# Dasar Keteknikan Pengolahan Pangan

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Dasar Keteknikan Pengolahan Pangan
Sudarminto Setyo Yuwono

Apple Cooling qfrig

INTRODUCTION The study of process engineering is an attempt to combine all forms of physical processing into a small number of basic operations, which are called unit operations Food processes may seem bewildering in their diversity, but careful analysis will show that these complicated and differing processes can be broken down into a small number of unit operations Important unit operations in the food industry are fluid flow, heat transfer, drying, evaporation, contact equilibrium processes (which include distillation, extraction, gas absorption, crystallization, and membrane processes), mechanical separations (which include filtration, centrifugation, sedimentation and sieving), size reduction and mixing.

DIMENSIONS AND UNITS All engineering deals with definite and measured quantities, and so depends on the making of measurements To make a measurement is to compare the unknown with the known record of a measurement consists of three parts: the dimension of the quantity, the unit which represents a known or standard quantity and a number which is the ratio of the measured quantity to the standard quantity

Dimensions These dimensions are length, mass, time and temperature.
For convenience in engineering calculations, force is added as another dimension Dimensions are represented as symbols by: length [L], mass [M], time [t], temperature [T] and force [F].

example: Length = [L], area = [L] 2, volume = [L] 3.
Velocity   = length travelled per unit time=[L]/[t] Pressure      = force per unit area=[F]/[L] 2 Energy         = force times length=[F] x [L]. Power          = energy per unit time=[F] x [L]/[t] h=[F] x [L]/[L]2 [t] [T] =[F] [L] -1 [t] -1 [T] -1

Units the metre (m) is defined in terms of the wavelength of light;
the standard kilogram (kg) is the mass of a standard lump of platinum-iridium; the second (s) is the time taken for light of a given wavelength to vibrate a given number of times; the degree Celsius (°C) is a one-hundredth part of the temperature interval between the freezing point and the boiling point of water at standard pressure; the unit of force, the newton (N), is that force which will give an acceleration of 1 m sec-2 to a mass of 1kg; the energy unit, the newton metre is called the joule (J), the power unit, 1 J s-1, is called the watt (W).

Dimensionless Ratios It is often easier to visualize quantities if they are expressed in ratio form and ratios have the great advantage of being dimensionless For example, specific gravity is a simple way to express the relative masses or weights of equal volumes of various materials. The specific gravity is defined as the ratio of the weight of a volume of the substance to the weight of an equal volume of water SG = weight of a volume of the substance/ weight of an equal volume of water . Dimensionally, SG=[F]/ [L]-3 divided by[F]/ [L]-3 = 1 it gives an immediate sense of proportion This sense of proportion is very important to food technologists as they are constantly making approximate mental calculations for which they must be able to maintain correct proportions Another advantage of a dimensionless ratio is that it does not depend upon the units of measurement used, provided the units are consistent for each dimension Dimensionless ratios are employed frequently in the study of fluid flow and heat flow. These dimensionless ratios are then called dimensionless numbers and are often called after a prominent person who was associated with them, for example Reynolds number, Prandtl number, and Nusselt number

Neraca Massa Tahapan perhitungan: Gambar diagram
Tulis reaksi kimia jika ada Tulis dasar-dasar perhitungan Hitung neraca massanya

Mass Balance soda api (NaOH), sebanyak 1000 kg/jam larutan mengandung 7,5% NaOH di pekatkan pada evaporator yang pertama sehingga kadarnya menjadi 20%. Larutan ini lalu dipekatkan pada evaporator yang kedua yang menghasilkan pekatan berkadar 60% NaOH. Hitung NaOH yang dihasilkan.

Dikerjakan dan dikumpulkan
Proses produksi jam buah dilakukan dengan cara memekatkan bubur buah dari kadar padatan 10% menjadi 35%. Pemekatan dilakukan dalam 2 tahap evaporator. Pada evaporator yang pertama kadar padatan meningkat menjadi 22%. Hitung jam buah yang dihasilkan untuk tiap 100 kg bubur buah yang dipakai.

Neraca massa jika terjadi reaksi kimia
Beberapa proses pengolahan kemungkinan terjadi reaksi kimia Fermentasi Pembakaran Dasar perhitungan bukan dari massa tetapi dari perubahan mol Setelah itu baru dikonversikan ke massa

contoh Bahan bakar mengandung 5 %mol H2, 30 %mol CO, 5 %mol CO2, 1 %mol O2, dan 59 %mol N2. Dibakar dengan media udara. Untuk 100 kg mol bahan bakar hitung mol gas buang dan kamponennya, jika : A. Pembakaran sempurna, udara pas B. Pembakaran 90% sempurna C. Udara berlebih 20%, pembakaran sempurna 80%

contoh Larutan NaOH diproduksi dengan cara menambahkan larutan Na2CO3 10% ke dalam aliran bubur Ca(OH) 2 25%. Bagaimana komposisi bubur akhir jika reaksi 90% sempurna dan 100% sempurna. Gunakan dasar 100 kg aliran bubur Ca(OH)2 Na2CO3 + Ca(OH) 2 => 2NaOH + CaCO3 Ca(OH) 2= 74,1; Na2CO3 = 106

Recycle Pada suatu proses produksi sodium sitrat, 1000kg/jam larutan sodium sitrat berkadar 20% dipekatkan di suatu evaporator bersuhu 353K sehingga diperoleh kadar 50%. Larutan lalu dimasukkan ke kristalizer yang bersuhu 303K sehingga diperoleh kristal Na sitrat berkadar 95%. Larutan jenuh yang mengandung 30% Na sitrat lalu direcycle ke evaporator. Hitung berapa laju aliran recycle dan produk yang dihasilkan.

Harap dikerjakan Pada industri gula, larutan gula 1000 kg/jam berkadar 30% dipekatkan hingga berkadar 60%. Larutan tersebut lalu dimasukkan ke kristalizer sehingga diperoleh kristal gula berkadar air 5%. Larutan jenuh berkadar gula 40% selanjutnya direcycle ke evaporator lagi. Hitung jumlah larutan yang direcycle dan gula yang dihasilkan.

FLUID FLOW THEORY Many raw materials for foods and many finished foods are in the form of fluids. Thin liquids - milk, water, fruit juices, Thick liquids - syrups, honey, oil, jam, Gases - air, nitrogen, carbon dioxide, Fluidized solids - grains, flour, peas. The study of fluids can be divided into: the study of fluids at rest - fluid statics, and the study of fluids in motion - fluid dynamics.

FLUID STATICS very important property : the fluid pressure
Pressure is force exerted on an area force is equal to the mass of the material multiplied by the acceleration due to gravity. mass of a fluid can be calculated by multiplying its volume by its density F = mg = Vρg F is force (Newton) or kg m s-2, m is the mass, g the acceleration due to gravity, V the volume and ρ the density.

The force per unit area in a fluid is called the fluid pressure
The force per unit area in a fluid is called the fluid pressure. It is exerted equally in all directions. F = APs + ZρAg Ps is the pressure above the surface of the fluid (e.g. it might be atmospheric pressure total pressure P = F/A = Ps + Zρg the atmospheric pressure represents a datum P = Zρg

EXAMPLE . Total pressure in a tank of peanut oil
Calculate the greatest pressure in a spherical tank, of 2 m diameter, filled with peanut oil of specific gravity 0.92, if the pressure measured at the highest point in the tank is 70 kPa.

Density of water. = 1000 kg m-3 Density of oil. = 0
Density of water     = 1000 kg m-3 Density of oil         = 0.92 x 1000 kg m-3 = 920 kg m-3 Z =greatest depth = 2 m and                   g = 9.81 m s-2 Now P = Zρg            = 2 x 920 x 9.81 kg m-1 s-2            = 18,050 Pa    = 18.1 kPa. To this must be added the pressure at the surface of 70 kPa. Total pressure                   = = 88.1 kPa. the pressure depends upon the pressure at the top of the tank, the depth of the liquid

Expressing the pressure

EXAMPLE. Head of Water Calculate the head of water equivalent and mercury to standard atmospheric pressure of 100 kPa. Density of water = 1000 kg m-3, Density of mercury = 13,600 kg m-3 g = 9.81 m s-2 and pressure   = 100 kPa                         = 100 x 103 Pa   =  100 x 103 kg m-1s-2. Water       Z     = P/ ρ g                         = (100 x 103)/ (1000 x 9.81)                         = 10.2 m Mercury   Z      = (100 x 103)/ (13,600 x 9.81)                         = 0.75m

FLUID DYNAMICS In most processes fluids have to be moved
Problems on the flow of fluids are solved by applying the principles of conservation of mass and energy The motion of fluids can be described by writing appropriate mass and energy balances and these are the bases for the design of fluid handling equipment.

Mass Balance ρ1A1v1 = ρ2A2v2 incompressible ρ1 = ρ2 so in this case
(continuity equation) area of the pipe at section 1 is A1 , the velocity at this section, v1 and the fluid density ρ1 , and if the corresponding values at section 2 are A2, v2, ρ2

EXAMPLE. Velocities of flow
Whole milk is flowing into a centrifuge through a full 5 cm diameter pipe at a velocity of 0.22 m s-1, and in the centrifuge it is separated into cream of specific gravity 1.01 and skim milk of specific gravity Calculate the velocities of flow of milk and of the cream if they are discharged through 2 cm diameter pipes. The specific gravity of whole milk of

Solving ρ1A1v1 = ρ2A2v2 + ρ3A3v3 where suffixes 1, 2, 3 denote respectively raw milk, skim milk and cream. since the total leaving volumes equal the total entering volume A1v1 = A2v2 + A3v3         v2 = (A1v1 - A3v3 )/A2    ρ1A1v1 = ρ2A2(A1v1 – A3v3)/A2 + ρ3A3v3 ρ1 A1v1 = ρ2 A1v1 - ρ2 A3v3 + ρ3 A3v3 A1v1(ρ1 - ρ2 ) = A3v3(ρ3 - ρ2 )

A1 = (π/4) x (0.05)2 = 1.96 x 10-3 m2 A2 = A3 = (π/4) x (0.02)2 = 3.14 x 10-4 m2  v1 = 0.22 m s-1 ρ1 = 1.035, ρ2 = 1.04, ρ3 = 1.01 A1v1(ρ1 - ρ2 ) = A3v3(ρ3 - ρ2 ) -1.96 x 10-3 x 0.22 (0.005) = x 10-4 x v3 x (0.03) v3 = 0.23 m s-1 v2 = (A1v1 - A3v3 )/A2   v2 = [(1.96 x 10-3 x 0.22) - (3.14 x 10-4 x 0.23)] / 3.14 x 10-4             = 1.1m s-1

Energy Balance Referring Fig. before we shall consider the changes in the total energy of unit mass of fluid, one kilogram, between Section 1 and Section 2. Firstly, there are the changes in the intrinsic energy of the fluid itself which include changes in:      (1) Potential energy = Ep = Zg    (J)      (2) Kinetic energy = Ek = v2/2  (J)      (3) Pressure energy = Er = P/ρ  (J) Secondly, there may be energy interchange with the surroundings including:      (4) Energy lost to the surroundings due to friction = Eƒ (J).      (5) Mechanical energy added by pumps = Ec (J).      (6) Heat energy in heating or cooling the fluid In the analysis of the energy balance, it must be remembered that energies are normally measured from a datum or reference level. Ep1 + Ek1 + Er1 = Ep2 + Ek2 + Er2 + Ef - Ec. Z1g + v12/2 + P1/ρ1 = Z2g + v22/2 + P2/ρ2 + Ef - Ec. Zg + v2/2 + P/ρ  = k Persamaan Bernouilli

Water flows at the rate of 0. 4 m3 min-1 in a 7
Water flows at the rate of 0.4 m3 min-1 in a 7.5 cm diameter pipe at a pressure of 70 kPa. If the pipe reduces to 5 cm diameter calculate the new pressure in the pipe. Density of water is 1000 kg m-3. Flow rate of water = 0.4 m3 min-1 = 0.4/60 m3 s-1. Area of 7.5 cm diameter pipe = (π/4)D2                                            = (π /4)(0.075)2                                            = 4.42 x 10-3 m2. So velocity of flow in 7.5 cm diameter pipe,                                        v1 = (0.4/60)/(4.42 x 10-3) = 1.51 m s-1 Area of 5 cm diameter pipe    = (π/4)(0.05)2                                            = 1.96 x 10-3 m2 and so velocity of flow in 5 cm diameter pipe,                                        v2 = (0.4/60)/(1.96 x 10-3) = 3.4 m s-1 Now            Z1g + v12/2 + P1 /ρ1 = Z2g + v22/2 + P2 / ρ2 and so 0 + (1.51)2/ x 103/1000 = 0 + (3.4)2/2 + P2/1000                          = P2/1000                                P2/1000 = ( ) = 65.3                                     P2 = 65.3k Pa.

Water is raised from a reservoir up 35 m to a storage tank through a 7
Water is raised from a reservoir up 35 m to a storage tank through a 7.5 cm diameter pipe. If it is required to raise 1.6 cubic metres of water per minute, calculate the horsepower input to a pump assuming that the pump is 100% efficient and that there is no friction loss in the pipe. 1 Horsepower = kW. Volume of flow, V = 1.6 m3 min-1 = 1.6/60 m3 s-1 = 2.7 x 10-2 m3 s-1 Area of pipe, A = (π/4) x (0.075)2 = 4.42 x 10-3 m2, Velocity in pipe, v = 2.7 x 10-2/(4.42 x 10-3) = 6 m s-1, And so applying eqn Z1g + v12/2 + P1/ρ1 = Z2g + v22/2 + P2/ρ2 + Ef - Ec. Ec = Zg +  v2/2 Ec = 35 x /2     =     = J Therefore total power required     = Ec x mass rate of flow     = EcVρ     = x 2.7 x 10-2 x 1000 J s-1     = 9758 J s-1 and, since     1 h.p. = 7.46 x 102 J s-1, required power = 13 h.p.

VISCOSITY Viscosity is that property of a fluid that gives rise to forces that resist the relative movement of adjacent layers in the fluid. Viscous forces are of the same character as shear forces in solids and they arise from forces that exist between the molecules. If two parallel plane elements in a fluid are moving relative to one another, it is found that a steady force must be applied to maintain a constant relative speed. This force is called the viscous drag because it arises from the action of viscous forces.

If the plane elements are at a distance Z apart, and if their relative velocity is v, then the force F required to maintain the motion has been found, experimentally, to be proportional to v and inversely proportional to Z for many fluids. The coefficient of proportionality is called the viscosity of the fluid, and it is denoted by the symbol µ (mu). From the definition of viscosity we can write F/A = µ v/Z

Unit of Viscosity N s m-2 = Pascal second, Pa s,
The older units, the poise and its sub-unit the centipoise, 1000 centipoises = 1 N s m-2, or 1 Pa s. the viscosity of water at room temperature 1 x 10-3 N s m-2 acetone, 0.3 x 10-3 N s m-2; tomato pulp, 3 x 10-3; olive oil, 100 x 10-3; molasses 7000 N s m-3. Viscosity is very dependent on temperature decreasing sharply as the temperature rises. For example, the viscosity of golden syrup is about 100 N s m-3 at 16°C, 40 at 22°C and 20 at 25°C.

Newtonian and Non-Newtonian Fluids
F/A = µ v /Z = µ(dv/dz) = t t = k(dv/dz)n power-law equation Newtonian fluids (n = 1, k = µ ) Non-Newtonian fluids (n ≠ 1) (1) Those in which n < 1. The viscosity is apparently high under low shear forces decreasing as the shear force increases. Pseudoplastic (tomato puree) (2) Those in which n > 1. With a low apparent viscosity under low shear stresses, they become more viscous as the shear rate rises. Dilatancy (gritty slurries such as crystallized sugar solutions). Bingham fluids have to exceed a particular shear stress level (a yield stress) before they start to move. Food : Non-Newtonian

STREAMLINE AND TURBULENT FLOW
STREAMLINE, flow is calm, in slow the pattern and smooth TURBULENT, the flow is more rapid, eddies develop and swirl in all directions and at all angles to the general line of flow. rv2D/mv = Dvr/m =Reynolds number (Re), dimensionless D is the diameter of the pipe For (Re)  < 2100 streamline flow, For 2100 < (Re) < 4000 transition, For (Re)  > 4000 turbulent flow.

EXAMPLE. Flow of milk in a pipe Milk is flowing at 0
EXAMPLE . Flow of milk in a pipe Milk is flowing at 0.12 m3 min-1 in a 2.5-cm diameter pipe. If the temperature of the milk is 21°C, is the flow turbulent or streamline? Viscosity of milk at 21°C = 2.1 cP = 2.10 x 10-3 N s m-2 Density of milk at 21°C = 1029 kg m-3. Diameter of pipe = m. Cross-sectional area of pipe = (p/4)D2 = p/4 x (0.025)2 = 4.9 x 10-4 m2 Rate of flow = 0.12 m3 min-1 = (0.12/60) m3 s-1 = 2 x 10 m3 s-1 So velocity of flow = (2 x 10-3)/(4.9 x 10-4) = 4.1 m s-1, and so (Re) = (Dvr/m) = x 4.1 x 1029/(2.1 x 10-3) = 50,230 and this is greater than 4000 so that the flow is turbulent.

ENERGY LOSSES IN FLOW Friction in Pipes
Energy Losses in Bends and Fittings Pressure Drop through Equipment Equivalent Lengths of Pipe

Friction in Pipes Eƒ : the energy loss due to friction in the pipe.
Eƒ : proportional to the velocity pressure of the fluid and to a factor related to the smoothness of the surface over which the fluid is flowing. F/A = f rv2/2 F is the friction force, A is the area over which the friction force acts, r is the density of the fluid, v is the velocity of the fluid, and f is a coefficient called the friction factor (depends upon the Reynolds number for the flow, and upon the roughness of the pipe). P1 - P2 = (4frv2/2)(L1 - L2)/D DPf = (4frv2/2) x (L/D) (Fanning-D'Arcy equation) Eƒ = DPf/r = (2fv2)(L/D) L = L1 - L2 = length of pipe in which the pressure drop, DPf = P1 - P2 is the frictional pressure drop, and Eƒ is the frictional loss of energy.

Friction factors in pipe (Moody graph)

predicted f f    = 16/(Re)   streamline flow, Hagen-Poiseuille equation 0 < (Re) < 2100 ƒ = ( Re)-0.25/4 ( Blasius equation for smooth pipes in the range 3000 < (Re) < 100,000) roughness ratio = Roughness factor (e)/pipe diameter (turbulent region)

ROUGHNESS FACTORS FOR PIPES
Material Roughness factor (e) Riveted steel Galvanized iron 0.0002 Concrete Asphalted cast iron 0.001 Wood staves Commercial steel Cast iron 0.0003 Drawn tubing Smooth

EXAMPLE Pressure drop in a pipe Calculate the pressure drop along 170 m of 5 cm diameter horizontal steel pipe through which olive oil at 20°C is flowing at the rate of 0.1 m3 min-1 Diameter of pipe = 0.05 m, Area of cross-section A                          = (π/4)D2                          = π /4 x (0.05)2                          = 1.96 x 10-3 m2 From Appendix 4, Viscosity of olive oil at 20°C = 84 x 10-3 Ns m-2 and density = 910 kg m-3,  and velocity = (0.1 x 1/60)/(1.96 x 10-3) = 0.85 m s-1, Now                   (Re) = (Dvρ/µ)                          = [(0.05 x 0.85 x 910)/(84 x 10-3)]                          = 460 so that the flow is streamline, and from Fig. moody, for (Re) = 460                       f  = 0.03. Alternatively for streamline flow from f  = 16/(Re)  = 16/460  = 0.03 as before. And so the pressure drop in 170 m,                  DPf = (4frv2/2) x (L/D)                         = [4 x 0.03 x 910 x (0.85)2 x 1/2] x [170 x 1/0.05]                          = 1.34 x 105 Pa                          = 134 kPa.

Thermal conductivity Specific heat Density Viscosity Temperature (J m-1 s-1 °C-1) (kJ kg-1 °C-1) (kg m-3) (N s m-2) (°C) Water 0.57 4.21 1000 1.87 x 10-3 987 0.56 x 10-3 50 0.68 4.18 958 0.28 x 10-3 100 Sucrose 20% soln. 0.54 3.8 1070 1.92 x 10-3 20 0.59 x 10-3 80              60% soln. 6.2 x 10-3 5.4 x 10-3 Sodium chloride 22% soln. 3.4 1240 2.7 x 10-3 2 Olive oil 0.17 2.0 910 84 x 10-3 Rape-seed oil 900 118 x 10-3 Soya-bean oil 40 x 10-3 30 Tallow 18 x 10-3 65 Milk (whole) 0.56 3.9 1030 2.12 x 10-3 Milk (skim) 1040 1.4 x 10-3            25 Cream 20% fat 1010 3            30% fat 13,8 x 10-3

Energy Losses in Bends and Fittings
energy losses due to altering the direction of flow, fittings of varying cross-section This energy is dissipated in eddies and additional turbulence and finally lost in the form of heat. Eƒ = kv2/2 Losses in fittings Ef = (v1 - v2)2/2 Losses in sudden enlargements Ef = kv22/2 Losses in sudden contraction

FRICTION LOSS FACTORS IN FITTINGS
k Valves, fully open: gate 0.13 globe 6.0 angle 3.0 Elbows: 90° standard 0.74 medium sweep 0.5 long radius 0.25 square 1.5 Tee, used as elbow Tee, straight through Entrance, large tank to pipe: sharp rounded 0.05 LOSS FACTORS IN CONTRACTIONS D2/D1 0.1 0.3 0.5 0.7 0.9 k 0.36 0.31 0.22 0.11 0.02

FLUID-FLOW APPLICATIONS
Two practical aspects of fluid flow in food technology : measurement in fluids: pressures and flow rates, and production of fluid flow by means of pumps and fans. Pumps and fans are very similar in principle and usually have a centrifugal or rotating action a gas : moved by a fan, a liquid: moved by a pump.

MEASUREMENT OF PRESSURE IN A FLUID
Method : Piezometer ("pressure measuring") tube U-tube Pitot tube Pitot-static tube Bourdon-tube P = Z1r1g

EXAMPLE. Pressure in a vacuum evaporator The pressure in a vacuum evaporator was measured by using a U-tube containing mercury. It was found to be less than atmospheric pressure by 25 cm of mercury. Calculate the extent by which the pressure in the evaporator is below atmospheric pressure (i.e. the vacuum in the evaporator) in kPa, and also the absolute pressure in the evaporator. The atmospheric pressure is 75.4 cm of mercury and the specific gravity of mercury is 13.6, and the density of water is 1000 kg m-3. We have P = Zrg = 25 x 10-2 x 13.6 x 1000 x = 33.4 kPa Therefore the pressure in the evaporator is 33.4 kPa below atmospheric pressure and this is the vacuum in the evaporator. For atmospheric pressure: P = Zrg P = 75.4 x 10-2 x 13.6 x 1000 x = kPa Therefore the absolute pressure in the evaporator = = 67.2 kPa

MEASUREMENT OF VELOCITY IN A FLUID
Pitot tube and manometer : Z1g + v12/2 + P1/r1 = Z2g + v22/2 + P2/r1 Z2 = Z + Z' Z' be the height of the upper liquid surface in the pipe above the datum, Z be the additional height of the fluid level in the tube above the upper liquid surface in the pipe; Z' may be neglected if P1 is measured at the upper surface of the liquid in the pipe, or if Z' is small compared with Z v2 = 0 as there is no flow in the tube P2 = 0 if atmospheric pressure is taken as datum and if the top of the tube is open to the atmosphere Z1 = 0 because the datum level is at the mouth of the tube. v12/2g + P1/r1 = (Z + Z')g » Z. Pitot-static tube Z = v2/2g

EXAMPLE . Velocity of air in a duct Air at 0°C is flowing through a duct in a chilling system. A Pitot-static tube is inserted into the flow line and the differential pressure head, measured in a micromanometer, is 0.8 mm of water. Calculate the velocity of the air in the duct. The density of air at 0°C is 1.3 kg m-3. Z = v12/2g r1Z1 = r2Z2. Now 0.8 mm water = 0.8 x 10-3 x 1000 1.3 = 0.62 m of air v12 = 2Zg = 2 x 0.62 x 9.81 = m2s-2 Therefore v1 = 3.5 m s-1

Venturi and orifice meters
v12/2 + P1/r1 = v22/2+ P2/r2 (Bernouilli's equation) A1v1 = A2v2 (mass balance, eqn) r1 = r2 = r v12/2 + P1/r = (v1A1/A2)2/2 + P2/r v12 = [2(P2 -P1)/r] x A22/(A22 -A12) (P2 -P1)/r = gZrm /r Z = (P2 -P1)/rm g v1 = C √[2(P2 -P1 )/r]x A22/(A22 -A12 ) In a properly designed Venturi meter, C lies between 0.95 and 1.0.

Pompa dan Fan mechanical energy from some other source is converted into pressure or velocity energy in a fluid. The food technologist is not generally much concerned with design details of pumps, but should know what classes of pump are used and something about their characteristics. The efficiency of a pump is the ratio of the energy supplied by the motor to the increase in velocity and pressure energy given to the fluid.

Jenis Pompa Positive Displacement Pumps
the fluid is drawn into the pump and is then forced through the outlet Positive displacement pumps can develop high-pressure heads but they cannot tolerate throttling or blockages in the discharge.

Jet Pumps a high-velocity jet is produced in a Venturi nozzle, converting the energy of the fluid into velocity energy. This produces a low-pressure area causing the surrounding fluid to be drawn into the throat Jet pumps are used for difficult materials that cannot be satisfactorily handled in a mechanical pump. They are also used as vacuum pumps. Jet pumps have relatively low efficiencies but they have no moving parts and therefore have a low initial cost.

Air-lift Pumps air or gas can be used to impart energy to the liquid
The air or gas can be either provided from external sources or produced by boiling within the liquid. Examples of the air-lift principle are: Air introduced into the fluid as shown in Fig. 4.3(e) to pump water from an artesian well. Air introduced above a liquid in a pressure vessel and the pressure used to discharge the liquid. Vapours produced in the column of a climbing film evaporator. In the case of powdered solids, air blown up through a bed of powder to convey it in a "fluidized" form. A special case of this is in the evaporator, where boiling of the liquid generates the gas (usually steam) and it is used to promote circulation. Air or gas can be used directly to provide pressure to blow a liquid from a container out to a region of lower pressure. Air-lift pumps and air blowing are inefficient, but they are convenient for materials which will not pass easily through the ports, valves and passages of other types of pumps.

Propeller Pumps and Fan
Propellers can be used to impart energy to fluids They are used extensively to mix the contents of tanks and in pipelines to mix and convey the fluid. Propeller fans are common and have high efficiencies. They can only be used for low heads, in the case of fans only a few centimetres or so of water

Centrifugal Pumps and Fans
The centrifugal pump converts rotational energy into velocity and pressure energy The fluid to be pumped is taken in at the centre of a bladed rotor and it then passes out along the spinning rotor, acquiring energy of rotation. This rotational energy is then converted into velocity and pressure energy at the periphery of the rotor. Centrifugal fans work on the same principles. These machines are very extensively used and centrifugal pumps can develop moderate heads of up to 20 m of water. They can deliver very large quantities of fluids with high efficiency.

Gambar jenis-jenis pompa

EXAMPLE Centrifugal pump for raising water Water for a processing plant is required to be stored in a reservoir to supply sufficient working head for washers. It is believed that a constant supply of 1.2 m3 min-1 pumped to the reservoir, which is 22 m above the water intake, would be sufficient. The length of the pipe is about 120 m and there is available galvanized iron piping 15 cm diameter. The line would need to include eight right-angle bends. There is available a range of centrifugal pumps whose characteristics are shown in Fig Would one of these pumps be sufficient for the duty and what size of electric drive motor would be required?

Reynold number Assume properties of water at 20°C are density 998 kg m-3, and viscosity N s m-2 Cross-sectional area of pipe A = (π/4)D2                                              = π /4 x (0.15)2                                              = m-2                     Volume of flow V = 1.2 m3 min-1                                              = 1.2/60 m3 s-1                                              = 0.02 m3 s-1.                 Velocity in the pipe = V/A                                              = (0.02)/(0.0177)                                              = 1.13 ms-1                                Now (Re) = Dvρ/µ                                              = (0.15 x 1.13 x 998)/0.001                                              = 1.7 x 105 so the flow is clearly turbulent.

friction loss of energy
From Table 3.1, the roughness factor ε is for galvanized iron and so               roughness ratio   ε /D = /0.15 = 0.001 So from Fig. 3.8,                                                  ƒ = Therefore the friction loss of energy = (4ƒv2/2) x (L/D) = [4ƒv2L/2D] = [4 x x (1.13)2 x 120]/(2 x 0.15) = 10.8 J.

TABLE 3.1 RELATIVE ROUGHNESS FACTORS FOR PIPES
Material Roughness factor (e) Riveted steel Galvanized iron 0.0002 Concrete Asphalted cast iron 0.001 Wood staves Commercial steel Cast iron 0.0003 Drawn tubing Smooth

Friction factors in pipe

TABLE 3.2 FRICTION LOSS FACTORS IN FITTINGS
k Valves, fully open: gate 0.13 globe 6.0 angle 3.0 Elbows: 90° standard 0.74 medium sweep 0.5 long radius 0.25 square 1.5 Tee, used as elbow Tee, straight through Entrance, large tank to pipe: sharp rounded 0.05

Energy loss from bends and discharge
For the eight right-angled bends, from Table 3.2 we would expect a loss of 0.74 velocity energies at each, making (8 x 0.74) = 6 in all.                    velocity energy = v2/2                                          = (1.13)2/2                                          = 0.64 J So total loss from bends and discharge energy                                          = (6 + 1) x                                          = 4.5 J There would be one additional velocity energy loss because of the unrecovered flow energy discharged into the reservoir.

Energy to move 1 kg water Energy to move 1 kg water against a head of 22 m of water is                                       E = Zg                                          = 22 x 9.81                                          = J. Total energy requirement per kg:                                    Etot =                                          = J

energy requirement of pump
and theoretical power requirement                                          = Energy x volume flow x density                                          = (Energy/kg) x kgs-1                                          = x 0.02 x 998                                          = 4613 J s-1. Now the head equivalent to the energy requirement                                          = Etot/g                                          = 231.1/9.81                                          = 23.5 m of water, and from Fig. 4.4 this would require the 150 mm impeller pump to be safe, and the pump would probably be fitted with a 5.5 kW motor.

Energy Balance

The Ideal Gas Equation Pressure, the force of collision between gas molecules and a surface, is directly proportional to temperature and the number of molecules per unit volume. PV = nRT the ideal gas equation. R is the gas constant and has values of L(atm)/(gmole.K); or 8315 N(m)/(kgmole.K) or 1545 ft(lbf)/(lbmole.◦R). a fixed quantity of a gas that follows the ideal gas equation undergoes a process where the volume, temperature, or pressure is allowed to change, the product of the number of moles n and the gas constant R is a constant

Calculate the quantity of oxygen entering a package in 24 hours if the packaging material has a surface area of 3000 cm2 and an oxygen permeability 100 cm3/(m2)(24 h) STP (standard temperature and pressure = 0oC and 1 standard atmosphere of kPa). Jawaban:

Calculate the volume of CO2 in ft3 at 70oF and 1 atm, which would be produced by vaporization of 1 lb of dry ice.

An empty can was sealed in a room at 80oC and 1 atm pressure
An empty can was sealed in a room at 80oC and 1 atm pressure. Assuming that only air is inside the sealed can, what will be the vacuum after the can and contents cool to 20oC? Solution:

vapor pressure of water at 20oC = 2336.6 Pa.
Calculate the quantity of air in the headspace of a can at 20oC when the vacuum in the can is 10 in. Hg. Atmospheric pressure is 30 in. Hg. The headspace has a volume of 16.4 cm3. The headspace is saturated with water vapor vapor pressure of water at 20oC = Pa. Let Pt be the absolute pressure inside the can.

Assume there are no dissolved gases in the product at the time of sealing, therefore the only gases in the headspace are air and water vapor. The vapor pressure of water at 20◦C and 80◦C are and kPa, respectively. In the gas mixture in the headspace, air is assumed to remain at the same quantity in the gaseous phase, while water condenses on cooling

A gas mixture used for controlled atmosphere storage of vegetables contains 5% CO2, 5% O2, and 90% N2. The mixture is generated by mixing appropriate quantities of air and N2 and CO2 gases. 100 m3 of this mixture at 20oC and 1 atm is needed per hour. Air contains 21% O2 and 79% N2. Calculate the volume at which the component gases must be metered into the system in m3/h at 20oC and 1 atm. All percentages are by volume. No volume changes occur on mixing of ideal gases. Because volume percent in gases is the same as mole percent, material balance equations may be made on the basis of volume and volume percentages. Let X = volume O2, Y = volume CO2, and Z = volume N2, fed into the system per hour. Oxygen balance: 0.21(X) = 100(0.05); X = 23.8 m3 CO2 balance: Y = 0.05(100); Y = 5 m3 Total volumetric balance: X + Y + Z = 100 Z = 100 − 23.8 − 5 = 71.2 m3

Temperature Pressure Enthalpy (sat. vap.) Latent heat Specific volume (°C) (kPa) (kJ kg-1) (m3 kg-1) 20 2.34 2538 2454 57.8 22 2.65 2542 2449 51.4 24 2.99 2545 2445 45.9 26 3.36 2549 2440 40.0 28 3.78 2553 2435 36.6 30 4.25 2556 2431 32.9 40 7.38 2574 2407 19.5 50 12.3 2592 2383 12.0 60 19.9 2610 2359 7.67 70 31.2 2627 2334 5.04 80 47.4 2644 2309 3.41 90 70.1 2660 2283 2.36 100 101.35 2676 2257 1.673 105 120.8 2684 2244 1.42 110 143.3 2692 2230 1.21 115 169.1 2699 2217 1.04 120 198.5 2706 2203 0.892 125 232.1 2714 2189 0.771 130 270.1 2721 2174 0.669 135 313.0 2727 2160 0.582 140 361.3 2734 2145 0.509 150 475.8 2747 2114 0.393 160 617.8 2758 2083 0.307

Heat Sensible heat is defined as the energy transferred between two bodies at different temperatures, or the energy present in a body by virtue of its temperature. Latent heat is the energy associated with phase transitions, heat of fusion, from solid to liquid, and heat of vaporization, from liquid to vapor. Enthalpy, is an intrinsic property, the absolute value of which cannot be measured directly. However, if a reference state is chosen for all components that enter and leave a system such that at this state the enthalpy is considered to be zero, then the change in enthalpy from the reference state to the current state of a component can be considered as the value of the absolute enthalpy for the system under consideration. The reference temperature (Tref) for determining the enthalpy of water in the steam tables is ◦F or 0.01◦C.

Specific Heat The specific heat (Cp) is the amount of heat that accompanies a unit change in temperature for a unit mass. The specific heat, which varies with temperature, is more variable for gases compared with liquids or solids. Most solids and liquids have a constant specific heat over a fairly wide temperature range.

specific heat J/(kg K)

Estimation of Cp Cavg = 3349M in J/(kg K) for fat free plant material Cavg = F SNF + 4l86.8M in J/(kg K) the mass fraction fat (F), mass fraction solids non-fat (SNF), and mass fraction moisture (M) Example: Calculate the heat required to raise the temperature of a kg roast beef containing 15% protein, 20% fat, and 65% water from 4.44◦C to 65.55◦C Solution: Cavg = 0.15(837.36) + 0.2( ) (4186.8) = 3182 J/(kg K) q = kg[3182 J/(kg K)] (65.55 − 4.44)K = MJ

Specific heat of gas and vapor
whereCpm is mean specific heat from the reference temperature To to T1. Tabulated values for the mean specific heat of gases are based on ambient temperature of 77◦F or 25◦C, as the reference temperature.

Contoh Hitung kebutuhan panas untuk menaikkan suhu udara pengering pd tekanan 1 atm dari suhu ruang 25oC ke suhu pengeringan 50oC jika tiap menit dialirkan udara sebanyak 100m3 q= mCp (50-25) m=PVM/RT R = m3 atm/kg mole K

PROPERTIES OF SATURATED AND SUPERHEATED STEAM
Steam and water are the two most used heat transfer mediums in food processing. Water is also a major component of food products. The steam tables that list the properties of steam are a very useful reference when determining heat exchange involving a food product and steam or water. At temperatures above the freezing point, water can exist in either of the following forms. Saturated Liquid:. Liquid water in equilibrium with its vapor. The total pressure above the liquid must be equal to or be higher than the vapor pressure. If the total pressure above the liquid exceeds the vapor pressure, some other gas is present in the atmosphere above the liquid. If the total pressure above a liquid equals the vapor pressure, the liquid is at the boiling point. Saturated Vapor: This is also known as saturated steam and is vapor at the boiling temperature of the liquid. Lowering the temperature of saturated steam at constant pressure by a small increment will cause vapor to condense to liquid. The phase change is accompanied by a release of heat. If heat is removed from the system, temperature and pressure will remain constant until all vapor is converted to liquid. Adding heat to the system will change either temperature or pressure or both. Vapor-Liquid Mixtures: Steam with less than 100% quality. Temperature and pressure correspond to the boiling point; therefore, water could exist either as saturated liquid or saturated vapor. Addition of heat will not change temperature and pressure until all saturated liquid is converted to vapor. Removing heat from the system will also not change temperature and pressure until all vapor is converted to liquid. Steam Quality: The percentage of a vapor-liquid mixture that is in the form of saturated vapor. Superheated Steam: Water vapor at a temperature higher than the boiling point. The number of degrees the temperature exceeds the boiling temperature is the degrees superheat. Addition of heat to superheated steam could increase the superheat at constant pressure or change both the pressure and temperature at constant volume. Removing heat will allow the temperature to drop to the boiling temperature where the temperature will remain constant until all the vapor has condensed.

Steam table The saturated steam table consists of entries under the headings of temperature, absolute pressure, specific volume, and enthalpy.

Temperature Pressure Enthalpy (sat. vap.) Latent heat Specific volume (°C) (kPa) (kJ kg-1) (m3 kg-1) 20 2.34 2538 2454 57.8 22 2.65 2542 2449 51.4 24 2.99 2545 2445 45.9 26 3.36 2549 2440 40.0 28 3.78 2553 2435 36.6 30 4.25 2556 2431 32.9 40 7.38 2574 2407 19.5 50 12.3 2592 2383 12.0 60 19.9 2610 2359 7.67 70 31.2 2627 2334 5.04 80 47.4 2644 2309 3.41 90 70.1 2660 2283 2.36 100 101.35 2676 2257 1.673 105 120.8 2684 2244 1.42 110 143.3 2692 2230 1.21 115 169.1 2699 2217 1.04 120 198.5 2706 2203 0.892 125 232.1 2714 2189 0.771 130 270.1 2721 2174 0.669 135 313.0 2727 2160 0.582 140 361.3 2734 2145 0.509 150 475.8 2747 2114 0.393 160 617.8 2758 2083 0.307

contoh Pada tekanan vakum berapa sehingga air mendidih pada suhu 80oC, nyatakan dalam kPa dan dalam cm Hg Lihat tabel uap= 47,4 kPa abs Tekanan vakum = ,4 = 53,6 kPa Tekanan vakum = (53,6/101) x 76 = 40,3 cmHg Sterilisasi dilakukan pada suhu 120oC, berapa tekanan yang terbaca pada manometer yang menggunakan satuan psi? Dari tabel pada suhu 120oC tekanan uap = 198,5 kPa, maka tekanan pada manometer = 198,5 – 101 = 97,5 kPa 1 atm = 14,7 psi = 101 kPa Tekanan pada manometer = (97,5/101) x 14,7 = 14,2 psig

Freezing Points of Food Products Unmodified from the Natural State
the heat to be removed during freezing of a food product : sensible heat and latent heat. determining the amount of heat by calculating the enthalpy change. calculating enthalpy change below the freezing point (good only for moisture contents between 73% and 94%) is the procedure of Chang and Tao (1981). In this correlation, it is assumed that all water is frozen at 227 K (−50◦ F).

Calculate the freezing point and the amount of heat that must be removed in order to freeze 1 kg of grape juice containing 25% solids from the freezing point to −30◦C. Solution: Y = 0.75. for juices: Tf = (0.75) − (0.75)2 = K Hf = ,096(0.75) = 313, 614 J a = (0.02) − 3.465(0.02)2 = b = 27.2 − (0.1316) − (0.1316)2 = 1.879 Tr = (− − 227.6)/(266.7 − 227.6) = 0.394 H = 313,614[(0.3616) (1 − )(0.394)1.879 ]= 79, 457 J/kg The enthalpy change from Tf to −30 ◦C is ΔH = 313,614 − 79, 457 = 234, 157 J/kg