2. ID11 beamline Multipurpose beamline for diffraction experiments
Physical, chemical and mechanical properties of materials
Diffraction + imaging
Optics hutch
Moderate to high energy / 18 – 140keV
(U22, CPM18, double bent crystal monochromator)
Focusing by in vacuum transfocator
Secondary optics hutch - KB mirrors
l ID11 l l Pavel Sedmak

3. ID11 beamline Two experimental hutches
EH1: powder diffraction, single crystals, PDF
Heavy load sample environments
Fast Frelon 2D detector
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4. ID11 beamline Two experimenteal hutches EH3: 3D XRD, DCT, Nanoscope
Frelon21 or Frelon4M
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5. Experiments Polycrystalline materials, single crystals, glasses
Sample environment - ADMET stress rig (5kN), ETMT stress rig
furnace, gas blower, cryostream …
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6. Experiments 3D XRD microscopy Data collection using 2D detectors
3D XRD experiments – transmission geometry
rotation around ω axis
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7. Experiments 3D XRD microscopy Data collection using 2D detectors
3D XRD experiments – transmission geometry
rotation around ω axis
Data analysis using ImageD11 software (ID11 & DTU)
Grainmap containing 1000s of grains
For each grain:
Centre of mass position
Size
Orientation
Averaged strain  stress
l ID11 l l Pavel Sedmak

8. Experiments Nanoscope Beamsize down to 250x300um
Small grained samples, highly defective
Similar experiments – 3dxrd, single crystals …
Diffraction tomography – scanning across the sample + rotation
Data analysis using ImageD11 software – adapted for diffraction tomography
Grainmaps
l ID11 l l Pavel Sedmak

9. Experiments DCT Data collection using 2D WB detector
(field of view depends on optics)
DCT experiments – transmission geometry
rotation around ω axis
Data analysis using Matlab software (ID11)
l ID11 l l Pavel Sedmak

10. pyFAI What do we use it for? Calibration of sample-detector distance
Averaging and Integration of the powder diffraction data
Future: part of the data analysis
Pole figures
l ID11 l l Pavel Sedmak