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CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile 20091 Rapid screening and identification of illegal Drugs by IR Absorption spectroscopy and gas.

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Presentation on theme: "CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile 20091 Rapid screening and identification of illegal Drugs by IR Absorption spectroscopy and gas."— Presentation transcript:

1 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Rapid screening and identification of illegal Drugs by IR Absorption spectroscopy and gas Chromatography (DIRAC) Rapid screening and identification of illegal Drugs by IR Absorption spectroscopy and gas Chromatography (DIRAC) Theme 10: Security, Cooperation Programme Topic: SEC : Drug precursors Proposal #: Proposal deadline: 8 dec 2008 Duration: 42 months Theme 10: Security, Cooperation Programme Topic: SEC : Drug precursors Proposal #: Proposal deadline: 8 dec 2008 Duration: 42 months Status: 1 st project in the reserve list Status: 1 st project in the reserve list April 2009 (unofficial communication): accepted for negotiation Status: 1 st project in the reserve list Status: 1 st project in the reserve list April 2009 (unofficial communication): accepted for negotiation Evaluation summary (mar 2009) Total: 12.5/15 S/T quality: 4/5Implementation: 4/5Impact: 4.5/5 Evaluation summary (mar 2009) Total: 12.5/15 S/T quality: 4/5Implementation: 4/5Impact: 4.5/5 S. Zampolli, I.Elmi, GC.Cardinali

2 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Partnership 1. 1.Consorzio CREO - LAquila, Italia (Coordinatore) 2. 2.Fraunhofer Institute IPM - Friburgo, Germania 3. 3.CNR IMM - Bologna, Italia 4. 4.EADS Innovation Works - Monaco di Baviera, Germania 5. 5.Elsag Datamat SpA - Italia 6. 6.Universite de Lausanne - Losanna, Svizzera 7. 7.University "Dunarea de Jos" - Galati, Romania 8. 8.National Institute for Criminalistics and Criminology - Bruxelles, Belgio 9. 9.National Bureau of Investigation - Helsinky, Finlandia CNISM - Unità di Parma – Parma, Italia 1. 1.Consorzio CREO - LAquila, Italia (Coordinatore) 2. 2.Fraunhofer Institute IPM - Friburgo, Germania 3. 3.CNR IMM - Bologna, Italia 4. 4.EADS Innovation Works - Monaco di Baviera, Germania 5. 5.Elsag Datamat SpA - Italia 6. 6.Universite de Lausanne - Losanna, Svizzera 7. 7.University "Dunarea de Jos" - Galati, Romania 8. 8.National Institute for Criminalistics and Criminology - Bruxelles, Belgio 9. 9.National Bureau of Investigation - Helsinky, Finlandia CNISM - Unità di Parma – Parma, Italia

3 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Project aim and concept Advanced sensor system to recognize and detect illicit drugs, illicit drug precursors and potential derivatives of key precursors (Amphetamine-type-stimulants - ATS) Innovative aspects Miniaturized Gas Chromatography (GC) as key chemical separation toolMiniaturized Gas Chromatography (GC) as key chemical separation tool Hollow-Fiber-based Infra Red Absorption Spectroscopy (HF- IRAS) as key analytical toolHollow-Fiber-based Infra Red Absorption Spectroscopy (HF- IRAS) as key analytical tool Advanced sensor system to recognize and detect illicit drugs, illicit drug precursors and potential derivatives of key precursors (Amphetamine-type-stimulants - ATS) Innovative aspects Miniaturized Gas Chromatography (GC) as key chemical separation toolMiniaturized Gas Chromatography (GC) as key chemical separation tool Hollow-Fiber-based Infra Red Absorption Spectroscopy (HF- IRAS) as key analytical toolHollow-Fiber-based Infra Red Absorption Spectroscopy (HF- IRAS) as key analytical tool

4 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Sensor system Sequence of operations and building blocks

5 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Particle selective collection Molecules with amine groups have a high proton affinityMolecules with amine groups have a high proton affinity

6 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Preconcentration modules: vapour-phase to treat analytes that can be vaporised without thermal decomposition:to treat analytes that can be vaporised without thermal decomposition: free-base form amphetamines and precursors selective-trapping using quinoxaline cavitands (aromatic amines)selective-trapping using quinoxaline cavitands (aromatic amines) flow-matchingflow-matching to treat analytes that can be vaporised without thermal decomposition:to treat analytes that can be vaporised without thermal decomposition: free-base form amphetamines and precursors selective-trapping using quinoxaline cavitands (aromatic amines)selective-trapping using quinoxaline cavitands (aromatic amines) flow-matchingflow-matching

7 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Preconcentration modules: liquid-phase detection of the ammonium salts of amphetamines (very low vapour pressure)detection of the ammonium salts of amphetamines (very low vapour pressure) selective trapping by phosphonate cavitands on Siselective trapping by phosphonate cavitands on Si detection of the ammonium salts of amphetamines (very low vapour pressure)detection of the ammonium salts of amphetamines (very low vapour pressure) selective trapping by phosphonate cavitands on Siselective trapping by phosphonate cavitands on Si

8 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile HF-IRAS module

9 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile GC module and detectors GC column and micro-fluidic circuitryGC column and micro-fluidic circuitry MOX and Surface Ionization (SI) detectorsMOX and Surface Ionization (SI) detectors GC column and micro-fluidic circuitryGC column and micro-fluidic circuitry MOX and Surface Ionization (SI) detectorsMOX and Surface Ionization (SI) detectors SI detector (EADS) GC column (IMM) Example of MEMS based GC module MOX array (IMM)

10 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile WPs and partner roles Work Package No Work package titleType of activiy Lead Participant No Lead Participant short name Person months Start month End month 0ManagementMGT1CREO18.25M01M42 1RequirementsRTD8NICC28.50M01M06 2Sensor System and ApplicationRTD1CREO69M04M42 3Sampling moduleRTD4EADS23M01M36 4Treatment/pre-concentration module RTD3CNR IMM47M01M36 5HF-IRAS moduleRTD2FRAUNHOFER68M01M36 6GC module and detectorsRTD4CNR IMM37M01M36 7Expert SystemRTD7UDJG50.50M01M42 8Experimental tests and performance assessment RTD6UNIL63.50M06M42 9Exploitation and dissemination of results OTHER5CREO21.50M01M42 TOTAL

11 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Project costs and EC contribution Organisation short name TOTAL Grant requested % CREO758, , FRAUNHOFER600, , CNR IMM454, , EADS660, , ED408, , UNIL432, , UDJG351, , NICC225, , NBI146, , INSTM220, , TOTAL ,002,987,

12 CNR – IMM Bologna Gruppo sensori e microsistemi21 aprile Related research projects (Previous and ongoing) EC FP4 SMOG EC FP5 Clean-Air EC FP6 GoodFood FISR RBNE019TMF FIRB Microsistemi per applicazioni ambientali ed agroalimentari Related research projects (Previous and ongoing) EC FP4 SMOG EC FP5 Clean-Air EC FP6 GoodFood FISR RBNE019TMF FIRB Microsistemi per applicazioni ambientali ed agroalimentari Staff: Ivan Elmi Stefano Zampolli Gian Carlo Cardinali Enrico Cozzani Fulvio Mancarella Piera Maccagnani Alberto Roncaglia Maurizio Severi Staff: Ivan Elmi Stefano Zampolli Gian Carlo Cardinali Enrico Cozzani Fulvio Mancarella Piera Maccagnani Alberto Roncaglia Maurizio Severi Luca Masini Antonio Zani Fabrizio Tamarri Michele Sanmartin Paolo Negrini Giulio Pizzochero Luca Masini Antonio Zani Fabrizio Tamarri Michele Sanmartin Paolo Negrini Giulio Pizzochero NetLab ENVIREN NetLab PROMINER PRRIITT – UNITEC Progetto Pollution NetLab ENVIREN NetLab PROMINER PRRIITT – UNITEC Progetto Pollution


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