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Published byAngèle Bessette Modified over 5 years ago
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Spinning Star: a precession method for electron diffraction installed on the Philips CM20 TEM
Increase the number of visible reflections more information "correct" for slight misalignement on zone axis nicer patterns! provides intensities closer to the kinematical ones interpretation of intensities: Debye-Waller factors, structure factors and crystal structure determination new routine in JEMS for precession (Thanks to Pierre!) reveals some components of the true symmetry hidden by dynamical effects phase identification, crystal structure determination
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precession tilt out of zone axis Ewald sphere reciprocal lattice
kinematic (002) absent precession tilt out of zone axis dynamic 65nm (002) present (002) very weak precession 4° Ewald sphere reciprocal lattice
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precession tilt out of zone axis Ewald sphere reciprocal lattice
kinematic (002) absent precession tilt out of zone axis dynamic 65nm (002) present (002) very weak precession 4° Ewald sphere reciprocal lattice
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centering the pattern on zone axis and enhancing the spots visibility in thick crystals
by courtesy of Micromegas
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revealing (part of) the true symmetry
by courtesy of Micromegas
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