First results of a novel silicon drift detector array designed for low energy X-ray fluorescence spectroscopy Alexandre Rachevski* a, Mahdi Ahangarianabhari.

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Presentation transcript:

First results of a novel silicon drift detector array designed for low energy X-ray fluorescence spectroscopy Alexandre Rachevski* a, Mahdi Ahangarianabhari d, Pierluigi Bellutti f, Giuseppe Bertuccio d,e, Elena Brigo d, Jernej Bufon a,b, Sergio Carrato c, Andrea Castoldi d,e, Giuseppe Cautero b,a, Sergio Fabiani a, Gabriele Giacomini f, Alessandra Gianoncelli b,a, Dario Giuressi b, Chiara Guazzoni d,e, George Kourousias b, Chang Liu d, Ralf Hendrik Menk b,a, Giuseppe Vito Montemurro d, Antonino Picciotto f, Claudio Piemonte f, Irina Rashevskaya g, Yongbiao Shi d, Andrea Stolfa b, Andrea Vacchi a, Gianluigi Zampa a, Nicola Zampa a, Nicola Zorzi f *) corresponding author, a) INFN Trieste, b) Elettra-Sincrotrone Trieste S.C.p.A., c) University of Trieste, d) Politecnico di Milano, e) INFN Milano, f) Fondazione Bruno Kessler (FBK), Trento, g) TIFPA-INFN, Trento ABSTRACT We developed a trapezoidal shaped matrix with 8 cells of Silicon Drift Detectors (SDD) featuring a very low leakage current (below 180 pA/cm 2 at 20 C) and a shallow uniformly implanted p + entrance window that enables sensitivity down to few hundreds of eV. The matrix consists of a completely depleted volume of silicon wafer subdivided into 4 square cells and 4 half- size triangular cells. The energy resolution of a single square cell, readout by the ultra-low noise SIRIO charge sensitive preamplifier, is 158 eV FWHM at 5.9 keV and 0 C. The total sensitive area of the matrix is 231 mm 2 and the wafer thickness is 450 µm. The detector was developed in the frame of the INFN R&D project ReDSoX in collaboration with FBK, Trento. Its trapezoidal shape was chosen in order to optimize the detection geometry for the experimental requirements of low energy X- ray fluorescence (LEXRF) spectroscopy, aiming at achieving a large detection angle. We plan to exploit the complete detector at the TwinMic spectromicroscopy beamline at the Elettra Synchrotron (Trieste, Italy). The complete system, composed of 4 matrices, increases the solid angle coverage of the isotropic photoemission hemisphere about 4 times over the present detector configuration. We report on the layout of the SDD matrix and of the experimental set-up, as well as the spectroscopic performance measured both in the laboratory and at the experimental beamline.

Sensor front (a) and back side (b) a b New LEXRF detection system consisting of 4 trapezoidal shaped matrixes of 8 SDD cells each 55 Fe spectrum measured in the climatic chamber at 0 ◦ C. The energy resolution for Mn K α line is 158 eV FWHM Spectrum measured with a standard reference sample: a 550nm layer of MgF 2 deposited on a 100nm thick Si 3 N 4 membrane. The peaks correspond to F (676.8 eV), Mg ( eV) and Si (1740 eV) Al (panel B, C) and Na (panel E, F) XRF maps of a soybean root section acquired with standard TwinMic LEXRF and the new detector system, respectively. C and F were acquired with a single square cell one trapezoidal multi-cell SDD. The corresponding absorption (panel A) and phase contrast (panel D) images are shown as well. Standard, Al Standard, Na New detector, Al New detector, Na F Mg Si