Microwave Spectrometer

Slides:



Advertisements
Similar presentations
Femtosecond lasers István Robel
Advertisements

I.R. Spectroscopy C.I. 6.4.
Raman Spectroscopy A) Introduction IR Raman
The Search is Over: Design and Applications of a Chirped Pulse Fourier Transform Microwave (CP- FTMW) Spectrometer for Ground State Rotational Spectroscopy.
Structural Information
1 Chapter Contents 1. Basics of Optical Spectrum Analysers 2. Fabry-Perot Interferometers 3. Interferometers-based Optical Spectrum Analysers 4. Diffraction.
Atomic Absorption Spectroscopy (AAS)
Physics for Scientists and Engineers, 6e Chapter 43 - Molecules and Solids.
Photons of Light The smallest unit of light is a photon A photon is often called a particle of light The Energy of an individual photon depends on its.
Infrared Spectroscopy Antonella Magnelli. Development Discovered in 1800 but commercially available in 1940s Prisms Grating Instruments Fourier-transform.
Microwave Spectroscopy I
Lecture 5 An Introduction to Spectroscopy Electromagnetic radiation, electromagnetic wave Emission, absorption, fluorescence.
Building a FT-FIR Towards a THz version of the Flygare R. Braakman 1,*) ; M.J. Kelley 1), K. Cossel 1), G.A. Blake 2) 1) Division of Chemistry & Chemical.
Fourier Transform IR Spectroscopy Saptarshi Basu.
Lecture 3 INFRARED SPECTROMETRY
Electron Paramagnetic Resonance spectrometer
Fourier transform infrared spectroscopy[FTIR]
Spectroscopy Microwave (Rotational) Infrared (Vibrational)
Electron Paramagnetic Resonance at Hunter College
ELECTRON SPIN RESONANCE SPECTROCOPY
 PART Requirements for Spectroscopic Techniques for Polymers 1. High resolution 2. High sensitivity (>1%) 3. High selectivity between molecular.
Spectroscopic Analysis Part 4 – Molecular Energy Levels and IR Spectroscopy Chulalongkorn University, Bangkok, Thailand January 2012 Dr Ron Beckett Water.
Physical and Chemical Tests 10-1 Purification: Chromatography Distillation Recrystallization Comparison to known compounds: Melting point Boiling point.
Infrared Spectroscopy
What is spectroscopy? It is the study of how matter interacts with electromagnetic radiation (gamma rays down to radio waves) Matter can interact with.
1 University of Petra Faculty of Science & Arts Department of Chemistry Seminar I.R Spectroscopy By Firas Al-ouzeh Supervisor : Nuha I. Swidan Summer 2007.
1 Waveguides This is the conduit that links the transmitter to the duplexer and antenna It is a hollow conducting tube along which the microwave energy.
A FABRY-PERÓT CAVITY PULSED FOURIER TRANSFORM W-BAND SPECTROMETER WITH A PULSED NOZZLE SOURCE. GARRY S. GRUBBS II, CHRISTOPHER T. DEWBERRY AND STEPHEN.
Edge ECE measurements with the AUG CTS receiver and the effects of ELMs during H-mode Morten Stejner.
1 Atomic Emission Spectroscopy Lecture Advantages of Plasma Sources 1.No oxide formation as a result of two factors including Very high temperature.
Infrared Spectroscopy. Spectroscopy The energy of the interaction of electromagnetic radiaiton (light) with molecules Several different techniques: Infrared.
SPECTROSCOPIC CONCEPTS BY Dr.JAGADEESH. INTRODUCTION SPECTROSCOPY: Study of interaction of matter with electromagnetic radiationelectromagnetic radiation.
Spectrophotometry.
Analytical chemistry 2 Mass spec cont. IR absorption spec.
Introduction to Spectrochemical Methods
INFRARED SPECTROSCOPY
Microwave Source Diode detector Waveguide. Microwave Source Diode detector Waveguide.
CH 3 D Near Infrared Cavity Ring-down Spectrum Reanalysis and IR-IR Double Resonance S. Luna Yang George Y. Schwartz Kevin K. Lehmann University of Virginia.
Infrared Waves  What are they?  Part of the electromagnetic spectrum.
For 3 rd year students- Biophysics Department – Faculty of Science – Cairo University Prepared by: Dr. Heba Mohamed Fahmy and Dr. Alaa Mamdouh.
By Madhu Gyawali Narayan Adhikari Yadab Paudel FTIR Measurements on November 06,08 at Reno Nov 18, 08 PHYS 749 UNIVERSITY OF NEVADA, RENO,NV.
Microwave Spectroscopy Wave length ~ 1 cm to 100  m Wave number ~ 1 to 100 cm -1. Frequency ~ 3 x to 3 x Hz Energy ~ 10 to 1000 Joules/mole.
Fourier Transform IR Spectroscopy. Absorption peaks in an infrared absorption spectrum arise from molecular vibrations Absorbed energy causes molecular.
Infrared Spectroscopy (IR) Fourier Transform Infrared (FTIR)
Infrared Infrared radiation extends from the nominal red edge of the visible spectrum at 700 nanometers (nm) to 1 mm. NameWavelength Gamma rayless than.
Introduction to Coherence Spectroscopy Lecture 1 Coherence: “A term that's applied to electromagnetic waves. When they "wiggle" up and down together they.
Extending the principles of the Flygare: Towards a FT-THz spectrometer Rogier Braakman Chemistry & Chemical Engineering California Institute of Technology.
Rotation and vibration spectra. Rotational States Molecular spectroscopy: We can learn about molecules by studying how molecules absorb, emit, and scatter.
IB NOTES: Modern Analytical Chemistry. Definitions: Qualitative Analysis: The detection of the __________________ but not the __________ of a substance.
MOLECULAR STRUCTURE ANALYSIS NMR Spectroscopy VCE Chemistry Unit 3: Chemical Pathways Area of Study 2 – Organic Chemistry.
How do we know? Spectroscopy: Experimental Evidence.
Dr S D AL_SHAMMA Dr S D AL_SHAMMA11.
Spectroscopy Utilizes the various regions of the electromagnetic spectrum to detect signal.
MOHAMED NIJAS V S5 I.S.P. CONTENT  SPECTROSCOPY.  IR SPECTROSCOPY.  MOLECULAR VIBRATIONS.  EXPERIMENTAL SETUP.  FUTURE DIRECTIONS.
K.-X. AuYong, J.M. King, A.R.W. McKellar, & J.K.G. Watson
INFRARED SPECTROSCOPY Pramod K Singh School of Basic Sciences &Research Sharda University, Greater Noida, INDIA.
Spectroscopy Microwave (Rotational) Infrared (Vibrational)
Components of Optical Instruments
Chem. 133 – 3/14 Lecture.
University of Arizona, Dept. of Physics
Introduction and Principle of IR Spectrophotometry
Lecture 10 IR Theory This Week In Lab: Ch 6 PreLab Due
Atomic Absorption Process
LI: To understand the purposes of spectroscopy.
Raman Spectroscopy A) Introduction IR Raman
Learning Outcomes By the end of this topic students should be able to:
Learning Outcomes By the end of this topic students should be able to:
Mr.Halavath Ramesh 16-MCH-001 Department of Chemistry Loyola College-Chennai University of Madras.
Diode Laser Experiment
Rotational Energy Levels for rigid rotor: Where Rotational Spectra of Rigid Diatomic molecule. BY G JANAKIRAMAN EGS A&S COLLAGE
Presentation transcript:

Microwave Spectrometer The radiation from the source passes through a gaseous sample and is detected by a crystal diode detector that is followed by an amplifier and display system (chart recorder). http://www.britannica.com/nobelprize/article-80625

Varian’s First Klystron

Fourier Transform Microwave Spectrometer … the radiation is confined in an evacuated cavity between a pair of spherical mirrors and the sample is introduced by a pulsed nozzle that lowers the temperature of the sample to less than 10 K. The sample is subjected to rotational energy excitation by application of a pulsed microwave signal, and the resulting emission signal is detected and Fourier-transformed to an absorption versus frequency spectrum. http://www.britannica.com/nobelprize/article-80625

Spectrum for HCl - Far IR

Fundamental Line for HCl

Vibration-Rotation Spectrum for Diatomic Mols.

Vibration – Rotation Spectrum of HCl in the Near IR

Types of Tops

Prolate vs. Oblate Tops

Emission Microwave Spectrum in Orion A

Search for HOC+