Presentation is loading. Please wait.

Presentation is loading. Please wait.

Headspace-GC/MS detection of TATP traces in post-explosion debris

Published byBrianne Jacobs Modified over 6 years ago

Similar presentations

Presentation on theme: "Headspace-GC/MS detection of TATP traces in post-explosion debris"— Presentation transcript:

1 Headspace-GC/MS detection of TATP traces in post-explosion debris
A. Stambouli, A. El Bouri, T. Bouayoun, M.A. Bellimam  Forensic Science International  Volume 146, Pages S191-S194 (December 2004) DOI: /j.forsciint Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

2 Fig. 1 GC/MS profile obtained from the injection of 1000μl of headspace explosion debris conditioned at 90°C, 30min (Tinj=270°C; Ttransferline=280°C; Tsource=180°C; Toven=40°C (2min), 5°C/min; 100°C (6min). Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

3 Fig. 2 Mass spectrum of triperoxide triacetone TATP I and diperoxide diacetone DADP II. Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

4 Fig. 3 HS-GC/MS chromatogram thermal decomposition of TATP; Tinj=270°C. Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

5 Fig. 4 HS-GC/MS chromatogram thermal decomposition of TATP avoided.
Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

6 Fig. 5 Results of optimization of the heating zones temperature.
Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

7 Fig. 6 Limit of the TATP detection (.1ng).
Forensic Science International  , S191-S194DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Download ppt "Headspace-GC/MS detection of TATP traces in post-explosion debris"

Similar presentations

The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:

The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:
The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,

The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,
DNA profiling of trace DNA recovered from bedding

DNA profiling of trace DNA recovered from bedding
Right heart ischemia in cases of sepsis

Right heart ischemia in cases of sepsis
Analysis of the headspace composition of smokeless powders using GC–MS, GC-μECD and ion mobility spectrometry  Monica Joshi, Kia Rigsby, Jose R. Almirall 

Analysis of the headspace composition of smokeless powders using GC–MS, GC-μECD and ion mobility spectrometry  Monica Joshi, Kia Rigsby, Jose R. Almirall 
Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,

Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,
Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.

Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.
The ideal subject distance for passport pictures

The ideal subject distance for passport pictures
Volatile organic compounds in polyethylene bags⿿A forensic perspective

Volatile organic compounds in polyethylene bags⿿A forensic perspective
Two fatal intoxication cases with imidacloprid: LC/MS analysis

Two fatal intoxication cases with imidacloprid: LC/MS analysis
Could NF-κB and caspase-3 be markers for estimation of post-interval of human traumatic brain injury?  Luyang Tao, Xiping Chen, Zhenghong Qin, Shizhong.

Could NF-κB and caspase-3 be markers for estimation of post-interval of human traumatic brain injury?  Luyang Tao, Xiping Chen, Zhenghong Qin, Shizhong.
The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.

The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.
Detecting and collecting traces of semen and blood from outdoor crime scenes using crime scene dogs and presumptive tests  A.G. Skalleberg, M.M. Bouzga 

Detecting and collecting traces of semen and blood from outdoor crime scenes using crime scene dogs and presumptive tests  A.G. Skalleberg, M.M. Bouzga 
Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 

Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.

Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.
Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS  Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.

Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS  Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.
Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N.

Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N.
Effective injection in pulsed splitless mode for impurity profiling of methamphetamine crystal by GC or GC/MS  Tetsuro Sasaki, Yukiko Makino  Forensic.

Effective injection in pulsed splitless mode for impurity profiling of methamphetamine crystal by GC or GC/MS  Tetsuro Sasaki, Yukiko Makino  Forensic.

Similar presentations

Ads by Google