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Prof Amal Ezzeldin Abdel Aziz Professor of Dental Biomaterials.

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Presentation on theme: "Prof Amal Ezzeldin Abdel Aziz Professor of Dental Biomaterials."— Presentation transcript:

1 Prof Amal Ezzeldin Abdel Aziz Professor of Dental Biomaterials

2 Elastic Aqueous Hydrocolloids Non-aqueous Elastomers Polysulfide Silicones Polyether Condensation Addition Agar (reversible) Alginate ( irreversible ) O’Brien Dental Materials & their Selection 1997

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4  Solution: homogenous mixture: one phase system.  Suspension: hetrogenous mixture: two phase system.  Colloids: hetrogenous, particle size of the particles are smaller than in suspension: two phase system.  Dispersed phase.  Dispersion medium  water  Hydrocolloid

5 Sol state: viscous liquid. Sol state: viscous liquid. Gel state: jelly like Gel state: jelly likesol   fibrils in a network pattern.  Brush heap structure SOL reversible hydrocolloid reversible hydrocolloid Or by: chemical reaction: irreversible hydrocolloid. Agglomeration of molecules reduction in temperature g el

6 Advantages:  Easy to manipulate.  Does not require special equipment.  Relatively inexpensive.  Comfortable for the patient. Uses Sol  gel by chemical reaction

7 Composition:  Potassium alginate.(soluble sol)  Calcium sulphate dihydrate.(reactor)  Potassium sulphate.  Sodium phosphate: retarder.  Diatomaceous earth: filler.  Glycols: dustless.  Pigments.  Flavours.  Quaternary ammonium salts: Disinfectants

8  Potassium alginate (15%)  Soluble alginate  Calcium sulfate dihydrate (16%)  Reactor  Diatomaceous earth (60%)  Fillers  Strength, Stiffness, Texture  Potassium titanium fluoride (3%)  Accelerator for the setting of the stone  Sodium phosphate (2%)  Retartder - reacts with calcium ions to slow the working time  Glycols  Decrease dust formation  Quaternary ammonium salts  Disinfectants  Pigments, taste

9 Substance is alginic acid, which was extracted from seaweed. Potassium salt form of alginic acid (Potassium alginate) react with calcium sulfate dihydrate and water to form a calcium alginate gel.

10 Reaction: 1.CaSO 4.2H 2 O + Na 3 PO 4 2.CaSO 4.2H 2 O + kalginate  K 2 SO 4 + calcium alginate (insoluble gel) Types: amount of Na 3 PO 4  Fast set: less amount of retarder.  Regular set. + H 2 O Ca 3 PO 4 + Na 2 SO 4

11  The final structure cross-linked calcium alginate gel. Cross-linking of Sodium alginate

12 Concentration of filler: Controls flexibility of set impression.  Soft set: less amount of filler.  Hard set. Manipulation:  Proportioning.  Mixing: vigorous mix – against sides of the rubber bowl.  Mixing time: 45 seconds (fast set). One minute (regular set).

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14 Gelation time: Time from the start of mix till material is no longer tacky when touched with finger.  Avoid movement of the tray during setting.  Remove the tray after additional/2-3 minutes as elasticity is improved with time and permanent deformation is .

15  Once gelation starts, the impression material must not be disturbed because the growing fibrils will fracture and the impression would be significantly weakened.  Fast setting = mins.  Normal setting = 3 – 4.5 mins  Best regulated by the amount of retarder added during manufacturing.

16 Control of the S.T: Do not reduce powder/H 2 O ratio as this affects consistency, accuracy and  strength. To prolong S.T: reduce temperature of H2O *not below 18°C. temperature of water should be between 18-24°C. Better to choose the suitable type of alginate. Fast setting = mins. Normal setting = 3 – 4.5 mins

17 Removal of the impression: one sudden pull-single stroke.  As the material is Visco Elastic:  Mechanical properties are time dependant and depends upon rate of load application. Rapid rate of removal: Tear Strength  4 times by sudden pull removal.

18 Pouring impression: washing under running tap H 2 O, to remove blood, saliva. No: separating medium. Avoid torquing or twisting when remove the impression

19 How to avoid such How to avoid such Dimensional changes.(synersis –imbibition –evaporation) 1. Immediate pouring of the impression. 2. Storing in a humidor: 100% relative humidity or wrapping in paper towel saturated with water. This does not prevent synersis. Done only for one hour maximum.

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21 Surface Hardness Of The Cast ( Gypsum casts poured against hydrocolloids sometimes have rough or chalky surface which causes inaccuracy or lack of sharp details. Causes: 1-Impression not washed from blood or saliva after removal from the mouth as blood and saliva retard the setting of gypsum.

22 2-Excess H 2 O left in impression surface before pouring  dilute surface of the model. 3-Impression stored in humidor for ½ or 1 hour, not washed to remove exudate. 4-Removal of the model after a long time (several hours)…contact of the gel containing H2O with gypsum which is slightly soluble. CaSO 4.2H 2 O  chalky surface. 5-Premature removal of the model: not before one hour.

23  Certain disinfectants my result in gypsum casts that have a lower surface hardness or diminished surface detail  Current protocol  Impression --> thoroughly rinsed --> spray disinfectant -- > wrap in a disinfectant-soaked paper towel --> place in a sealed plastic bag for 10 minutes  Iodophor, Sodium hypochlorite, Glutaraldehyde

24 Syringed agar: boiled for 8 minutes cooled to 65°C for 10 minutes, injected around preparation. Alginate: mixed in tray over agar. Setting time: 4 minutes.

25 Advantages: Simple heating equipment.Simple heating equipment. No water cooling system trays.No water cooling system trays. Fine details of preparation.Fine details of preparation. Agar: more compatible with gypsum model materials than alginate, & has higher tear strength than algianteAgar: more compatible with gypsum model materials than alginate, & has higher tear strength than algiante


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