1. PHILADELPHIA UNIVERSITY Faculty of Pharmacy
Medicinal chemistry lab.

2. Assessment Instruments
Allocation of Marks
Mark
Assessment Instruments 20
Quizzes 30
Reports and evaluation 10
Practical exam 40
Final examination
100
Total

3. Measuring saponification value of Castor oil 3 19-20/7
Lab.
No.
Suggested date
Experiment title
Notes 1
12-13/7
Introduction 2
17-18/7
Measuring saponification value of Castor oil 3
19-20/7
The identification and the assay of Ammonium Chloride Q 4
24-25/7
Assay test of Povidone Iodine solution 5
26-27/7
Assay test of Ibuprofen tablets 6
31/7-1-8
Assay test of Rifampicin capsules
First exams 31/7-1-3/7 7
2-3/8
Synthesis and purification of Acetaminophen 8
7-8/8
Synthesis and purification of Benzociane 9
9-10/8
Practical lab exam 10
14-15/8
Synthesis & purification of Aspirin
Second exams
14-17/8 11
16-17/8
Analysis of Aspirin 12
21-22/8
Lab Final exams

6. You must wear your lab coat and safety glasses all the time.
LAB SAFETY RULES
You must wear your lab coat and safety glasses all the time.

7. LAB SAFETY RULES
Identify the safety equipment’s and know how to use them (fire extinguisher, eye wash, shower, and the fire exit).

9. Never eat or drink inside the lab.
LAB SAFETY RULES
Never eat or drink inside the lab.
Do not pipette by mouth, use the bulb
Keep your belongings and bags away from the work area especially from flame.

10. LAB SAFETY RULES Follow the procedure as described to you.
You must read the chemical safety information for each chemical reagent you are using.
Do not taste or sniff chemicals.
Do not dispose chemicals down the sink.
Toxic and volatile chemicals should be handled inside the fume cupboard all the time.

12. LAB SAFETY RULES

13. COMMON LABORATORY GLASSWARE

14. Titration technique

15. End point & equivalence point