Fig. 3 1D NMR. 1D NMR. Time-domain (left) and frequency-domain (right) NV NMR signals for (A) water, (B) trimethyl phosphate (TMP), and (C) 1,4-difluorobenzene.

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Fig. 3 1D NMR. 1D NMR. Time-domain (left) and frequency-domain (right) NV NMR signals for (A) water, (B) trimethyl phosphate (TMP), and (C) 1,4-difluorobenzene (DFB). Signals were averaged over ∼103 traces for a total acquisition of ∼1 hour. A ∼1-kHz-bandwidth bandpass filter is applied to the time-domain data for better visualization. The frequency-domain spectra show the imaginary component of the Fourier transform. Each spectrum is fit with Gaussian functions (black lines). For TMP, we constrain the widths of both lines to be equal with a 1:1 amplitude ratio and find JHP = 11.04 ± 0.06 Hz. For DFB, we constrain the widths of all three lines to be equal with a 1:2:1 amplitude ratio and find JHF¯=6.09±0.05 Hz. Janis Smits et al. Sci Adv 2019;5:eaaw7895 Copyright © 2019 The Authors, some rights reserved; exclusive licensee American Association for the Advancement of Science. No claim to original U.S. Government Works. Distributed under a Creative Commons Attribution License 4.0 (CC BY).