1. Modular Sampling System Initiative CPAC: Nov 6, 2000 Modular Sampling System Initiative Modular Sampling System Initiative Background and Status 2000 Fall Sponsor Meeting Center for Process Analytical Chemistry

2. Modular Sampling System Initiative CPAC: Nov 6, 2000 Agenda Status and Update Status and Update Preview of Swagelok Proposal Preview of Swagelok Proposal

3. Modular Sampling System Initiative CPAC: Nov 6, 2000 CPAC as a Multi-Purpose PA Forum Legal Umbrella for Sponsors to Meet Legal Umbrella for Sponsors to Meet R&D: Long Range / Short Range Information Clearing House Enabling Mechanism to Address Other Common Needs Focus Groups: Forum to Focus Groups: Forum to Review R&D Programs Present Industry Common Needs - RFP Address Industry Common Needs Fieldbus Datalink Specification - Done NeSSI - In progress MatLab On-line/Connectivity - Future?

4. Modular Sampling System Initiative CPAC: Nov 6, 2000 Background and Chronology of NeSSI Activities O&P Focus Group May 1999 O&P Focus Group May 1999 Identified Sampling Systems as Common Area Of Interest Sponsored Tutorial for Nov99 Sponsor Meeting Tutorial Nov99 CPAC Meeting Tutorial Nov99 CPAC Meeting Background/Reasons for Interest Presentations by Suppliers/ End Users Participation in IFPAC2000 MeetingParticipation in IFPAC2000 Meeting Plenary/General Papers (SS Enjoyed High Profile) Workshop

5. Modular Sampling System Initiative CPAC: Nov 6, 2000 FLAN (Optical Fiber) Sensor/Signal Bus IA Control ler (ASIC) A T P F Sensor = Moisture Probe Sampling System Vision

6. Modular Sampling System Initiative CPAC: Nov 6, 2000 Process Analyzer Vision

7. Modular Sampling System Initiative CPAC: Nov 6, 2000 Background and Chronology of NeSSI Activities (cnt’d) Ad-hoc O&P Meeting @ Pittcon2000 Ad-hoc O&P Meeting @ Pittcon2000 End-users Discuss Initial Target Designs CPAC2000 Spring Meeting CPAC2000 Spring Meeting Formed SS Focus Group Defined Information Package (basis of RFP) Distributed RFP (July 2000)Distributed RFP (July 2000) Clarification Meeting at ISAEXPO2000 (40 attendees) Received Proposals from Swagelok, Parker Expect Additional Proposals/Comments from Autoflow, ABB Analytical, SAAI, Rosemount Analytical

8. Modular Sampling System Initiative CPAC: Nov 6, 2000 Background and Chronology of NeSSI Activities (cnt’d) CPAC2000 Fall Meeting CPAC2000 Fall Meeting Preview of Swagelok Proposal Other Feedback Micro-Reactor Proposal (MicroAnalytics) What is Next? What is Next? Distribute Proposals to All Interested Parties Follow-up by Report Sampling System Session at IFPAC2001 Review and Summary of NeSSI Effort Papers by Swagelok, Parker, Autoflow, ABB, Rosemount

9. Modular Sampling System Initiative CPAC: Nov 6, 2000 Acknowledgements DowRob Dubois/Ron O’Reily/ Brian Worthington Dow CorningJim Tatera/Gary Bokerman DuPont Bob Bucher Rohm&HaasJoe Sung Honeywell Ken Creasy Akzo Nobel Foad Mozayeni ExxonMobil Dan Podkulski/Rajko Puzic/ John Cumbus/Jeff Gunnell SwagelokDave Simko CPACLloyd Burgess/Larry Ricker

10. Modular Sampling System Initiative CPAC: Nov 6, 2000 The End

11. Modular Sampling System Initiative CPAC: Nov 6, 2000 O&P Focus Group Meeting May 99 Recognized Modular Sampling System Efforts in Semi Conductor Industry (Standard) Vendors like Autoflow, A+, Swagelok etc. promoted modular designs Recognized that current implementations of sample systems designs have not changed for many years CPAC has promoted Versatile Micro Analytical Systems (VMAS) as a basis for future micro-analytical techniques O&P decided to sponsor a SSISSS (Small Smart Integrated Sensor and Sampling System) Tutorial at CPAC Nov Meeting

12. Modular Sampling System Initiative CPAC: Nov 6, 2000 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

13. Modular Sampling System Initiative CPAC: Nov 6, 2000 Driving Forces for Change Reduce Cost of Ownership Non Recurring Costs = Cost to Build Operating Cost Data Validation (Fit for Use)

14. Modular Sampling System Initiative CPAC: Nov 6, 2000 A F T P AnalyzerController Field LAN Integration of Sample System and Sensors Sample Conditioning System Level 0 Level 1 Process Stream All System Components in Contact with Sample including the Sensors All Additional Electronic and Computing Components Required to Generate Analytical Result Mainly a Trust Configuration Now a Trust & Verify Configuration

15. Modular Sampling System Initiative CPAC: Nov 6, 2000 Integrated Sampling/Sensor System A F T P Level 0 Subsystem Integration Sample Conditioning System Level 0 Process Stream Purpose: Prepare and Verify a Representative Sample (Compatible with Analyzer Sensor) Opportunity: Packaging as an Integrated Sensor and Sampling System Size Cost Issues: Size Standardization VMAS

16. Modular Sampling System Initiative CPAC: Nov 6, 2000 A F T P AnalyzerController Field LAN Separation or Integration of Level 0/1 Subsystems Level 0 Level 1 Process Stream Integrated Sampling/Sensor System Objective: Close to Sample Tap Options: RemoteRemote Separate but CloseSeparate but Close IntegratedIntegrated

17. Modular Sampling System Initiative CPAC: Nov 6, 2000 Integrated Sampling/Sensor/Controller System A F T P AnalyzerController Field LAN Integration of Level 0/1 Subsystems Level 0 Level 1 Process Stream $$

18. Modular Sampling System Initiative CPAC: Nov 6, 2000 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) Micro Fluidics Sensors/Analyzers

19. Modular Sampling System Initiative CPAC: Nov 6, 2000 Nov99 CPAC SSISSS Tutorial (Vendor Presentations) Autoflow RosemountA+ Swagelok

20. Modular Sampling System Initiative CPAC: Nov 6, 2000 Nov99 CPAC SSISSS Tutorial ExxonMobil/DuPont Provided Introduction to Tutorial Validation of Sample System Performance Integration of Sensor with Sampling System Four Suppliers of Sampling/Analyzer Systems Participated in Tutorial: A+, Autoflow, Swagelok, Rosemount Many components commercially Available GCX example of self-contained miniaturized GC (GC on a pole) Recognition Modular Sampling System can be a platform to integrate VMAS Bridge between Process Sample (Macro world) and Micro Fluidics Sensors/Analyzers

21. Modular Sampling System Initiative CPAC: Nov 6, 2000 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design for SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

22. Modular Sampling System Initiative CPAC: Nov 6, 2000 TODAY’S COST OF BUILD For a major greenfield project

23. Modular Sampling System Initiative CPAC: Nov 6, 2000 TODAY’S COST OF OWNERSHIP

24. Modular Sampling System Initiative CPAC: Nov 6, 2000 IMAGINE THE FUTURE A T P AnalyzerController Field LAN Level 0 Level 1 Process Stream F

25. Modular Sampling System Initiative CPAC: Nov 6, 2000 IMAGINE THE FUTURE FLAN (Optical Fiber) Sensor/Signal Bus IA Controller (ASIC) & Interface Module Original Picture of Gas Delivery System courtesy Valin Corporation; A T P F Sensor = Moisture Probe

26. Modular Sampling System Initiative CPAC: Nov 6, 2000 IMAGINE THE FUTURE A T P F Sensor = RAMAN Probe Interface Module

27. Modular Sampling System Initiative CPAC: Nov 6, 2000 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

28. Modular Sampling System Initiative CPAC: Nov 6, 2000 IFPAC2000 ExxonMobil Presented Plenary Paper Promoting SSISSS Sample System Infrastructure accounts for 50+% Cost to Build Proposed Conceptual Design fro SSISSS Highlighted sensor and analyzer transmitter configurations Sampling System Session Presentations by A+, Autoflow, etc. Sampling Systems enjoyed a High Profile CPAC/ExxonMobil sponsored Workshop Confirmed high interest in Modular Sampling System Provided input for the ISA Standardization effort

29. Modular Sampling System Initiative CPAC: Nov 6, 2000 Pittcon2000 (New Orleans) O&P Ad-Hoc Meeting of Sponsor End-users DuPont, Dow, Dow-Corning, CPAC, Rohm&Haas, ExxonMobil Main Goal: Identify Typical Sample System Designs as Candidates for Modular Design Reviewed some typical gas/liquid sample System Designs Rob DuBois Presented a Modular Component/Service Matrix Discussed next steps Present Sample System Data at May CPAC Meeting Next Step is to Open Up Discussion (3 rd parties) Leverage ISA Meeting in New Orleans (Aug00) Role of CPAC in Facilitating Development/Testing of a Prototype System Larry Ricker/Lloyd Burgess to Present Proposal

30. Modular Sampling System Initiative CPAC: Nov 6, 2000Status CPAC Meeting May 1999Done O&P Identified Modular Sampling Systems CPAC Meeting Nov 1999Done O&P Sponsored Tutorial IFPAC2000 MeetingDone Plenary Presentation Promoted SSISS Session on Modular Sampling Systems CPAC Sponsored Workshop Pittcon2000Done Ad-hoc O&P Meeting Propose Candidate Sampling System Descriptions CPAC Meeting May 2000TBD

31. Modular Sampling System Initiative CPAC: Nov 6, 2000 What is Next? CPAC Meeting May 2000 (Sampling Focus Group – Wednesday) Review and Agree on Sample System Information Package Involvement of 3 rd parties How do we distribute package (Distribution List, Meeting?) Expectations for proposals from Suppliers (Paper designs?) Joint Effort with ISA (Meeting in Aug, New Orleans) Evaluation of Designs - Recommendation Prototype design/manufacturing/testing at CPAC Larry Ricker/Lloyd Burgess proposal Program to Evaluate Test Platforms fro Micro Analytical Devices CPAC Proposal – Lloyd Burgess