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An Introduction. Product Categories: Product Categories: - Fully Formulated DielectricTelecommunicationRefrigeration - Intermediates Alkylates, Sulfonates,

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Presentation on theme: "An Introduction. Product Categories: Product Categories: - Fully Formulated DielectricTelecommunicationRefrigeration - Intermediates Alkylates, Sulfonates,"— Presentation transcript:

1 An Introduction

2 Product Categories: Product Categories: - Fully Formulated DielectricTelecommunicationRefrigeration - Intermediates Alkylates, Sulfonates, Polybutene - Synthetic Basestocks Alkylates, PB, PAO - Additives Component and Packages Soltex has been formulating, qualifying and supplying alkylate Soltex has been formulating, qualifying and supplying alkylate and polybutene based performance products to the power, telecommunication, refrigeration, lubrication, plastics, adhesives, rubber and personal care industries for over 20 years.

3 Dielectric Fluids Dielectric Fluids Alkylate / Polybutene blends insulation oils with optimum high oxidative and thermal stability. QUALIFIED AT THESE UTILITY/CABLE COMPANIES: Dominion Electric – Richmond, VA Potomac Electric – Washington, D. C. Boston Edison (N Star) – Boston, MA NYPA – Newburg, NY Cambridge Electric/Okonite – Cambridge, MA PS of Colorado – Denver, CO Baltimore Gas & Electric – Baltimore, MD Consolidated Edison – New York, NY Los Angeles Power & Water – Los Angeles, CA WA Chester/Florida Power & Light – Miami, FL Jacksonville Electric, - Jacksonville, FL National Grid / Keyspan-Hicksville, NY Exelon/Commonwealth Edison – Chicago, IL MAC Products – Kearney, NJ Underground Systems – Armonk, NY W.A. Chester/Northeast Utility- Bethel, CT W.A. Chester/Memphis P&L Memphis, TN PSE&G – Somerset, NJ The Okonite Company – Ramsey, NJ Prysmian – Canada and US Hydro One, EHV,Comstock – Toronto, ON

4 Telecommunication Oils and Gels Formulations of PB/Waxes and antioxidants which impart tack, oxidation stability and water repellency.

5 Synthetic Alkylate Refrigeration Fluids Excellent low temperature properties, low flocculant points indicating good solvency for a hydrocarbon in polar fluids, low foaming, good lubrication, thermal stability, excellent elastomeric compatibility. Excellent low temperature properties, low flocculant points indicating good solvency for a hydrocarbon in polar fluids, low foaming, good lubrication, thermal stability, excellent elastomeric compatibility. OEM APPROVALS Tecumseh Products Bristol Compressors York Greenville Products Mycom FES Carrier/Carlyle Copeland General Electric Trane Scroll Technologies Whirlpool Embraco

6 Intermediates Products -Alkylates-Sulfonates-Polybutenes

7 Alkylates Alkylates have good low temperature properties, solubility, oxidative and thermal stability. Possible alternatives to more expensive esters or less oxidative stable naphthenic. PropertyNapthenicEsterAlkylate Oxidative Stability * ** *** Pour Point *** Aniline Point ****** Hydrolytic Stability ***** Current Alkylate ProductsQualitative Comparison

8 Sulfonates – oleum and mixture of oleum and natural sulfonation yielding neutral and over based sulfonates of Sodium, Barium, Calcium,Magnesium Sulfonates Gelled Sulfonates – crystalline calcium sulfonates in solvent, oil or water carriers. Sulfonic Acid – oleum sulfonated linear alkylaromatic sulfonic acid Sulfonic Acid – oleum sulfonated linear alkylaromatic sulfonic acid

9 Sulfonic Acid: oleum sulfonated, highly active sulfonic acid with little free acidity and almost no odor which yields products of very light color.

10 Sulfonates Sulfonates MetalCharacteristic SodiumSolvency, low ash and stain CalciumAsh, general purpose, scavenger for combustion acids BariumAsh, best corrosion inhibition, non- staining MagnesiumAsh, vanedium scavenger Applications: Detergent in lubricant (neutralizing acidic products of combustion and degradation). Rust and corrosion inhibition Boundary and extreme pressure lubrication in metal working Base for Calcium Sulfonate grease (overbased) Emulsifiers

11 Metal (%) Inorganic Salt % Oil %Avg. MW TBNVis @ 100 cSt Sulfol 465Emulsifiable oils or as bases, dispersants Sodium (62) 0.634465 Sulfol 500Same as 465Sodium (62) 0.634500 Neutral Bar 50First intent, non-staining rust protection with good demulsibility and detergency Barium (6.6) 504.025 – 100 Neutral Cal 10High activity, imparts good rust and corrosion properties Calcium (60) 6098010212 AmorCal 400Excellent gelling, excess alkalinityCalcium (20) 98040075 AmorCal 800High solubility, excess alkalinity, good detergency Calcium (20) 980400110 AmorCal 400 FGExcellent gelling, excess alkalinity and food grade Calcium (20) 980400

12 Soltex Gelled Calcium Sufonates PRODUCTDescription Application % Non Volatile Viscosity cPFlash Pt Dens ity Salt Spray Test ThixoCal 7600 Dispersion of modified calcium in mineral. Corrosion preventive compound with enhanced penetrating characteristics,. 58-6550-90,0001059.0 ThixoCal 2000/A Solvent free, gelled calcium sulfonate in an oil carrier. Basestock, removable rust preventative Bearings, hinges, wire rope cable lubes 9685-135,000340 8.9- 9.9 ThixoCal 3000A Gelled calcium sulfonate, wax, oil and others in mineral spirits Base for formulations, short term outdoor or long-term indoor storage 58-6240-65,000105 7.8- 8.0 ThixoCal 5300/5400 High solids, moderately formulated corrosion preventive compound 68-7310-25,0001051.0 Excess of 5000 hrs at 3 mils ThixoCal 5752x Formulated with waxes, oils and other ingredients in mineral spirits. General rust proofing 52-583-6000105 7.2- 7.4 ThixoCal 8100 High solids, low VOC, corrosion preventionBase for architectural and plant equipment and structural steel coatings 68-745-13,000105 8.0- 8.3 ThixoCal 8200 80% solids corrosion preventive base compound with additives Base, penetrant. 78-827-15,000105 8.0- 8.23 ThixoCal 4400 Morpholine-Free, water-based rust and corrosion preventive coating Automotive anti-corrosion coating OEM and aftermarket 453.5-9,000 7.8- 8.2 ThixoCal 4500 Formulated corrosion prenentive water-borne coating excess amine Base for water-borne anticorrosion coatings 46-5225-60,000 8.1- 8.3

13 Sulfonate New Products Under Development : 1. Biodegradable Rail Curve Lubricant 2. Grease base (No.1 and 2 grease available) 3. Food Grade Overbased Calcium Sulfonate (available) 4. Magnesium Carboxylate

14 Polybutylenes: Soltex Polybutene products are range from 350 to 2600 MW and from 12cSt at 40C to 4900cSt at 100C. We react, formulate and blend these – to make derivatives of PB and custom PB blends just right for the application. Polybutenes increase viscosity, add tack, decompose cleanly, are synthetic, NSF, Kosher and Halal approved, and have good oxidative and thermal stability.

15 I - alpha- Vinylidene Polybutenes: II beta-VinylideneIII - Tri-substitutedIV - Tetra-substituted No.Terminal Olefin Structure Conventional PIB % HR PIB % I-PIB % I alpha-Vinylidene (alpha- olefin) 4 - 575 - 9050 – 65 II beta-Vinylideneabsent or minor10 - 2535 – 50 III Tri-substituted63 -67absent or minor IV Tetra-substituted22 – 281 - 51 – 5 IV-A Tetra-substituted5 - 101 – 2 IV-A Tetra-substituted

16 High Molecular Weight Polyisobutylenes: Extremely high molecular weight polymers which are solid at ambient conditions. They are used in food contact applications, greases, medical adhesives, asphalt Improver, electrical insulating material, adhesives sealants, special pigments.

17 Lubricant Additive Components: Polymeric Thickeners Tackifiers Emulsifiers / Intermediates Detergents Dispersants Viscosity Index Improvers Pour Point Depressants Antiwear/EP Additive Grease Additives

18 Soltex Polymeric Thickener - BSR-900 Viscosity Modifier Description: Soltex BSR 900 is a polybutene based polymeric thickener viscosity modifier developed for use in a wide range of high viscosity industrial lubricants. Features and Benefits Excellent thickening at low treat levels( 5 to 40 %) High shear stability Superior oxidation resistance compared to Napthenic Lower cost than PAO and PAG Excellent solubility and clarity Good viscosity index boost

19 Soltex OMG Tackifiers – E857, E858, E859 FG Description: High molecular weight PIB based polymeric Tackifiers developed for use in a wide range of industrial lubricants: 2500 to 3000 cSt @ 100 C: industrial grade, light colored grade and food grades available. Features and Benefits Imparts a tack or stringiness to a substance and is typically used to provide adherence in fluid lubricants and stringiness in greases. Food grade and non-food grade available light colored available for color sensitive applications

20 Soltex Polybutene Derivatives Emulsifiers / Intermediates / Dispersants / Anti-foulants Soltex PCA 9010, 9030,9050, 9060, 9070, 9080 and 9090 PIBSA – Polybutenyl Succinic Anhydride – emulsifier, raw material PIBSI – Polybutenyl Succinimide - dispersant Di-PIBSI – Di-Polybutenyl Succinimide – anti-foulant Soltex has the technical expertise to custom formulate a polyisobutylene emulsifier, dispersant, anti-foulant or other functional product to customers needs.

21 Soltex Detergents AmorCal 800, Fricshun, PCA 4001 Soltex has the technical expertise to custom formulate a polyisobutylene emulsifier, dispersant, anti-foulant or other functional product to customers needs. Description: Numerous metal salts of organic acids and non-metal compounds with and without excess base used to neutralize the acids to form salts and protect metal. Features and Benefits React with acids formed in lubricants to form inert salts. Numerous metals (sodium, sulfur and barium available) Over based available Ashless, biodegradable and nontoxic available – allowing a boost in TBN without an increase in sulfur.

22 Viscosity Index Improvers Soltex S-Flow V1201 and S-Flow V6200 Description: Alkyl methacrylate co-polymers in a highly refined mineral oil. Benefits: Excellent shear stability and viscosity modification. Numerous grades available allow formulator to taylor to your specific applications.

23 Pour Point Depressants Soltex S-Flow P702, P750, P801, P821 Description: Alkyl methacrylate co-polymers that exhibit highly effective control of paraffinic wax crystal formation in both industrial and automotive lubricants. A variety of product grades allow you to taylor to your specific application requirements: from low Napthenic content to heavier base oils and broad applicability. Benefits: Offer lubricant formulator flexibility to choose a broad application PPD and thus minimize inventory, or tailor to specific applications. They will not impact color of high quality base oils.

24 Antiwear / EP Additive - Soltex PCA 3001 Functional Bismuth Soap Non Toxic Extreme Pressure / Anti-wear Additive Soltex PCA 3001 is a very thermally stable EP/AW additive which works in conjunction with all types of sulfur to provide outstanding antiwear for gear oils, engine oils, hydraulic oils, and other industrial and automotive fluids. It will dramatically increase 4-ball weld loads and Timken OK weld points. Typical treat rates of 3.3% in combination with 0.4 elemental sulfur will produce a 4-ball weld load of 620kg in a ISO 220 base oil lithium complex, Lithium, or calcium complex grease. Features and Benefits  Excellent Extreme Pressure Properties  Low Volatility yielding long life at high-temperatures.  Non-Toxic Environmentally preferred Table 1: Typical Characteristics PropertyTest MethodUnitsValue Specific Gravity @ 20 ºC (77ºF) ASTM D 287G/ml0.956 Kinematic Viscosity @ 40 ºC(104ºF) ASTM D 445CSt163 Flash Point COCºC198 Weight Loss, 204 ºC, 22 hoursASTM D972Wt. %6.3 Pour PointASTM D 97ºC(ºF)-15(5)

25 Soltex Additive Packages: PCMO, DEO Tractor Hydraulic Detergent Dispersants Friction Modifiers Antioxidant Extreme Pressure Performance Boosters: Extra TBN Rust and Oxidation Inhibitors Viscosity Modifier Economy grade tractor hydraulic fluid Safely used in most sump-type agricultural equipment including John Deere, Case and New Holland, Massey Ferguson and Ford Provides gear wear protection, maintains hydraulic system performance and prevents oxidation to prolong fluid life. Treat rate is 4.0 wt% in Group I,II base oil. Tractor Hydraulic Additive Package Multifunctional lube oil additive package used to formulate high quality mono-grade and multi-grade gasoline and diesel engine oils with properties similar to a wide range of API classifications. Contains detergents, dispersants, antioxidants, friction modifiers, rust and oxidation inhibitors Non-detergent VI improvers required to meet multi-grade viscosity classifications Performance boosters required to meet high TBN (>10) specifications Passenger Car Motor Oil Additive Package Diesel Engine Oil Additive Package High performance diesel engine oil additive package for high speed turbocharged engines operating on fuel containing up to 0.5% S Contains Ashless dispersant, ZDDP, metallic detergents. Non-detergent VM with SSI of 20 – 40 recommended for multigrade oils

26 Passenger Car Motor Oil Additive Packages Comparison PCA 2877PCA2886 Viscosity @ 100C9065 TBN11578 Calcium wt%3.82.0 Nitrogen wt %0.551.10 Phosphorus wt%1.870.87 Zinc Wt %2.101.0 Molybdenum ppm425 Soltex Passenger Car Motor Oil Additives – PCA 2877 and PCA 2886

27 Passenger Car Motor Oil Additive Packages Comparison High performance diesel engine oil additive package for high speed turbocharged engines operating on fuel containing up to 0.5 % Sulfur. Contains Ashless dispersant, ZDDP, metallic detergents. Field tested over 5 years with no complaints. Non- detergent VM with SSI of 20-40 recommended for multi grade oils. Performance LevelWt % CH-4 / SJ Premium15.04 CH-4/SJ Fighting13.07 CG-4, CF, CF2,CF4,CE/SJ11.28 CF-2, CF9 Specific Gravity @ 15.6C0.971 Viscosity, cSt @ 100C30 TBN, mg KOH/g66 Calcium, Wt %1.8 Nitrogen, Wt %0.72 Phosphorus, Wt%0.91 Zinc, Wt %0.98 Molybdenum, ppm700 Soltex Diesel Engine Oil Additive PCA 2861

28 Soltex Custom Additive Packages: Blends of quality dispersants, detergents, antioxidants, AW/EP additives and other ingredients can be custom blended to your specification. - create many different lubricants from these bases - consolidate your purchases, - decrease your blending time - save money. You specify the nitrogen, zinc, calcium, sulfur, phosphorus, total base number…

29 Soltex Services: Technical Expertise: Ed Baxter: - Over 30 years experience in R&D including, R&D Director, Laboratory Director and Pilot Plant Manager -Experienced in Intellectual Property (IP) management; over 25 patents filed in last three years. -Broad product development experience in the areas of polymers (polyisobutylene, polyolefins, polyurethanes, polyethers), hydrocarbon products, hydrocarbon resins, fuel and lube additives, lube basestocks, caulks, sealants, adhesives (PSA and hot melt), crop protection chemicals, bulk pharmaceuticals and cosmetic formulations. -Synthetic organic experience in alkylations, etherifications, benzoylations, halogenation, alkylene oxide polymerizations (EO,PO,BO), olefin oligomerizations and polymerizations, hydroformylations, catalysis, aminations, maleations, hydrodimerizations (butadiene), dehydrations, hydrogenations, mannich base reactions, and, high pressure reaction chemistry.Experienced in instrumental methods of analysis including Gel Permeation Chromatography (GPC), High Performance Liquid Chromatography (HPLC), UV/Vis, FTIR, H1 NMR, C13 NMR, packed and capillary column GC and GC/MS. Soltex has a full-service, independent, analytical laboratory specializing in petroleum and petrochemical applications. We offer a complete battery of standard ASTM test methods, from acid number to wax content, plus hard to find specialty procedures. Laboratory Services:

30 Soltex Services: - Bulk handling / trans - loading - packaging drums and totes - warehousing - heating of tank trucks / iso-containers


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