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The forensic analysis of office paper using carbon isotope ratio mass spectrometry— Part 2: Method development, validation and sample handling  Kylie Jones,

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Presentation on theme: "The forensic analysis of office paper using carbon isotope ratio mass spectrometry— Part 2: Method development, validation and sample handling  Kylie Jones,"— Presentation transcript:

1 The forensic analysis of office paper using carbon isotope ratio mass spectrometry— Part 2: Method development, validation and sample handling  Kylie Jones, Sarah Benson, Claude Roux  Forensic Science International  Volume 231, Issue 1, Pages (September 2013) DOI: /j.forsciint Copyright © Terms and Conditions

2 Fig. 1 (a) Linear range for medium fiber cellulose – mean instrument response (mV). (b) Linear range for medium fiber cellulose – mean δ13CVPDB (‰). Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

3 Fig. 2 (a) Linear range for cellulose acetate – mean instrument response (mV). (b) Linear range for cellulose acetate – mean δ13CVPDB (‰). Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

4 Fig. 3 (a) Linear range for alpha glucose – mean instrument response (mV). (b) Linear range for alpha glucose – mean δ13CVPDB (‰). Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

5 Fig. 4 Linearity of CO+ production for paper, cellulose acetate and alpha glucose samples. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

6 Fig. 5 Day 1 (diamond) vs. day 16 (square) δ13C values for samples left exposed to the laboratory atmosphere. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

7 Fig. 6 Mean δ13CV-PDB (‰) paper sample values for storage/handling experiment. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

8 Fig. 7 Plot of corrected measurements of international standard polyethylene over a 24-month period. Mean value and 95% confidence interval represented by the solid and dashed lines. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

9 Fig. 8 Plot of corrected measurements of international standard sucrose over a 24-month period. Mean value and 95% confidence interval also represented by the solid and dashed lines. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

10 Fig. 9 Plot of corrected measurements of international standard cellulose over a 24-month period. Mean value and 95% confidence interval also represented by the solid and dashed lines. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

11 Fig. 10 Accuracy results for medium cellulose.
Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

12 Fig. 11 Accuracy results for cellulose acetate.
Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

13 Fig. 12 Accuracy results for alpha glucose.
Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions

14 Fig. 13 Mean δ13CVPDB (‰) values obtained for samples prepared and run by three different operators. Forensic Science International  , DOI: ( /j.forsciint ) Copyright © Terms and Conditions


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