456 series Gas Chromatograph

456 series Gas Chromatograph
For Performance and Flexibility

456 Product Value Proposition Competitive Positioning Sales Tools
How to Order

436-GC – 2 Channel Architecture
2 Inert Inlets Up to 2 Detectors (1 MS): Full Color Touchscreen UI 14 languages! Fast Acquisition rates 600 HZ on all Detectors Smallest Footprint 32 CM Fastest Ramping Oven (up to 170°/min) Electronic Flow controls up to 3 modules, 9 channels. High pressure inlet Up to 150 psi Automation capabilities SPME, dual/duplicate, cool zone 1 Backflush option ATEX certified

456-GC – 3 Channel Architecture
3 Inert Inlets Up to 4 detectors (1 MS): Full Color Touchscreen UI 14 languages! Fast Acquisition rates 600 HZ Fastest Ramping Oven up to 150°/min 180°C with Column Oven Insert Electronic Flow controls Up to 9 modules, 21 channels. Inert Inlets High pressure inlet Up to 150 psi Automation capabilities SPME, dual/duplicate, cool zone Backflush options Versatile for analyzer builds ATEX certified

Inlet & Detector Portfolio Scope
Data Rate Sensitivity Linearity Flame Ionization Detector (FID) 600 Hz 1.4 pg/s (as n-C14) 107 Electron Capture Detector (ECD) 7 fg/s (as Lindane) 104 Thermal Conductivity Detector (TCD) 300 pg/mL (as n-C4) 106 Nitrogen-Phosphorous Detector (NPD or TSD) N: 100 fg N/sec (as Azobenzene) P: 100 fg P/sec (as Malathion) N: 105 P: 104 Pulsed Flame Photometric Detector (PFPD) 50 Hz S: 1 pg S/sec (S/P tube) P: 100 fg P/sec (S/P tube) N: 20 pg N/sec (S/P/N tube) S: 103 N: 102 Pulsed Discharge Helium Ionisation Detector (PDHID 50 ppb (Methane)

Packed Wide Bore Narrow bore
Inlet & Detector Portfolio Scope Inlet Septum Purge Temp. Progr. Pressure / Flow Range EFC Type Column Types Packed Wide Bore Narrow bore Split Splitless (S/SL) Yes Isothermal (450° max) up to 150 psi 500 mL/min N2/Ar 1500 mL/min He/H2 Split :1 21 25 Cold On column (COC) (-160/450°)* 50 mL/min 23 Yes** Programmable Temperature Vaporizer or Large Volume Inlet (PTV / LVI) Packed Wide bore on Column (PWOC) No (max 450°) 24 Flash Inlet (Flash) *With Liquid Nitrogen Cooling **0.32 mm column only in Narrow bore – smaller ID require precolumn/retention gap

User Interface Larger Multi-language Local Control
9”, Full Colour WVGA 800 x 480 Res. Multi-language 14 languages, adding one possible! Local Control Touch Screen + Hard Keys Remote access GC Portal software

Fastest Oven Ramp Rates up to 180°/min with 456 Column Oven Insert
Resolution <0.1°C , Ambient reject <0.01°C Cool Down 400° to 50° in <4.5 mins Easy Access Oven, Removable oven door! Temp Range Ramp Rate (°C/min) 50-70 170 70-115 105 80 55 35 Temp Range Ramp Rate (°C/min) 50-70 150 70-115 95 70 45 30 Temp Range Ramp Rate (°C/min) 50-70 180 70-115 115 90 65 45 436 Oven Heating Rates 456 Oven Heating Rates 456 Oven Heating Rates (insert)

8400/8410 Sampler 2 different user Profiles: All models
Large throughput  8400 Small volume, but best repeatability  8410 All models 2 ml vials only 8400 vs 3 different vial sizes (2,5,10 ml) in 8410 Better accuracy than manual Dual / Duplicate Capability Inject Into Two Ports Requires Only One Tower Control Through LUI Control via Work Station Side mounted Sampler. Syringe not over hot injection port SPME mode option

8400/8410 Sampler Flow Through Cell. On-line sampling of liquids
Always fresh sample available No time-consuming sample collection

8400/8410 Sampler SPME. Large Solvent vials Solvent drain/waste line
Integrated Part of method Available on 436/456 & 8400/8410 Large Solvent vials Extends capacity of solvent vials to 100 ml Solvent drain/waste line No more full vials…. And a safe accumulation of solvent

Inert Mini Splitter What is it: Applicable to: In-line Splitter
Vent outlet for back flush Low ithermal mass Low dead volume External heated (column oven) Less connections = robust Inert (UltiMetalTM) No polymers used (Septa, O-rings) Applicable to: Gas samples only SPT, PDHID based applications Sulfur in Gas samples

Comparing Mini Splitter & S/SL
Smaller Better Repeatability S/SL liquid injections Separate heating Different Liner designs Septum purge Metal column Carrier gas in Vent out Vent out Heating block Capillary column Capillary column

Safety Options H2 Sensor - Senses Hydrogen in oven (ATEX) Certified
Safety Shutdown when Hazardous error Hydrogen flows set to zero Other gas supply unchanged Detectors set to off (also for filaments!) Heated zones set to low (oven, injector, detector) (ATEX) Certified Personal safety on the lab No flying parts after an “explosion”

Electronic Flow Controls
EFC Resolution: psi for Superior Retention Time Stability Retention Time Repeatability n-C14 n-C15 n-C16 Average 6.0407 6.6858 7.3306 RSD (min) 0.0004 0.0003 0.0006 0.0061 0.0052 0.0079 Specification : RT RSD <0.008%, < min Area Repeatability n-C14 n-C15 n-C16 Average RSD %RSD 0.57 0.58 Specification : % Area RSD <1% Measured under standard conditions in split mode using CP-8400 autosampler. Different conditions and/or samples will affect the results.

Need for Fast? Reduce column ID from 0.25 to 0.1mm
Reduce column length from 15 to 4 mtr Increase column head pressure from 7 to 21 psi Increase oven ramp rate from 10 to 65 ºC/min Increase data rate from 25 to 200 Hz Not done here: hydrogen! Sample is typical diesel sample in both chromatograms, run on apolar column phase..

Platform Flexibility – 4X6 can offer it!
Different Levels of ‘Delivery’, depending on customer expectation (436 and 456 both) GC Solutions Pre-defined hardware Standard Analyzers Custom Solutions Standard GC hardware is modified for a specific application Eliminates the need to modify in the field by Scion Instruments or the customer Saves customer time Pre-configured and tested at the factory to conform with a specific “standard” method Includes method, column, reference/performance validation standard, checkout chromatogram, documentation specific to the method, installation GC systems that are configured and tested per specific customer requirements Configuration provided via custom factory modification Testing performed by factory in accordance with customers request provided via special testing specification

Multi-Stream Sampling
Platform Flexibility Solutions - Examples Process Valves Valves with Micro packed Columns Integrating Stream Conditioners Multi-Stream Sampling and Automation LSV with Sample Port

Platform Flexibility Solutions - Examples

Platform Flexibility Solutions - Examples
Pneumatic High Temp. / High Pressure On/Off valve in sample line Packed column(-s) installed in Multi-valve oven

436 – Value Proposition

Value Proposition 436 Confidence in Data
Proven Results (designed, built, tested, documented & commissioned to spec) Software for automation, calculus, reporting Electronic flow control Better ROI / Lower Cost of Ownership Robust Platform - Low maintenance due to superior build quality Fast cycle times Cost efficient Space efficient Flexibility for tailoring to your need! 2 channels with MS Solution Driven Options

456 – Value Proposition

Value Proposition 456 Confidence in Data
Proven Results (designed, built, tested, documented & commissioned to spec) Software for automation, calculus, reporting Electronic flow control Better ROI / Lower Cost of Ownership Robust Platform - Low maintenance due to superior build quality Fast cycle times Cost efficient Flexibility for tailoring to your need! 4 channels with MS Solution Driven Options

Competitive Positioning

Competitive Landscape
436 USP: Size Allows ‘all applications’ (2 channel – full suite inlets/detectors) PFPD! 9” WVGA Touch Screen w. GC Language Localization Fast oven (also works with narrow bore – Intuv’O’). 84X0 Liquid sampler with added capability (SPME…) Dual / Duplicate sampling Software: CompassCDS with Hydrocarbon Reporting Scalable, C/S, across brands.

456 USP: Unsurpassed configurability Allows ‘all applications’ 4 channel w. MS Full suite inlets/detectors PFPD 9 EFC Modules, 8+8 Electr. Events, 16 timed events, up to 9 heated zones 9” WVGA Touch Screen w. GC Language Localization Fastest oven with oven insert. 84X0 Liquid sampler with added capability (SPME…) Dual / Duplicate sampling Software: CompassCDS with Hydrocarbon Reporting Scalable, C/S, across brands.

50 fg as perchloroethylene
Competitive Brands side by side Scion 436 456 Agilent 8890 Shimadzu Nexus Perkin Elmer Clarus 681 Thermo 13X0 Max. Oven Rate 170°/min 180°/min* 120°/min 230V* 75°/min 120V 40°/min (std oven) 120°/min (HP oven) 140°/min 230V 80°/min 120V 125°/min 230V* 90°/min 120V Colum T Range -100° / 450° CO2 / N2 -80° / 450° -50° / 450° CO2 only -99° / 450° Column Cooldown 400°50° 4.5 min 450°50° 4.0 min 3.4 min 2.0 min 4 min Detector Sensitivity FID 1.4 pg/s 1.2 pg/s 3 pg/s (S/N = 2 to 1 ) ECD 7 fg/s <3.8 fg/s 4.0fg/s 50 fg as perchloroethylene 4.5 fg/s TCD 300 pg/mL 400 pg/ml n/s 9 µV/ppm nonane NPD N: 100 fg N/s P: 100 fg P/s N: 80 fg N/s P: 10 fg P/s N: 500 fg N/s P: 50 fg P/s P: 20 fg P/s (P)FPD S: 1 pg S/s N: 20 pg N/s <2.5 pg S/s <45 fg P/s S:2pgS/s 45fgP/s 10 pg S/s 1000 fg P/s 5 pg S/s 100 fg P/s PDHID 50 ppb n/a SCD 0.3 pg/s 0.5 pg/s NCD Acq. rate 600 Hz (select detectors) 1000 Hz 500 Hz 300 Hz *with oven insert

Competitive Brands side by side
Scion 436 456 Agilent 8890 Shimadzu Nexis Perkin Elmer Clarus Thermo 13X0 Inlets S/SL Max T 450° 400° 450 %RSD <1%** <0.5%*** 1% n/s <0.5% (‘typical’) EFC # modules/channels 9 / 21 8 / 19 8/12 8/18 Accuracy RT <0.008%, <0.008 min <0.008%, < min < min Flow Accuracy 2% FS 5% 5% FS Flow Repeatability 0.5% 0.35% SP Pressure Accuracy 0.1%FS Press. Repeatability 0.05% 0.34% Press. Range (S/SL) Up to 150 psi Up to 100 psi Up t 145 psi Max Split Ratio : 1 7.500 : 1 : 1 : 1 User Interface 9” WVGA 7” Multi Language Yes (14) ? Yes (8) No **measured in split mode ***measured in splitless mode

Agilent - Intuvo: Guard Chip Works best for dirty samples, no need for other applications Leak prone…depends on user skill 1 channel only Fast Heating option commonly not used (Temp transfer…) No Wide bore columns only, max col length 50m So not compliant to many solutions! Not many valve options Intuvo pricing. Sometimes allows competing with 2*436 (productivity, Throughput) Intuvo Consumable pricing

Shimadzu - Nexis: Low-Quality Plastic Covers… User Interface is user unfriendly. ‘Non’-features: ClickTek Nut – ‘no tools’, special jig? Max Temperature 350°C, no COC! Oven Light – Varians 3800 had that in 1998, and it was deemed unneeded….

Shimadzu - Nexis: Flow Control… FID linearity… known problem in GC-2010 ≠ 107 FID-2030

Sales Tools

Sales Tools PPT 436 / 456 Product Brochure
Customer Value How to order Competitive Product Brochure App Notes, Posters, Demonstrated Analysis

How to Order - 436

How to Order – Standard Preconfigured
P/N DESCRIPTION 436-GC, S/SL-EFC 21, FID-DEFC 11, 120V 436-GC, S/SL-EFC 21, FID-DEFC 11, 230V 436-GC, PWOC-EFC 24, FID-DEFC 11, 120V 436-GC, PWOC-EFC 24, FID-DEFC 11, 230V 436-GC, PWOC-EFC 24, TCD-DEFC 14, 120V 436-GC, PWOC-EFC 24, TCD-DEFC 14, 230V 436-GC, S/SL- EFC 21, TCD-DEFC 14, 120V, 436-GC, S/SL- EFC 25, TCD-DEFC 14, 120V, 436-GC, S/SL- EFC 21, TCD-DEFC 14, 230V, 436-GC, S/SL- EFC 25, TCD-DEFC 14, 230V, 436-GC, S/SL-EFC 25, FID-DEFC 11, 120V / for P&T Devices. 436-GC, S/SL-EFC 25, FID-DEFC 11, 230V / for P&T Devices.

How to Order – Base Platform
P/N DESCRIPTION 436-GC Gas Chromatograph, 120V 436-GC Gas Chromatograph, 230V

How to Order – S/SL Inlets
P/N DESCRIPTION S/SL, Type 21 EFC, SST, 120V S/SL, Type 21 EFC, SST, 230V INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. S/SL, Type 25 EFC, SST, 120V S/SL, Type 25 EFC, SST, 230V Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Super Inert Upgrade for S/SL Injectors Recommended for applications requiring the ultimate in inert surfaces such as low level sulfur analysis. NOTE: Order one upgrade for each injector. On the sales quote and sales order, the inert upgrade part number should immediately follow the injector requiring the inert upgrade. CP742826 45x-GC Injector EFC Power Fail Option, Field Installed Power fail protection of your GC capillary column and MS system. Upon power failure the solenoid closes septum purge line and supplies supplemental helium flow through the column to vent MS.

How to Order – PTV Inlets
P/N DESCRIPTION PTV, Type 21 EFC, SST, LCO2, 120V PTV, Type 21 EFC, SST, LCO2, 230V PTV, Type 21 EFC, SST, LN2, 120V PTV, Type 21 EFC, SST, LN2, 230V PTV, Type 21 EFC, SST, Air, 120V PTV, Type 21 EFC, SST, Air, 230V PTV, Type 25 EFC, SST, LCO2, 120V PTV, Type 25 EFC, SST, LCO2, 230V PTV, Type 25 EFC, SST, LN2, 120V PTV, Type 25 EFC, SST, LN2, 230V PTV, Type 25 EFC, SST, Air, 120V PTV, Type 25 EFC, SST, Air, 230V Super Inert Upgrade for PTV Injectors Recommended for applications requiring the ultimate in inert surfaces such as low level sulfur analysis. NOTE: Order one upgrade for each injector. On the sales quote and sales order, the inert upgrade part number should immediately follow the injector requiring the inert upgrade. CP742826 45x-GC Injector EFC Power Fail Option, Field Installed Power fail protection of your GC capillary column and MS system. Upon power failure the solenoid closes septum purge line and supplies supplemental helium flow through the column to vent MS. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

How to Order – PWOC / Flash Inlets
P/N DESCRIPTION PWOC, Type 23 EFC, SST, 120V PWOC, Type 23 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. INCLUDES: Programmable flow control (0-50 mL/min), electronic head pressure readout (0-150 psi). PWOC, Type 24 EFC, SST, 120V PWOC, Type 24 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. Type 24 EFC is optimized for Purge & Trap systems, headspace sampling, and valved GC systems. INCLUDES: Programmable head pressure control (0.1 to 150 psi), programmable vent control, and electronic head pressure readout (0-150 psi). Flash, Type 23 EFC, SST, 120V Flash, Type 23 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. Includes: Programmable flow control (0-50 mL/min), electronic head pressure readout (0-150 psi), and glass insert. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

How to Order – COC Inlets
P/N DESCRIPTION COC, EFC Type 23, LN2, 120V COC, EFC Type 23, LN2, 230V COC, EFC Type 23, LCO2, 120V COC, EFC Type 23, LCO2, 230V COC, EFC Type 23, Air cooled, 120V COC, EFC Type 23, Air cooled, 230V This Injector is typically used for simulated distillation and biodiesel (glycerides) analysis. It is generally the best Injector to offer the customer who wants to minimize or eliminate the possibility of sample discrimination typically associated with vaporizing Injectors. The injector can be ramp heated and cooled with either Air, LCO2 or LN2. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

How to Order – Detector Options
P/N DESCRIPTION FID with Electrometer, DEFC Type 11, 120V FID with Electrometer, DEFC Type 11, 230V FID with Electrometer, DEFC Type 11, 120V HIGH TEMPERATURE VERSION FID with Electrometer, DEFC Type 11, 230V HIGH TEMPERATURE VERSION NPD with Electrometer, DEFC Type 12, 120V NPD with Electrometer, DEFC Type 12, 230V ECD with Electrometer, DEFC Type 13, Specific License, 120V ECD with Electrometer, DEFC Type 13, Specific License, 230V NT ECD kit; no tower. (Macao only!) PFPD with Electrometer, S and P Modes, DEFC Type 15, 120V PFPD with Electrometer, S and P Modes, DEFC Type 15, 230V PFPD with Electrometer, N, S, and P Modes, DEFC Type 15, 120V PFPD with Electrometer, N, S, and P Modes, DEFC Type 15, 230V TCD with 2 Channel DEFC Type 14 (non-H2), 120V TCD with 2 Channel DEFC Type 14 (non-H2), 230V TCD with 2 Channel DEFC Type 16 (H2 version), 120V TCD with 2 Channel DEFC Type 16 (H2 version), 230V CP740022 Upgrade of single TCD detector to nickel filaments, nickel block and monel fittings. For Chlorine applications only. (Must order TCD separately).

How to Order - Options P/N DESCRIPTION 4360000010
Column Oven Cryogenics for 436-GC, LCO2, Factory Installed Cools column oven to -60°C. Requires LCO2 cylinder with educator (dip) tube at psig ( bar). Column Oven Cryogenics for 436-GC, LN2, Factory Installed Cools column oven to -160°C. Requires LN2 cylinder at psig ( bar). CP742562 Vertical exhaust for 436-GC. Outside vent diameter 10.0 cm The exhaust creates a mounting point at the column oven outlet for removal of excess heat generated by the GC.

436-GC Injector EFC Power Fail Option, Factory Installed Septum Purge Flow Controller Option, Factory Installed For PTV & S/SL Injectors. Very useful if both regular and pulsed-pressure injections are made. Eliminates the need to re-measure and re-enter septum purge flow measurement when injector pressure is changed. Packed Column Adapter Kit, ¼” Universal Glass Columns, PWOC Injector Packed Column Adapter Kit, ¼” Single Piece Glass column and ¼” Metal Columns, PWOC/Flash Injector Packed Column Adapter Kit, 1/8” Metal Columns, PWOC Injector Packed Column Adapter Kit, 1/8” Metal Columns, Flash Injector

Back Flush Option for 436/456-GC w/ Valco Inert Steel T-union For additional pressure control between two columns. Factory installed. Includes Type 24 EFC (0-150 psi) and Valco T-union Inert Steel fittings. SilFlow Back Flush Option for 436/456-GC w/ SilTite FingerTite Fittings For additional pressure control between two columns. Factory installed. Includes Type 24 EFC (0-150 psi) and SilFlow GC 3-port microchannel device splitter (port A: 1.1mm OD; ports B & C: 0.25/0.32mm ID). Also includes SilTite™ FingerTite fittings that are easy to set up and can be tightened using finger force to achieve a perfect, reliable seal. 550021 Electronic Flow Control, Type EFC 21 (0-150psi) For S/SL and PTV injectors. Factory installed 550023 Electronic Flow Control, Type EFC 23 (0-150psi) For PWOC and Flash injectors. Factory installed. 550024 Electronic Flow Control, Type EFC 24 (0-150psi) For PWOC and Flash injectors with purge & trap, headspace, or valved systems. Factory installed. 550025 Electronic Flow Control, Type EFC 25 (0-150psi) For S/SL and PTV injectors with purge & trap, headspace, or valved systems. Factory installed.

How to Order - 456

How to Order – Base Platform
P/N DESCRIPTION 456-GC Gas Chromatograph, 120V 456-GC Gas Chromatograph, 230V

How to Order – S/SL Inlets
P/N DESCRIPTION S/SL, Type 21 EFC, SST, 120V S/SL, Type 21 EFC, SST, 230V INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. S/SL, Type 25 EFC, SST, 120V S/SL, Type 25 EFC, SST, 230V Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Super Inert Upgrade for S/SL Injectors Recommended for applications requiring the ultimate in inert surfaces such as low level sulfur analysis. NOTE: Order one upgrade for each injector. On the sales quote and sales order, the inert upgrade part number should immediately follow the injector requiring the inert upgrade. CP742826 45x-GC Injector EFC Power Fail Option, Field Installed Power fail protection of your GC capillary column and MS system. Upon power failure the solenoid closes septum purge line and supplies supplemental helium flow through the column to vent MS.

How to Order – PTV Inlets
P/N DESCRIPTION PTV, Type 21 EFC, SST, LCO2, 120V PTV, Type 21 EFC, SST, LCO2, 230V PTV, Type 21 EFC, SST, LN2, 120V PTV, Type 21 EFC, SST, LN2, 230V PTV, Type 21 EFC, SST, Air, 120V PTV, Type 21 EFC, SST, Air, 230V PTV, Type 25 EFC, SST, LCO2, 120V PTV, Type 25 EFC, SST, LCO2, 230V PTV, Type 25 EFC, SST, LN2, 120V PTV, Type 25 EFC, SST, LN2, 230V PTV, Type 25 EFC, SST, Air, 120V PTV, Type 25 EFC, SST, Air, 230V Super Inert Upgrade for PTV Injectors Recommended for applications requiring the ultimate in inert surfaces such as low level sulfur analysis. NOTE: Order one upgrade for each injector. On the sales quote and sales order, the inert upgrade part number should immediately follow the injector requiring the inert upgrade. CP742826 45x-GC Injector EFC Power Fail Option, Field Installed Power fail protection of your GC capillary column and MS system. Upon power failure the solenoid closes septum purge line and supplies supplemental helium flow through the column to vent MS. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

How to Order – PWOC / Flash Inlets
P/N DESCRIPTION PWOC, Type 23 EFC, SST, 120V PWOC, Type 23 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. INCLUDES: Programmable flow control (0-50 mL/min), electronic head pressure readout (0-150 psi). PWOC, Type 24 EFC, SST, 120V PWOC, Type 24 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. Type 24 EFC is optimized for Purge & Trap systems, headspace sampling, and valved GC systems. INCLUDES: Programmable head pressure control (0.1 to 150 psi), programmable vent control, and electronic head pressure readout (0-150 psi). Flash, Type 23 EFC, SST, 120V Flash, Type 23 EFC, SST, 230V Injector can also be used with packed columns using one of the packed column adapter kits. Includes: Programmable flow control (0-50 mL/min), electronic head pressure readout (0-150 psi), and glass insert. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

How to Order – COC Inlets
P/N DESCRIPTION COC, EFC Type 23, LN2, 120V COC, EFC Type 23, LN2, 230V COC, EFC Type 23, LCO2, 120V COC, EFC Type 23, LCO2, 230V COC, EFC Type 23, Air cooled, 120V COC, EFC Type 23, Air cooled, 230V This Injector is typically used for simulated distillation and biodiesel (glycerides) analysis. It is generally the best Injector to offer the customer who wants to minimize or eliminate the possibility of sample discrimination typically associated with vaporizing Injectors. The injector can be ramp heated and cooled with either Air, LCO2 or LN2. The PTV injector is a Programmable Temperature Vaporizing (PTV) Injector. Active cooling with either Air, LCO2 or LN2 is standard. Select injector with appropriate part number. This injector is sometimes referred to as LVI (large volume injector) Type 21: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC. Type 25 EFC is optimized for Purge & Trap systems, static headspace sampling. For headspace syringe injection (PAL Combi-xt) use type 21 EFC . INCLUDES: Programmable head pressure control (0.1 to 150 psi) or constant electronic flow control ( mL/min), programmable split ratio control (1 to 10,000), adjustable septum purge, pressure pulse injection mode ( psi) and gas saver mode. For 100 to 1000 µm diameter fused silica columns, 1 to 250 m. length. Maximum temperature limit 450ºC.

P/N DESCRIPTION FID with Electrometer, DEFC Type 11, 120V FID with Electrometer, DEFC Type 11, 230V FID with Electrometer, DEFC Type 11, 120V HIGH TEMPERATURE VERSION FID with Electrometer, DEFC Type 11, 230V HIGH TEMPERATURE VERSION NPD with Electrometer, DEFC Type 12, 120V NPD with Electrometer, DEFC Type 12, 230V ECD with Electrometer, DEFC Type 13, Specific License, 120V ECD with Electrometer, DEFC Type 13, Exempt License, 120V ECD with Electrometer, DEFC Type 13, Specific License, 230V NT ECD kit; no tower. (Macao only!) PFPD with Electrometer, S and P Modes, DEFC Type 15, 120V PFPD with Electrometer, S and P Modes, DEFC Type 15, 230V PFPD with Electrometer, N, S, and P Modes, DEFC Type 15, 120V PFPD with Electrometer, N, S, and P Modes, DEFC Type 15, 230V

P/N DESCRIPTION TCD with 2 Channel DEFC Type 14 (non-H2), 120V Includes electrometer. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) make-up gas. TCD with 2 Channel DEFC Type 14 (non-H2), 230V Includes electrometer. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) make-up gas. TCD with 2 Channel DEFC Type 16 (H2 version), 120V Includes electrometer. Detector EFC is optimized for Hydrogen make-up gas. TCD with 2 Channel DEFC Type 16 (H2 version), 230V Includes electrometer. Detector EFC is optimized for Hydrogen make-up gas. TCD with Transfer line, 2 Channel DEFC Type 14 (non-H2), 120V Includes electrometer. Transfer line allows effluent to be directed into a second detector. Detector EFC is optimized for non-hydrogen (helium, nitrogen, argon, etc.) make-up gas. TCD with Transfer line, 2 Channel DEFC Type 14 (non-H2), 230V Includes electrometer. Transfer line allows effluent to be directed into a second detector. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) make-up gas. TCD with Transfer line, 2 Channel DEFC Type 16 (H2 version), 120V Includes electrometer. Transfer line allows effluent to be directed into a second detector. Detector EFC is optimized for Hydrogen make-up gas. TCD with Transfer line, 2 Channel DEFC Type 16 (H2 version), 230V Includes electrometer. Transfer line allows effluent to be directed into a second detector. Detector EFC is optimized for Hydrogen make-up gas.

P/N DESCRIPTION Dual Independent TCDs with 4 Channel DEFC (non-H2), 120V Includes 2 electrometers. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) make-up gas. Dual Independent TCDs with 4 Channel DEFC (non-H2), 230V Includes 2 electrometers. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) make-up gas. Dual Independent TCDs with 4 Channel-DEFC 14 (non-H2), including transfer line, 120V. Includes 2 electrometers and one transfer line. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) Including make-up and reference gas for capillary column applications Dual Independent TCDs with 4 Channel-DEFC 14 (non-H2), including transfer line, 230V. Includes 2 electrometers and one transfer line. Detector EFC is optimized for non-Hydrogen (Helium, Nitrogen, Argon, etc.) Including make-up and reference gas for capillary column applications Dual Independent TCDs with 4 Channel DEFC (H2 version), 120V Includes 2 electrometers. DEFC is optimized for Hydrogen make-up gas. Includes reference gas & make-up gas adapter. Dual Independent TCDs with 4 Channel DEFC (H2 version), 230V Includes 2 electrometers. DEFC is optimized for Hydrogen make-up gas. Includes reference gas & make-up gas adapter. Dual Independent TCDs with 4 Channel-DEFC 16 (H2 version), Including transfer line, 120V. Includes 2 electrometers and one transfer line. DEFC is optimized for Hydrogen make-up gas. Includes reference gas & make-up gas adapter. Dual Independent TCDs with 4 Channel-DEFC 16 (H2 version), including transfer line, 230V. Includes 2 electrometers and one transfer line. DEFC is optimized for Hydrogen make-up gas. Includes reference gas & make-up gas adapter. CP740022 Upgrade of single TCD detector to nickel filaments, nickel block and monel fittings. For Chlorine applications only. (Must order TCD separately).

Column Oven Cryogenics for 450-GC/456-GC, LCO2, Factory Installed Cools column oven to -65°C. Requires LCO2 cylinder with educator (dip) tube at psig ( bar). Column Oven Cryogenics for 450-GC/456-GC, LN2, Factory Installed Cools column oven to -160°C. Requires LN2 cylinder at psig ( bar). Column Oven Vent Deflector Kit for 456-GC Directs column oven heat during cool down when the rear of 456-GC is placed within 6” (15 cm) of wall. CP742562 Vertical exhaust for 456-GC. Outside vent diameter 10.0 cm. The exhaust creates a mounting point at the column oven outlet for removal of excess heat generated by the GC. CP741100 450-GC/456-GC Oven "Reducer" Used to reduce the volume of the oven to improve both heat up and cool down rates; typically used for application requiring fast oven heating rates (e.g. Fast Temperature Simulated Distillation). Note: Front channel can not be configured with injector or detector.

436-GC Injector EFC Power Fail Option, Factory Installed Septum Purge Flow Controller Option, Factory Installed For PTV & S/SL Injectors. Very useful if both regular and pulsed-pressure injections are made. Eliminates the need to re-measure and re-enter septum purge flow measurement when injector pressure is changed. Packed Column Adapter Kit, ¼” Universal Glass Columns, PWOC Injector Packed Column Adapter Kit, ¼” Single Piece Glass column and ¼” Metal Columns, PWOC/Flash Injector Packed Column Adapter Kit, 1/8” Metal Columns, PWOC Injector Packed Column Adapter Kit, 1/8” Metal Columns, Flash Injector

Back Flush Option for 436/456-GC w/ Valco Inert Steel T-union For additional pressure control between two columns. Factory installed. Includes Type 24 EFC (0-150 psi) and Valco T-union Inert Steel fittings. SilFlow Back Flush Option for 436/456-GC w/ SilTite FingerTite Fittings For additional pressure control between two columns. Factory installed. Includes Type 24 EFC (0-150 psi) and SilFlow GC 3-port microchannel device splitter (port A: 1.1mm OD; ports B & C: 0.25/0.32mm ID). Also includes SilTite™ FingerTite fittings that are easy to set up and can be tightened using finger force to achieve a perfect, reliable seal. 550021 Electronic Flow Control, Type EFC 21 (0-150psi) For S/SL and PTV injectors. Factory installed 550023 Electronic Flow Control, Type EFC 23 (0-150psi) For PWOC and Flash injectors. Factory installed. 550024 Electronic Flow Control, Type EFC 24 (0-150psi) For PWOC and Flash injectors with purge & trap, headspace, or valved systems. Factory installed. 550025 Electronic Flow Control, Type EFC 25 (0-150psi) For S/SL and PTV injectors with purge & trap, headspace, or valved systems. Factory installed.

Thank you

Pre-Install Requirements
Carrier gas Helium , > %, with Moisture and Oxygen filter Supply pressure 80 psi (5.3 bar) Detector gases FID Hydrogen (>99.999%, 40 psi / 2.6 bar) Air (moisture & oil free, 60 psi / 4 bar) Helium (>99.999%, 80 psi / 5.3 bar). TCD Helium (>99.999%, 80 psi / 5.3 bar) Charcoal filters for Helium, Hydrogen and Air are required.

Pre-Install requirements
Compressed Air (Valves) Minimum supply pressure 60 psi / 4 bar Connections 1/8” Swagelok. Gas Filters P/N Description #Required BRB1024B8 Filter kit for TCD incl. 2 filters (1/8” tube) 1 BRB1040S8 Filter kit for FID incl. 4 filters (1/8” tube) BRB0010B8 Connecting unit for 1 filter (1/8” tube) BRF0103 Hydrocarbon filter

456 series Gas Chromatograph

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