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间歇精馏 - 吸附耦合工艺 课题进展 袁利. Review  Introduction  Discussion on definition of Hybrid Process  Lipnizki, F., R.W. Field, and P.K. Ten, Pervaporation-based.

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Presentation on theme: "间歇精馏 - 吸附耦合工艺 课题进展 袁利. Review  Introduction  Discussion on definition of Hybrid Process  Lipnizki, F., R.W. Field, and P.K. Ten, Pervaporation-based."— Presentation transcript:

1 间歇精馏 - 吸附耦合工艺 课题进展 袁利

2 Review  Introduction  Discussion on definition of Hybrid Process  Lipnizki, F., R.W. Field, and P.K. Ten, Pervaporation-based hybrid process: a review of process design, applications and economics. Journal of Membrane Science, 1999. 153(2): p. 183-210.  Different hybrids specification and their application, benefits, in general  Skouras, S. and S. Skogestad, Time requirements for heteroazeotropic distillation in batch columns. Computers & Chemical Engineering, 2004. 28(9): p. 1689-1700.  Zhang, X.M., et al., The operation of draining column holdup for slop cut withdrawal in batch distillation. Chinese Journal of Chemical Engineering, 2006. 14(3): p. 337-342.  Design, modeling and simulation approach of hybrid process  Peters, M., et al., Application of membrane residue curve maps to batch and continuous processes. Industrial & Engineering Chemistry Research, 2008. 47(7): p. 2361-2376.

3 Review  Hybid configurations and case study  Batch Extractive Distillation as hybrid  Kotai, B., P. Lang, and G. Modla, Batch extractive distillation as a hybrid process: separation of minimum boiling azeotropes. Chemical Engineering Science, 2007. 62(23): p. 6816- 6826.  Batch Distillation with decantation  Skouras, S. and S. Skogestad, Separation of ternary heteroazeotropic mixtures in a closed multivessel batch distillation-decanter hybrid. Chemical Engineering and Processing, 2003. 43(3): p. 291-304.  Distillation with crystallization  Franke, M. B., et al. (2008). "Design and Optimization of a Hybrid Distillation/Melt Crystallization Process." Aiche Journal 54(11): 2925-2942.  Myasnikov, S. K., et al. (2009). "Hybrid separation processes combining vacuum distillation with fractional crystallization, partial melting, and granulation." Theoretical Foundations of Chemical Engineering 43(3): 227-237.

4 Review  Hybid configurations and case study  Batch Distillation with membrane, especially pervaporation  Gonzalez, B. and I. Ortiz (2002). "Modelling and simulation of a hybrid process (pervaporation-distillation) for the separation of azeotropic mixtures of alcohol- ether." Journal of Chemical Technology and Biotechnology 77(1): 29-42.  Other configurations to be searched  Process evaluation criteria and multi-objectives optimization of hybrid process, including economic accessment  Skouras, S. and S. Skogestad, Time requirements for heteroazeotropic distillation in batch columns. Computers & Chemical Engineering, 2004. 28(9): p. 1689-1700.

5 Modeling and Simulation  Tool: Matlab  精馏模型:动态累积循环全回流间歇精馏  吸附模型:平衡吸附模型  目前研究精馏模型的程序,现在程序还不 能在全回流和无回流阶段循环

6 Experiment  听王磊师兄说制定了初步的实验方案  但是实验设施和场地还没有,希望尽快把 实验室改造出来


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