87 Hook Up Loop Supply UPW...Ultra Pure Water AP...Purified Water HPW...High Purified Water DI...Dionisized Water WFI...Water for injection...Specified Water Differences exist in the water quality Bacteria quantity:...cfu/ml TOC:...ppb or µg/l Conductivity:...µs or MOhm Anions/Cations:...ppb or µg/l Temperature:...cold (15 – 20 °C)...hot (85 °C) Ultra high purity water supply SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 87

88 Pre-cleaning Water treatment Ultra high purity water treatment Loop supply line/return line Submain supply line/return line Hook Up supply line/return line PVC, SS, PE, PP PP, (PVC, SS) PVDF-UHP, PP-Pure, Polypure PVDF-UHP / PP-Pure, Polypure Tanks (RO / UPW tank) FRP, steel with PP or PVDF lining Ultra high purity water supply SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 88

89 Supply systems Process cooling water (PCW) PP, SS, PVC, PE PP, PVC, PVDF, ECTFE Pipe/Double containment systems Chemicals / waste water treatment CMP-treatment Acid/Alkaline treatment Ammonia treatment HF treatment Copper treatment H 2 SO 4 treatment Dilute Metals treatment SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 89

90 Supply systems Chemicals / waste water treatment Chemical mixing system and distribution CMP (chemical mechanical polishing slurry) Exhaust systems PP, PVC, PVDF, ECTFE Pipe/Double containment piping system (with transparent PVC) PFA, PVDF, ECTFE, PP-natural Pipe/Double Containment piping system (with transparent-PVC) PFA, PP-natural (advantage of PP-natural: high stiffness, no installation of double containment piping necessary, cost-effective) SS-coated, PVDF, ECTFE SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 90

91 Process chains in the Photovoltaic (silicon solar cells) Solar wafer manufacturing Pre-cleaning of the crystal Separating / cutting Cleaning Transfer system Inspection SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 91

92 Process chains in the Photovoltaic (silicon solar cells) Solar cell manufacturing Etching of cutting damages with a mixture of hydroflouric and nitric acid (surface enlargement) Texturing (etching - rinsing (UPW) - NaOH rinsing - HF process - rinsing (UPW) - drying Transfer system Doting by means of phosphorus/water clouds – annealing in the diffusion oven for creation of emitter/pn barrier Oxide etching (remove of the phosphorus glass film) Edge isolation (mostly with laser technology) Single-side etching Electroplating Characterisation SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 92

93 Photovoltaic – Production concept Fully integrated equipment concepts including automated material handling Equipments up to 60 m length Equipments generally consist of high-grade thermoplastics due to the used wet processes as well as requirements on purity and leach-out behavior FM 4910 listed products are preferred SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 93

94 Processing units for Photovoltaic (silicon solar cells) PP, PP-white, PP-natural PP, PP-natural, PVDF, ECTFE PFA, ECTFE, PVDF, PP PFA, PVDF-UHP, PP-Pure, Polypure PVC, PP, PVDF, PP-natural, ECTFE Semi-finished products Semi-finished prod. Chemicals UPW Chemical / Waste Drain Frames/cover panels Process basin Piping systems Welding technologies: Hot gas welding/Extrusion welding for semi-finished products IR-welding for piping systems (also for PFA) Flare-links for small PFA-dimensions SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 94

95 SS-coated, PVC, PPs, PP, PVDF (FM 4910), PipesExhaust air system Processing units for Photovoltaic (silicon solar cells) PFA, ECTFE, PVDF, PP-natural, teflon Regulating valves, flow meters, pH measurement, gauge guards Measurement and control technology PFA, PVDF, ECTFE Filters PTFE, PFA Semi-finished products/round bars Pumps PP, PVDF, ECTFE Semi-finished products/round bars Transport system SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 95

96 Processing units for Semiconductor compact construction transport system with so-called "carrier boxes" same materials as used for Photovoltaic facilities currently available for wafer sizes up to 300 mm (12") larger equipments same transport system as used for Photovoltaic facilities usually out of PP Processing units for PCB SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 96

97 Chemical mixing stations PP, PP-white, PP-natur PFA, PVDF, ECTFE, PP-natural PTFE, PFA PFA, PVDF, ECTFE PFA, teflon, PVDF, ECTFE Semi-finished products Medias Filter Measurement and control technology Regulating valves, flow meters, pH measurement, gauge guards Frames/cover panels Piping systems Pumps SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 97

98 References Semiconductor 1st Silicon AMD AMS Austria Mikro Systeme A-Nam Atmel Bosch CSM Cypress Semiconductor Dong Bu Flush Partners Grace Semiconductor Hynix IBM IMFT Infineon Inotera Intel Komag LG Silcon LG Philips Micron Mosel Vitalic Motorola National Semiconductor NEC Osram Philips Powerchip Prologic Promos PSC Samsung Samsung LCD Seagate Shanghai Belling Microelectronics Silterra SMIC Sony SSMC ST Microelectronics Tech Semiconductor Texas Instruments Toshiba Tower TSMC UMC UMCI Vanguard Vistera Wacker Wacker Siltronics Winbond Xi Yue SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 98

99 References Solar USA - Global Solar (Tucson, AZ) - Sunpower - First Solar Germany - Q-Cells AG - Deutsche Solar AG - Kilimanjaro (First Solar) / Frankfurt/Oder - ErSol Solar Energy AG - Bosch Arnstadt China - Suntech - LDK Norway - REC Philippines - Sunpower Malaysia - First Solar - Sunpower - Q-Cells Spain - BP Solar Singapore -REC India - Solar Semiconductor SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 99

100 References Pharma / Hospitals / Research facilities USA: - Dartmouth Science Bldg - Mallinckrodt Baker - Genzyme - Ventana Medical - Amgen - Women & Infants Hospital - Elan - Merck - Forrest Labs - John Hopkins Hospital - Hamilton College - 4C Clinic VA Mediacl Center - Wester WA U - University of Michigan - North Carolina State Vet. Lab. - University of Wisconsin Biotech. Center - Applied Bioscience Pfizer (USA, IRL, SG) Glaxo Welcome (UK) Glaxo SmithKline (UK) Pepthysintha (B) Pharmacie Centrale de LArmée (F) Sachem (CN) Lonza (SG) Johnson & Johnson (USA, IRL, Puerto Rico, B, UK, SG) Wyeth (SG, USA, Philippines) Janssen Pharmaceutica (B) SYSTEM SOLUTIONS Material properties Production Supply Program Application Seal clean gasket Product library 100

101 FPD-Industry: (Thin Film Transistor – Liquid Crystal Display: TFT-LCD, Plasma Display Panel: PDP) AO Optoelectronics, Chunghwa Picture Tubes, LG Philips LCD P3 - P6 and P7, LG-LCD, Samsung,… REFERENCES Material properties Production Supply Program Application Seal clean gasket Product library 101

102 SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 102

103 Style 800 : Advantages: Made form 100 % virgin PTFE High resistance against chemicals and high temperatures PTFE with a multidirectionally orientated fibrous structure Very low diffusion values High dimensional stability and creep resistance Seals even at low bolt torques High blowout resistance SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 103

104 Style 800 Benefits: Available for plastic flanges in DIN, ANSI and JIS Gasket dimensions especially designed for AGRU stub flanges PVDF UHP, PP-Pure, (minimised dead leg areas) No gap inside Minimal torque values necessary UHP quality available Centre from flange OD (see picture) SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 104

105 Style 800 SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library

106 Style 800 Before Installation After Installation Highly densified ePTFE as a diffusion layer SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 106

107 Style 800 Gasket is suitable for PN 16 (TÜV approved) SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 107

108 Test duration: 24 hours Test medium: 5 % HNO 3 Test equipment: ICP-MS Test unit: ng metal / gasket SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 108

109 Style 800 Leach-out Behaviour: Comparison of the AGRU Seal Clean ePTFE gasket versus conventional EPDM/PTFE profile flange sealing: 1. Type A 2. Type G SEAL CLEAN GASKET Material properties Production Supply Program Application Seal clean gasket Product library 109

110 PRODUCT LIBRARY FOR ALL ESTABLISHED CAD-SYSTEMS

111 All different piping products are available in 2D and 3D More then 90 different data formats are online available 2D vector data and 3D solids are generated from one Data source Colour, thickness and type of the lines can be changed individually The library is available through the internet or on CD Free of charge! CONTENT Material properties Production Supply Program Application Seal clean gasket Product library

112 Exact measurement of the products A complete library is available for the design engineers Efficient and fast design of isometrics is the benefit 3D2D 3D ADVANTAGE Material properties Production Supply Program Application Seal clean gasket Product library

113 Native format: - ADEM - AllPlan - AutoCad - Bihler CAT - Cadceus - Caddy - CADISON - Cadkey - Cadra - Catia - CCD/ProfCADAM - Cimatron - Fides - Helix - HiCAD - Ideas - Inventor - Logocad Triga - Mastercam - Materialise - Mechanical Desktop - Medusa - MegaCAD - Microstation - One Space Designer - Parasolid - ProE - SolidDesigner - SolidEdge - SolidWorks - Swiss Precision - Thinkdesign - TopSolid - Unigraphics - Varimetrix - Visi Series - and others..... SUPPORTED CAD-SYSTEMS Material properties Production Supply Program Application Seal clean gasket Product library

114 Neutral format: - SAT - STEP - IGES - DXF - VRML - DWG - and others.... SUPPORTED CAD-SYSTEMS Material properties Production Supply Program Application Seal clean gasket Product library

115 SUPPORTED CAD-SYSTEMS Material properties Production Supply Program Application Seal clean gasket Product library

116 AGRU Kunststofftechnik GmbH Ing.-Pesendorfer-Str. 31 A-4540 Bad Hall Austria / EU T +43 (0) F +43 (0) E Subject to errors of typesetting, misprints and modifications. Illustration are generic and for reference only! THANKS FOR YOUR ATTENTION


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