Presentation is loading. Please wait.

Presentation is loading. Please wait.

Www.anton-paar.com Synthos 3000 Enhanced Microwave Assisted Organic Synthesis.

Similar presentations


Presentation on theme: "Www.anton-paar.com Synthos 3000 Enhanced Microwave Assisted Organic Synthesis."— Presentation transcript:

1 Synthos 3000 Enhanced Microwave Assisted Organic Synthesis

2 Big Deal Organic Synthesis in

3 3 Contents  Synthos General Features  Rotor System - General Information  Rotor 16 - Details & Vessels  Rotor 8 - Details & Vessels  Accessories

4 4 A Versatile and Modular Microwave Platform System  Built-in magnetic stirrer  Dual remote temperature sensing  Sophisticated accessories  High performance rotors & vessels IR

5 5  1400W unpulsed microwave output power  66L PTFE coated cavity  Built in cooling unit  Proven safety door  Easy access to connectors  Dual magnetron system Synthos General Features  Large rotor drive ring

6 6 Pulsed vs. Unpulsed Power Power 1000 W 500 W Time Pulsed Average microwave power control, ev. with a few unpulsed levels (300 & 600W) Unpulsed Continuous (true) microwave power forbetter reaction control Power 1000 W 500 W Time  Reduced risk of spontaneous reactions  Minimized occurence of hot spots

7 7 Built-In Cooling Unit  No overheating during reaction  Reduction of material stress  Cooling within 20 minutes  Safe exhaust of vapors after reaction  Supports control of exothermic reactions by drawing off heat  Integral part of the solvent safety system Unique !

8 8 Proven Safety Door  Stable stainless steel door with window  Pushbutton operation  Magnetically supported opening and closing  Overpressure release and resealing action  4 interlock switches  Tested for more than cycles

9 9 Built-In Controller Features  Big, bright display  Corrosion resistant and spill proof design  8 function keys  Optional external keyboard  Standard serial RS232 and parallel printer port Benefits  Easily readable from across the lab  No extra space required  Compatible with LIMS

10 10 Intuitive Software  Easy documentation  Automated calibration  Multitasking facilities Numeric Data Screen  Serial port for data transfer to PC  Excel Plug-in for online data acquisition  Printer Port  Ready to use library with tested methods  User can edit and store own methods

11 11 Documentation P-graph IR-graphT-graph

12 12 Synthos 3000 Rotors Rotor Code: Rotor 16HF100 Number of vessels (8 or 16) Vessel pressure M... Medium press. (20/70 bar) H... High press. (40/70 bar) SX... Extremely high pressure (60 or 80/120 bar) Vessel material F... fluoroplastic Q... Quartz glass Vessel volume (in mL)

13 13 16MF100 / 16HF100 Synthos 3000 Rotors 16-position Rotors  Magazine-type rotor  Screw Cap vessels  Fluoroplastic vessels  Medium or high pressure  IR temperature control  Magnetic Stirrer Options  Reference p/T-sensor in one vessel

14 14 8SXF100 / 8SQ80 Synthos 3000 Rotors 8-position Rotors  Closed "cage style" rotor  Plugged vessels  Fluoroplastic or quartz glass  "X"tremely high pressure  Pressure sensor on all positions  IR temperature control  Magnetic Stirrer Options  Immersing temperature probe in.one vessel

15 15 Synthesis Applications Rotor 8SXF100  High Pressure Reactions  Solid-Phase Synthesis  Pre-pressurized Reactions Rotor 16MF100/16HF100  Standard Synthesis  Medium Pressure Reactions  Solid-Phase Synthesis  Library Generation  High Throughput Applications Rotor 8SXQ80  High Pressure Reactions  Metal Catalysis  Pre-pressurized Reactions  Near Critical Water Chemistry

16 16 10-fold Overpressure Safety 1.Tested Synthos 3000 methods library 2.Controlled pressure release after reaction 3.Efficient Cooling ("negative energy") 4.Pressure increase control 5.Pressure limit (e.g. 60 bar for XF100-vessels) bar safety disk  overpressure tolerance bar test pressure (for 1 minute) 8.Bomb jacket resp. vessel holder 9.Closed rotor with protection lid 10.Stable oven cavity with resealing safety door Active feature Passive feature

17 17 Rotor 16 Design Protection lid with bayonet lock Shielded sensor module Sensor vessel Venting valve Seal Sapphire thermowell Cooling air guide Bowl shaped rotor body IR measurement port Rotor base

18 18 Optimized Vessel Design (MF/HF100) Exhaust Port for directed gas release Venting Screw Safety release grooves Liner (PTFE-TFM) Screw Cap Safety Disk & Holder Lip-type Seal Vessel Jacket reinforced PEEK or ceramics

19 19 MF100 & HF100 Vessels  Easy hand tightening of lip- type seals  Hermetic closure, no loss  Safety disks made of resistant metal alloy  High overpressure tolerance  Controlled venting inside the oven after digestion  Upgrade from MF to HF by changing vessel jackets

20 20 Rotor 16 - Reaction Vessels MF100 vessel Liner materialPTFE-TFM Pressure Jacketreinforced PEEK Volume100mL Controlled pressure20 bar (290 psi) Max. rated pressure70 bar (1000 psi) Test pressure140 bar (2000 psi) Max. temperature200°C HF100 vessel PTFE-TFM Ceramics 100 mL 40 bar (580 psi) 70 bar (1000 psi) 140 bar (2000 psi) 240 °C

21 21 Rotor 8 Design Unique ! Cooling air Wireless data transmission Upper (sensor) plate Shielded pressure transducer and electronics module Tension bar Hydraulic system Piston Plug with lip-type seal Air guide Reaction vessel (SXQ / SXF) Base plate with IR-ports IR temperature sensor

22 22 Rotor 8 - Reaction Vessels SXQ80 vessel Liner materialQuartz Pressure Jacket Volume80mL Controlled pressure80 bar (1160 psi) Max. rated pressure120 bar (1740 psi) Test pressure140 bar (2000 psi) Max. temperature300°C SXF100 vessel PTFE-TFM Ceramics 100 mL 60 bar (870 psi) 120 bar (1740 psi) 140 bar (2000 psi) 260 °C

23 23 Synthos 3000 Vessel Overview Assembled "X" vessel SXF100 vessel SXQ80 vessel p-T Sensor Accessory for MF100 and HF100 vessels MF100 vessel HF100 vessel

24 24 Pressure / Temperature Sensor * Limited by an internal microprocessor SapphireThermowell 280°CMax. Temperature 86 bar (1250 psi)Max. Pressure p/T Sensor 3.0 bar/secPressure rate* Infrared LEDData transmission All acids (incl. HF) and solventsReagents Unique !  Optional available for Rotor 16

25 25 Temperature Sensor Accessory  Temperature range: °C Accuracy: 1%  Shielded electronics module with wireless data transmission by IR-LED  Quartz glass thermowell, compatible with all solvents and most acids  Optional available for Rotor 8 Unique !

26 26 Seal Forming Device Features  For both types of seals  Fits to Rotor 8 and 16  Made of easy to clean materials Benefits  Safe storage of caps  Comfortable and fast vessel closure  Avoids handling errors Unique !

27 27 Temperature Calibration Tool Features  Automatic calibration for invasive T-sensors  Connected to “CAL” plug of Synthos 3000  Documentation and calculation automatically by the software Benefits  Calibration within 15 min without manual work or calculation  Accurate temperature measurement within 1% uncertainty

28 28 Gas Loading Accessory Benefits  Simplified application of gaseous reagents in microwave reactions  Substitition of toilsome autoclave systems Features  Individual pre-pressurizing up to 20 bar  Creation of inert or reactive gas atmosphere  Easy bayonet connection for use with already closed rotor

29 29 Filtration Unit / Rack 16 Rack 16 For all kinds of vessels & liners Filtration Unit Screw-on tool for convenient solid phase applications without change of vessels Various filters with different pore size Filtration of precipitated products

30 30 “An invasion of armies can be resisted, but not an idea resisted, but not an idea whose time has come“ whose time has come“ Victor Hugo ( ) Time has come for Synthos 3000


Download ppt "Www.anton-paar.com Synthos 3000 Enhanced Microwave Assisted Organic Synthesis."

Similar presentations


Ads by Google